Extraction of Sugars and Cellulose Fibers from Cannabis Stems by Hydrolysis, Pulping, and Bleaching
Falguni Pattnaik
University of Saskatchewan, Department of Chemical and Biological Engineering, S7N 5A9 Saskatoon, Saskatchewan, Canada
Indian Institute of Technology Delhi, Centre for Rural Development and Technology, 110016 New Delhi, India
Search for more papers by this authorSonil Nanda
University of Saskatchewan, Department of Chemical and Biological Engineering, S7N 5A9 Saskatoon, Saskatchewan, Canada
Search for more papers by this authorVivek Kumar
Indian Institute of Technology Delhi, Centre for Rural Development and Technology, 110016 New Delhi, India
Search for more papers by this authorSatyanarayan Naik
Indian Institute of Technology Delhi, Centre for Rural Development and Technology, 110016 New Delhi, India
Search for more papers by this authorCorresponding Author
Ajay K. Dalai
University of Saskatchewan, Department of Chemical and Biological Engineering, S7N 5A9 Saskatoon, Saskatchewan, Canada
Correspondence: Ajay K. Dalai ([email protected]), Department of Chemical and Biological Engineering, University of Saskatchewan, Saskatoon, Saskatchewan, S7N 5A9, Canada.Search for more papers by this authorMahendra K. Mohanty
Odisha University of Agriculture and Technology, Department of Farm Machinery and Power, 751003 Bhubaneswar, Odisha, India
Search for more papers by this authorFalguni Pattnaik
University of Saskatchewan, Department of Chemical and Biological Engineering, S7N 5A9 Saskatoon, Saskatchewan, Canada
Indian Institute of Technology Delhi, Centre for Rural Development and Technology, 110016 New Delhi, India
Search for more papers by this authorSonil Nanda
University of Saskatchewan, Department of Chemical and Biological Engineering, S7N 5A9 Saskatoon, Saskatchewan, Canada
Search for more papers by this authorVivek Kumar
Indian Institute of Technology Delhi, Centre for Rural Development and Technology, 110016 New Delhi, India
Search for more papers by this authorSatyanarayan Naik
Indian Institute of Technology Delhi, Centre for Rural Development and Technology, 110016 New Delhi, India
Search for more papers by this authorCorresponding Author
Ajay K. Dalai
University of Saskatchewan, Department of Chemical and Biological Engineering, S7N 5A9 Saskatoon, Saskatchewan, Canada
Correspondence: Ajay K. Dalai ([email protected]), Department of Chemical and Biological Engineering, University of Saskatchewan, Saskatoon, Saskatchewan, S7N 5A9, Canada.Search for more papers by this authorMahendra K. Mohanty
Odisha University of Agriculture and Technology, Department of Farm Machinery and Power, 751003 Bhubaneswar, Odisha, India
Search for more papers by this authorAbstract
Cannabis indica stems were hydrolyzed with subcritical water at various temperatures, reaction times, and feed concentrations. The highest total yield of reducing sugars of 16.4 wt % was obtained at 190 °C in 37.5 min with a feed concentration of 3.5 wt %. Solid residues from the optimized process were treated with 0.5 M NaOH (pulping) and 0.5–3 % H2O2 (bleaching) to isolate cellulose fibers. The maximum yield of cellulose was 34.8 wt % with lowest lignin content of 0.5 wt %. With the removal of hemicellulose and lignin through the integrated hydrothermal processes, the crystallinity index and thermal stability of the cellulose fibers increased.
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