• Issue

    Journal of Synchrotron Radiation: Volume 27, Issue 6

    1459-1754
    November 2020

international union of crystallography

Open Access

Announcement of two new Main Editors for Journal of Synchrotron Radiation

  • Page: 1459
  • First Published: 05 November 2020
Announcement of two new Main Editors for Journal of Synchrotron Radiation

Two new Main Editors of JSR are announced.

Open Access

Announcement of conversion of Journal of Synchrotron Radiation to 100% open access from January 2022

  • Page: 1460
  • First Published: 05 November 2020
Announcement of conversion of Journal of Synchrotron Radiation to 100% open access from January 2022

The proposed conversion of Journal of Synchrotron Radiation to 100% open access from January 2022 is announced.

research papers

Ronchi shearing interferometry for wavefronts with circular symmetry

  • Pages: 1461-1469
  • First Published: 14 September 2020
Ronchi shearing interferometry for wavefronts with circular symmetry

The circular symmetry in the wavefront of an X-ray free-electron laser beam focused with Be compound refractive lenses is explored in order to derive the wavefront from a single Ronchigram.

Speckle correlation as a monitor of X-ray free-electron laser induced crystal lattice deformation

  • Pages: 1470-1476
  • First Published: 09 October 2020
Speckle correlation as a monitor of X-ray free-electron laser induced crystal lattice deformation

Free-electron laser X-ray beam-induced lattice disorder is investigated by measuring shot-to-shot evolution of near-Bragg coherent diffuse scattering from single-crystal germanium. It is shown that X-ray photon correlation analysis of sequential speckle measurements can be used to monitor the nature and extent of the lattice displacement rearrangement.

Third-order aberration of soft X-ray optical systems with orthogonal and coplanar arrangement of the main planes of elements

  • Pages: 1477-1484
  • First Published: 14 September 2020
Third-order aberration of soft X-ray optical systems with orthogonal and coplanar arrangement of the main planes of elements

Soft X-ray optical systems are widely used in synchrotron radiation, X-ray microscopes, etc. Here, a third-order aberration analytical analysis method for soft X-ray optical systems with orthogonal and coplanar arrangement of the main planes of elements is proposed. It will provide an analytical measure in design and optimization of this kind of optical system.

Phase analysis for partially coherent light propagating through an optimized aperture in a synchrotron beamline

  • Pages: 1485-1493
  • First Published: 14 September 2020
Phase analysis for partially coherent light propagating through an optimized aperture in a synchrotron beamline

The phase distribution, intensity and spot size at the focal plane of partially coherent light are analyzed by optimizing the size and position of an aperture.

Practical design and performance of a new merged APPLE-Knot undulator

  • Pages: 1494-1498
  • First Published: 09 October 2020
Practical design and performance of a new merged APPLE-Knot undulator

A new design of a magnet-merged APPLE-Knot undulator with low on-axis heat load and high polarization is presented.

On obtaining high spectral resolution in extreme ultraviolet/soft X-ray monochromators operating off-plane diffraction in a divergent incident beam

  • Pages: 1499-1509
  • First Published: 14 October 2020
On obtaining high spectral resolution in extreme ultraviolet/soft X-ray monochromators operating off-plane diffraction in a divergent incident beam

Severe aberrations arise in off-plane diffraction from a plane grating with constant groove density when the incident beam is uncollimated. It is shown that they can be eliminated downstream of the grating by the use of astigmatic focusing.

Investigation of the damping wiggler effect and application on the PAL fourth-generation storage ring

  • Pages: 1510-1517
  • First Published: 22 October 2020
Investigation of the damping wiggler effect and application on the PAL fourth-generation storage ring

An investigation of the damping wiggler effect to reduce the emittance in the Pohang Accelerator Laboratory (PAL), a fourth-generation storage ring (4GSR) that uses a multi-bend achromat, is presented.

Open Access

Correction of the X-ray wavefront from compound refractive lenses using 3D printed refractive structures

  • Pages: 1518-1527
  • First Published: 19 October 2020
Correction of the X-ray wavefront from compound refractive lenses using 3D printed refractive structures

The knife-edge imaging-based wavefront-sensing technique is used for wavefront error characterization of Be X-ray lenses with and without corrector plate. Different 3D printed corrector plates are proposed to achieve pseudo-perfect compensation of wavefront errors of Be X-ray lenses.

Open Access

Focusing a round coherent beam by spatial filtering the horizontal source

  • Pages: 1528-1538
  • First Published: 20 October 2020
Focusing a round coherent beam by spatial filtering the horizontal source

The use of spatial filtering with a horizontal slit near the source to enlarge the horizontal coherence in an experimental station and produce a diffraction-limited round focus at an insertion device beamline for X-ray photon correlation spectroscopy experiments is illustrated. This scheme has now been in use since 2019 for the 8-ID beamline at the Advanced Photon Source, sharing the undulator beam with two separate beamlines, 8-ID-E and 8-ID-I at 7.35 keV, with increased partially coherent flux, reduced horizontal spot sizes on samples, and good speckle contrast.

Open Access

Fast convolution-based performance estimation method for diffraction-limited source with imperfect X-ray optics

  • Pages: 1539-1552
  • First Published: 26 October 2020
Fast convolution-based performance estimation method for diffraction-limited source with imperfect X-ray optics

A theoretical approach is proposed to describe the performance degradation caused by imperfect X-ray optical elements.

Open Access

Small Bragg-plane slope errors revealed in synthetic diamond crystals

  • Pages: 1553-1563
  • First Published: 26 October 2020
Small Bragg-plane slope errors revealed in synthetic diamond crystals

X-ray rocking curve imaging is used to study the smallest achievable Bragg-plane slope errors in the best presently available synthetic diamond crystals and how they compare with those of perfect silicon crystals

Recent advances in the development of high-resolution 3D cadmium–zinc–telluride drift strip detectors

  • Pages: 1564-1576
  • First Published: 25 September 2020
Recent advances in the development of high-resolution 3D cadmium–zinc–telluride drift strip detectors

New high-resolution cadmium–zinc–telluride drift strip detectors have been developed with excellent room-temperature energy resolution of 0.8% FWHM at 662 keV.

Backside-illuminated scientific CMOS detector for soft X-ray resonant scattering and ptychography

  • Pages: 1577-1589
  • First Published: 26 October 2020
Backside-illuminated scientific CMOS detector for soft X-ray resonant scattering and ptychography

This paper reports measurement results and an experimental demonstration of a new backside-illuminated scientific CMOS sensor for soft X-ray experiments at the SOLEIL synchrotron.

Nanoparticle dose enhancement of synchrotron radiation in PRESAGE dosimeters

  • Pages: 1590-1600
  • First Published: 26 October 2020
Nanoparticle dose enhancement of synchrotron radiation in PRESAGE dosimeters

The physical absorbed dose enhancement due to the presence of gold and bismuth nanoparticles by synchrotron X-ray beams was measured in PRESAGE dosimeters.

Absolute intensity calibration for carbon-edge soft X-ray scattering

  • Pages: 1601-1608
  • First Published: 16 September 2020
Absolute intensity calibration for carbon-edge soft X-ray scattering

A facile method for calibrating the absolute scattering intensity at the carbon K absorption edge, taking advantage of X-ray fluorescence produced at that edge, is presented. The method is verified by measuring the Flory–Huggins interaction parameter between two segments of a block copolymer melt.

Counting-loss correction method based on dual-exponential impulse shaping

  • Pages: 1609-1613
  • First Published: 25 September 2020
Counting-loss correction method based on dual-exponential impulse shaping

A new dual-exponential impulse shaping method is proposed, and its deployment in hardware to test its performance is shown.

Improving the soft X-ray reflectivity of Cr/Ti multilayers by co-deposition of B4C

  • Pages: 1614-1617
  • First Published: 09 October 2020
Improving the soft X-ray reflectivity of Cr/Ti multilayers by co-deposition of B4C

Systematic analysis on interfaces of Cr/Ti multilayers has been performed. The near-normal-incidence reflectivity increases from 4.48% to 15.75% at a wavelength of 2.73 nm using co-deposition of B4C.

Bent crystal Laue analyser combined with total reflection fluorescence X-ray absorption fine structure (BCLA + TRF-XAFS) and its application to surface studies

  • Pages: 1618-1625
  • First Published: 16 October 2020
Bent crystal Laue analyser combined with total reflection fluorescence X-ray absorption fine structure (BCLA + TRF-XAFS) and its application to surface studies

A bent crystal Laue analyser combined with total reflection fluorescence X-ray absorption fine structure is a promising technique for in situ surface analysis of highly dispersed systems even in the presence of solution.

Extracting contrast in an X-ray speckle visibility spectroscopy experiment under imperfect conditions

  • Pages: 1626-1632
  • First Published: 19 October 2020
Extracting contrast in an X-ray speckle visibility spectroscopy experiment under imperfect conditions

Contrast can be recovered by selectively binning the detector in a double-pulse X-ray speckle visibility spectroscopy experiment where an angular misalignment and imperfect overlap would otherwise destroy the contrast.

Influence of spin orbit splitting and satellite transitions on nickel soft X-ray optical properties near its L2,3 absorption edge region

  • Pages: 1633-1639
  • First Published: 20 October 2020
Influence of spin orbit splitting and satellite transitions on nickel soft X-ray optical properties near its L2,3 absorption edge region

Experimentally obtained optical constants of the nickel near L-edge energy region show signatures of different excitations which are absent in the available databases. These excitations are explained using charge transfer effects and core-hole interactions in valence and core excited states.

Local structure change of luminescent Ag zeolite-A and -X studied by in situ XAFS and IR spectroscopy

  • Pages: 1640-1647
  • First Published: 21 October 2020
Local structure change of luminescent Ag zeolite-A and -X studied by in situ XAFS and IR spectroscopy

Local structure changes of luminescent Ag zeolite-A and -X are analysed by in situ XAFS. The relation between the behaviour of the Ag cluster in the cavity of zeolite and the intensity of the photoluminescence is given.

Theoretical spectral analysis of FEL radiation from multi-harmonic undulators

  • Pages: 1648-1661
  • First Published: 22 October 2020
Theoretical spectral analysis of FEL radiation from multi-harmonic undulators

A comparative theoretical analysis of the free-electron laser (FEL) radiation in main FEL experiments is given. It is shown that an elliptic undulator with field harmonics and electron–photon phase-shifting yields significantly higher harmonic power than that from a planar undulator with phase-shifting.

Time and space resolved modelling of the heating induced by synchrotron X-ray nanobeams

  • Pages: 1662-1673
  • First Published: 16 September 2020
Time and space resolved modelling of the heating induced by synchrotron X-ray nanobeams

The heating effects of hard X-rays from synchrotron sources are simulated by coupling the Monte Carlo method with the Fourier heat equation. The temperature behaviours simulated are found to be critically dependent on the filling mode of the electron storage ring and on the distribution of the energy density absorbed by the material.

Geometric determination of direction of dislocations using synchrotron X-ray transmission topography

  • Pages: 1674-1680
  • First Published: 28 September 2020
Geometric determination of direction of dislocations using synchrotron X-ray transmission topography

A geometric method for resolving dislocation directions in synchrotron X-ray topography is described.

Open Access

Mjölnir: a miniature triaxial rock deformation apparatus for 4D synchrotron X-ray microtomography

  • Pages: 1681-1687
  • First Published: 16 October 2020
Mjölnir: a miniature triaxial rock deformation apparatus for 4D synchrotron X-ray microtomography

The design, construction and assembly details for an X-ray transparent triaxial deformation cell for 4D investigations of rock deformation and coupled chemical–mechanical processes in the geosciences are presented. The portability and flexibility of the cell are demonstrated by deployment on four different synchrotron beamlines.

Open Access

Hard X-ray ptychography for optics characterization using a partially coherent synchrotron source

  • Pages: 1688-1695
  • First Published: 16 October 2020
Hard X-ray ptychography for optics characterization using a partially coherent synchrotron source

Ptychography has been developed and routinely employed as an at-wavelength metrology method on a low coherence dipole magnet beamline.

Zernike phase-contrast full-field transmission X-ray nanotomography for 400 micrometre-sized samples

  • Pages: 1696-1702
  • First Published: 21 October 2020
Zernike phase-contrast full-field transmission X-ray nanotomography for 400 micrometre-sized samples

A method for sub-millimetre field-of-view full-field X-ray tomography at a resolution of hundreds of nanometres is presented.

Open Access

A coded aperture microscope for X-ray fluorescence full-field imaging

  • Pages: 1703-1706
  • First Published: 21 October 2020
A coded aperture microscope for X-ray fluorescence full-field imaging

First results from a 10 µm MURA coded aperture optic for a full-field X-ray fluorescence microscope are presented.

Open Access

3D virtual histology of human pancreatic tissue by multiscale phase-contrast X-ray tomography

  • Pages: 1707-1719
  • First Published: 26 October 2020
3D virtual histology of human pancreatic tissue by multiscale phase-contrast X-ray tomography

This paper presents propagation-based phase-contrast tomography in two configurations at the beamline endstation GINIX, demonstrated on the application of 1 mm human pancreatic tumor tissue biopsies.

short communications

Two-color X-ray free-electron laser consisting of broadband and narrowband beams

  • Pages: 1720-1724
  • First Published: 14 October 2020
Two-color X-ray free-electron laser consisting of broadband and narrowband beams

A new scheme is proposed and demonstrated to generate a two-color X-ray free-electron laser consisting of broadband and narrowband beams.

Dynamic pulse-to-pulse thermal load effects in pulse-train-mode self-seeded X-ray free-electron laser

  • Pages: 1725-1729
  • First Published: 20 October 2020
Dynamic pulse-to-pulse thermal load effects in pulse-train-mode self-seeded X-ray free-electron laser

Thermal load in pulse train mode can be a haunting factor that undermines the brightness and coherence of self-seeded X-ray free-electron lasers. The pulse-to-pulse thermal load effects on the seed quality and some instructive information for the tuning process are studied and presented.

Open Access

Implementation of a crossed-slit system for fast alignment of sealed polycapillary X-ray optics

  • Pages: 1730-1733
  • First Published: 26 October 2020
Implementation of a crossed-slit system for fast alignment of sealed polycapillary X-ray optics

A fast X-ray focusing polycapillary alignment method was implemented and tested using a compact short-pulse laser-driven broadband X-ray source.

computer programs

Open Access

X-ray Spectral Imaging Program: XSIP

  • Pages: 1734-1740
  • First Published: 14 September 2020
X-ray Spectral Imaging Program: XSIP

An open source Python software package, developed for data analysis for spectral K-edge subtraction imaging and wide-field energy-dispersive X-ray absorption spectroscopy imaging, is reported.

THORONDOR: a software for fast treatment and analysis of low-energy XAS data

  • Pages: 1741-1752
  • First Published: 28 September 2020
THORONDOR: a software for fast treatment and analysis of low-energy XAS data

THORONDOR is a Python software realized for the analysis of multiple NEXAFS spectra collected in situ. It allows the correction and normalization of the acquired spectra through a fast and intuitive interface. Moreover, it offers a sophisticated toolbox for the fitting of the NEXAFS rising-edge peaks.

obituaries

Antonio Ricardo D. Rodrigues (1951–2020)

  • Pages: 1753-1754
  • First Published: 05 November 2020
Antonio Ricardo D. Rodrigues (1951–2020)

Obituary for Antonio Ricardo D. Rodrigues