A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell
Corresponding Author
Rachel J. Husband
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Rachel J. Husband, e-mail: [email protected]; Hanns-Peter Liermann, e-mail: [email protected]Search for more papers by this authorCornelius Strohm
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorKaren Appel
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorOrianna B. Ball
The University of Edinburgh, SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, Peter Guthrie Tait Road, Edinburgh, EH9 3FD United Kingdom
Search for more papers by this authorRichard Briggs
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorJohannes Buchen
University of Oxford, Department of Earth Sciences, South Parks Road, Oxford, OX1 3AN United Kingdom
Search for more papers by this authorValerio Cerantola
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorStella Chariton
The University of Chicago, Consortium for Advanced Radiation Sources, 5640 South Ellis Avenue, Chicago, IL, 60637 USA
Search for more papers by this authorAmy L. Coleman
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorHyunchae Cynn
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorDana Dattelbaum
Los Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM, 87545 USA
Search for more papers by this authorAnand Dwivedi
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorJon H. Eggert
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorLars Ehm
Department of Geosciences, 255 Earth and Space Sciences Building (ESS), Stony Brook, NY, 11794-2100 USA
Search for more papers by this authorWilliam J. Evans
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorKonstantin Glazyrin
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorAlexander F. Goncharov
Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road, NW, Washington, DC, 20015 USA
Search for more papers by this authorHeinz Graafsma
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorAlex Howard
Washington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA, 99164 USA
Search for more papers by this authorLarissa Huston
Los Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM, 87545 USA
Search for more papers by this authorTrevor M. Hutchinson
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorHuijeong Hwang
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorSony Jacob
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorJohannes Kaa
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Technische Universität Dortmund, Maria-Goeppert-Mayer-Straße 2, Dortmund, 44227 Germany
Search for more papers by this authorJaeyong Kim
Hanyang University, Department of Physics, 17 Haengdang Dong, Seongdong gu Seoul, 133-791 Republic of Korea
Search for more papers by this authorMinseob Kim
Washington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA, 99164 USA
Search for more papers by this authorEgor Koemets
University of Oxford, Department of Earth Sciences, South Parks Road, Oxford, OX1 3AN United Kingdom
Search for more papers by this authorZuzana Konôpková
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorFalko Langenhorst
Friedrich-Schiller-Universität Jena, Institut für Geowissenschaften, Carl-Zeiss-Promenade 10, Jena, 07745 Germany
Search for more papers by this authorTorsten Laurus
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorXinyang Li
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorJona Mainberger
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorHauke Marquardt
University of Oxford, Department of Earth Sciences, South Parks Road, Oxford, OX1 3AN United Kingdom
Search for more papers by this authorEmma E. McBride
SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, CA, 94025 USA
Search for more papers by this authorChristopher McGuire
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorJames D. McHardy
The University of Edinburgh, SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, Peter Guthrie Tait Road, Edinburgh, EH9 3FD United Kingdom
Search for more papers by this authorMalcolm I. McMahon
The University of Edinburgh, SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, Peter Guthrie Tait Road, Edinburgh, EH9 3FD United Kingdom
Search for more papers by this authorR. Stewart McWilliams
The University of Edinburgh, SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, Peter Guthrie Tait Road, Edinburgh, EH9 3FD United Kingdom
Search for more papers by this authorAlba S. J. Méndez
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorAnshuman Mondal
Universität Münster, Institut für Mineralogie, Corrensstraße 24, Münster, 48149 Germany
Search for more papers by this authorGuillaume Morard
Univ. Grenoble Alpes, Univ. Savoie Mont Blanc, CNRS, IRD, Univ. Gustave Eiffel, ISTerre, Grenoble, 38000 France
Search for more papers by this authorEarl F. O'Bannon
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorChristoph Otzen
Friedrich-Schiller-Universität Jena, Institut für Geowissenschaften, Carl-Zeiss-Promenade 10, Jena, 07745 Germany
Search for more papers by this authorCharles M. Pépin
CEA, DAM, DIF, Arpajon Cedex, 91297 France
Université Paris-Saclay, CEA, Laboratoire Matière en Conditions Extrêmes, Bruyères-le-Châtel, 91680 France
Search for more papers by this authorVitali B. Prakapenka
The University of Chicago, Consortium for Advanced Radiation Sources, 5640 South Ellis Avenue, Chicago, IL, 60637 USA
Search for more papers by this authorClemens Prescher
Albert-Ludwigs University of Freiburg, Institute of Earth and Environmental Sciences, Hermann-Herder-Str. 5, Freiburg, D-79104 Germany
Search for more papers by this authorThomas R. Preston
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorRonald Redmer
Universität Rostock, Institut für Physik, Albert-Einstein-Straße 23–24, Rostock, 18059 Germany
Search for more papers by this authorMichael Roeper
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorCarmen Sanchez-Valle
Universität Münster, Institut für Mineralogie, Corrensstraße 24, Münster, 48149 Germany
Search for more papers by this authorDean Smith
Argonne National Laboratory, High Pressure Collaborative Access Team (HPCAT), X-ray Science Division (XSD), 9700 S. Cass Avenue, Lemont, IL, 60439 USA
Search for more papers by this authorRaymond F. Smith
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorDaniel Sneed
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorSergio Speziale
Deutsches GeoForschungsZentrum GFZ, Telegrafenberg, Potsdam, 14473 Germany
Search for more papers by this authorTobias Spitzbart
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorStephan Stern
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorBlake T. Sturtevant
Los Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM, 87545 USA
Search for more papers by this authorJolanta Sztuk-Dambietz
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorPeter Talkovski
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorNenad Velisavljevic
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorCara Vennari
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorZhongyan Wu
Hanyang University, Department of Physics, 17 Haengdang Dong, Seongdong gu Seoul, 133-791 Republic of Korea
Search for more papers by this authorChoong-Shik Yoo
Washington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA, 99164 USA
Search for more papers by this authorUlf Zastrau
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorZsolt Jenei
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorCorresponding Author
Hanns-Peter Liermann
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Rachel J. Husband, e-mail: [email protected]; Hanns-Peter Liermann, e-mail: [email protected]Search for more papers by this authorCorresponding Author
Rachel J. Husband
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Rachel J. Husband, e-mail: [email protected]; Hanns-Peter Liermann, e-mail: [email protected]Search for more papers by this authorCornelius Strohm
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorKaren Appel
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorOrianna B. Ball
The University of Edinburgh, SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, Peter Guthrie Tait Road, Edinburgh, EH9 3FD United Kingdom
Search for more papers by this authorRichard Briggs
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorJohannes Buchen
University of Oxford, Department of Earth Sciences, South Parks Road, Oxford, OX1 3AN United Kingdom
Search for more papers by this authorValerio Cerantola
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorStella Chariton
The University of Chicago, Consortium for Advanced Radiation Sources, 5640 South Ellis Avenue, Chicago, IL, 60637 USA
Search for more papers by this authorAmy L. Coleman
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorHyunchae Cynn
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorDana Dattelbaum
Los Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM, 87545 USA
Search for more papers by this authorAnand Dwivedi
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorJon H. Eggert
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorLars Ehm
Department of Geosciences, 255 Earth and Space Sciences Building (ESS), Stony Brook, NY, 11794-2100 USA
Search for more papers by this authorWilliam J. Evans
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorKonstantin Glazyrin
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorAlexander F. Goncharov
Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road, NW, Washington, DC, 20015 USA
Search for more papers by this authorHeinz Graafsma
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorAlex Howard
Washington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA, 99164 USA
Search for more papers by this authorLarissa Huston
Los Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM, 87545 USA
Search for more papers by this authorTrevor M. Hutchinson
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorHuijeong Hwang
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorSony Jacob
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorJohannes Kaa
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Technische Universität Dortmund, Maria-Goeppert-Mayer-Straße 2, Dortmund, 44227 Germany
Search for more papers by this authorJaeyong Kim
Hanyang University, Department of Physics, 17 Haengdang Dong, Seongdong gu Seoul, 133-791 Republic of Korea
Search for more papers by this authorMinseob Kim
Washington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA, 99164 USA
Search for more papers by this authorEgor Koemets
University of Oxford, Department of Earth Sciences, South Parks Road, Oxford, OX1 3AN United Kingdom
Search for more papers by this authorZuzana Konôpková
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorFalko Langenhorst
Friedrich-Schiller-Universität Jena, Institut für Geowissenschaften, Carl-Zeiss-Promenade 10, Jena, 07745 Germany
Search for more papers by this authorTorsten Laurus
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorXinyang Li
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorJona Mainberger
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorHauke Marquardt
University of Oxford, Department of Earth Sciences, South Parks Road, Oxford, OX1 3AN United Kingdom
Search for more papers by this authorEmma E. McBride
SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, CA, 94025 USA
Search for more papers by this authorChristopher McGuire
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorJames D. McHardy
The University of Edinburgh, SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, Peter Guthrie Tait Road, Edinburgh, EH9 3FD United Kingdom
Search for more papers by this authorMalcolm I. McMahon
The University of Edinburgh, SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, Peter Guthrie Tait Road, Edinburgh, EH9 3FD United Kingdom
Search for more papers by this authorR. Stewart McWilliams
The University of Edinburgh, SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, Peter Guthrie Tait Road, Edinburgh, EH9 3FD United Kingdom
Search for more papers by this authorAlba S. J. Méndez
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorAnshuman Mondal
Universität Münster, Institut für Mineralogie, Corrensstraße 24, Münster, 48149 Germany
Search for more papers by this authorGuillaume Morard
Univ. Grenoble Alpes, Univ. Savoie Mont Blanc, CNRS, IRD, Univ. Gustave Eiffel, ISTerre, Grenoble, 38000 France
Search for more papers by this authorEarl F. O'Bannon
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorChristoph Otzen
Friedrich-Schiller-Universität Jena, Institut für Geowissenschaften, Carl-Zeiss-Promenade 10, Jena, 07745 Germany
Search for more papers by this authorCharles M. Pépin
CEA, DAM, DIF, Arpajon Cedex, 91297 France
Université Paris-Saclay, CEA, Laboratoire Matière en Conditions Extrêmes, Bruyères-le-Châtel, 91680 France
Search for more papers by this authorVitali B. Prakapenka
The University of Chicago, Consortium for Advanced Radiation Sources, 5640 South Ellis Avenue, Chicago, IL, 60637 USA
Search for more papers by this authorClemens Prescher
Albert-Ludwigs University of Freiburg, Institute of Earth and Environmental Sciences, Hermann-Herder-Str. 5, Freiburg, D-79104 Germany
Search for more papers by this authorThomas R. Preston
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorRonald Redmer
Universität Rostock, Institut für Physik, Albert-Einstein-Straße 23–24, Rostock, 18059 Germany
Search for more papers by this authorMichael Roeper
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorCarmen Sanchez-Valle
Universität Münster, Institut für Mineralogie, Corrensstraße 24, Münster, 48149 Germany
Search for more papers by this authorDean Smith
Argonne National Laboratory, High Pressure Collaborative Access Team (HPCAT), X-ray Science Division (XSD), 9700 S. Cass Avenue, Lemont, IL, 60439 USA
Search for more papers by this authorRaymond F. Smith
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorDaniel Sneed
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorSergio Speziale
Deutsches GeoForschungsZentrum GFZ, Telegrafenberg, Potsdam, 14473 Germany
Search for more papers by this authorTobias Spitzbart
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorStephan Stern
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorBlake T. Sturtevant
Los Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM, 87545 USA
Search for more papers by this authorJolanta Sztuk-Dambietz
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorPeter Talkovski
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Search for more papers by this authorNenad Velisavljevic
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorCara Vennari
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorZhongyan Wu
Hanyang University, Department of Physics, 17 Haengdang Dong, Seongdong gu Seoul, 133-791 Republic of Korea
Search for more papers by this authorChoong-Shik Yoo
Washington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA, 99164 USA
Search for more papers by this authorUlf Zastrau
European XFEL, Holzkoppel 4, Schenefeld, 22869 Germany
Search for more papers by this authorZsolt Jenei
Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA, 94550 USA
Search for more papers by this authorCorresponding Author
Hanns-Peter Liermann
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
Rachel J. Husband, e-mail: [email protected]; Hanns-Peter Liermann, e-mail: [email protected]Search for more papers by this authorAbstract
An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s−1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s−1 was observed during the fast compression of Au, while a strain rate of ∼1100 s−1 was achieved during the rapid compression of N2 at 23 TPa s−1.
