Journal of Polymer Science Part B: Polymer Physics

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Phase transitions of the rapid-compression-induced mesomorphic isotactic polypropylene under high-pressure annealing

Xiaobo Fu

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Wenxia Jia,

Wenxia Jia

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Xiaoting Li,

Xiaoting Li

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Yaming Wang,

Yaming Wang

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Zhen Wang,

Zhen Wang

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Chuntai Liu,

Chuntai Liu

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Changyu Shen,

Changyu Shen

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Chunguang Shao,

Corresponding Author

Chunguang Shao

[email protected]

orcid.org/0000-0003-2316-4262

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

Correspondence to: C. Shao (E-mail: [email protected])Search for more papers by this author

Xiaobo Fu,

Xiaobo Fu

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Wenxia Jia,

Wenxia Jia

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Xiaoting Li,

Xiaoting Li

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Yaming Wang,

Yaming Wang

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Zhen Wang,

Zhen Wang

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Chuntai Liu,

Chuntai Liu

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Changyu Shen,

Changyu Shen

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

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Chunguang Shao,

Corresponding Author

Chunguang Shao

[email protected]

orcid.org/0000-0003-2316-4262

National Engineering Research Center for Advanced Polymer Processing Technology, School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450002, China

Correspondence to: C. Shao (E-mail: [email protected])Search for more papers by this author

First published: 23 March 2019

https://doi.org/10.1002/polb.24820

Citations: 13

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ABSTRACT

The mesomorphic isotactic polypropylene was prepared by rapid compression instead of the common method of temperature quenching, and their phase transition under high pressure was investigated in depth by combining wide-angle X-ray diffraction, small-angle X-ray scattering, and differential scanning calorimetry techniques. It was found that annealing under pressure can promote the further arrangement of chain segments of the mesophase toward the crossed state in the orthorhombic γ-phase, and the long period of the mesophase slightly decreased from 8.2 to 7.2 nm. The kinetics of this meso-γ transition strongly depends on pressure. As annealing pressure increased, the mobility of molecular segments was reduced, and then the onset and finishing time of phase transition were both delayed significantly. A critical annealing pressure was found between 1.6 and 1.75 GPa, which determines whether the phase transition occurs or not. When pressure reaches 1.75 GPa, mesophase did not transform at all within 120 min. Based on the results, a reasonable mechanism was proposed to show the crystallization process of mesophase under high-pressure annealing. © 2019 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2019, 57, 651–661

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Volume57, Issue11

June 1, 2019

Pages 651-661

Phase transitions of the rapid-compression-induced mesomorphic isotactic polypropylene under high-pressure annealing

ABSTRACT

Supporting Information

REFERENCES AND NOTES

Citing Literature

References

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Phase transitions of the rapid-compression-induced mesomorphic isotactic polypropylene under high-pressure annealing

ABSTRACT

Supporting Information

REFERENCES AND NOTES

Citing Literature

References

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