Volume 139, Issue 16 51965

ARTICLE

Optimization of interface microstructure of high-strength-high-modulus polyimide fibers composites utilizing waterborne polyamide and hybrid sizing agent

Li Zhu,

Li Zhu

State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, China

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Yinong Li,

Yinong Li

State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, China

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Mengying Zhang,

Mengying Zhang

Research and Development Department, Jiangsu Shino New Materials Technology Co., Ltd, Changzhou, China

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Dezhen Wu,

Dezhen Wu

State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, China

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Hongqing Niu,

Corresponding Author

Hongqing Niu

[email protected]

orcid.org/0000-0001-8805-035X

State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, China

Correspondence

Hongqing Niu, State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029, China.

Email: [email protected]

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Li Zhu,

Li Zhu

State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, China

Search for more papers by this author

Yinong Li,

Yinong Li

State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, China

Search for more papers by this author

Mengying Zhang,

Mengying Zhang

Research and Development Department, Jiangsu Shino New Materials Technology Co., Ltd, Changzhou, China

Search for more papers by this author

Dezhen Wu,

Dezhen Wu

State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, China

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Hongqing Niu,

Corresponding Author

Hongqing Niu

[email protected]

orcid.org/0000-0001-8805-035X

State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, China

Correspondence

Hongqing Niu, State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029, China.

Email: [email protected]

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First published: 27 November 2021

https://doi.org/10.1002/app.51965

Citations: 3

Funding information: Fundamental Research Funds for the Central Universities, Grant/Award Number: XK1802-2; The Aeronautical Science Foundation of China, Grant/Award Number: 201718S9001; The National Key Research and Development Program of China, Grant/Award Number: 2017YFB0307600; Innovative Research Group Project of the National Natural Science Foundation of China, Grant/Award Number: Grant 51790501

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Abstract

The weak interface adhesion between high-strength-high-modulus polyimide (PI) fibers and epoxy (EP) resin matrix has seriously hampered the application of PI/EP composites. Herein, a waterborne polyamide (WPA) sizing agent was used to modify PI fibers to enhance the interface adhesion strength between the PI fibers and EP resin matrix. The surface characteristics of PI fibers were investigated to determine chemical composition, morphology, roughness, wettability, interfacial shear strength (IFSS) and interlinear shear strength. The results indicated that the WPA sizing agent significantly enhanced the interface adhesion properties between the PI fibers and EP resin matrix with a 132% and 22.35% increment obtained for IFSS and interlaminar shear strength (ILSS) compared with unsized PI/EP composites. Then, the hybrid sizing agent generated by WPA and waterborne EP sizing agent exhibited the highest interface adhesion with 168.65% and 28.62% increment obtained for IFSS and ILSS compared with unsized PI/EP composites. Based on these results, a sizing mechanism with chemical interaction and mechanical interlocking was proposed, which provides an effective and feasible method to enhance the interface adhesion between the PI fibers and EP resin matrix.

CONFLICT OF INTEREST

The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Open Research

DATA AVAILABILITY STATEMENT

No. Research data are not shared.

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Volume139, Issue16

April 20, 2022

51965

Optimization of interface microstructure of high-strength-high-modulus polyimide fibers composites utilizing waterborne polyamide and hybrid sizing agent

Abstract

CONFLICT OF INTEREST

Open Research

DATA AVAILABILITY STATEMENT

REFERENCES

Citing Literature

References

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Optimization of interface microstructure of high-strength-high-modulus polyimide fibers composites utilizing waterborne polyamide and hybrid sizing agent

Abstract

CONFLICT OF INTEREST

Open Research

DATA AVAILABILITY STATEMENT

REFERENCES

Citing Literature

References

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