Research Article

Synthesis of High-Performance Pebax®-1074/DD3R Mixed-Matrix Membranes for CO₂/CH₄ Separation

Farahnaz Karamouz

Sahand University of Technology, Faculty of Chemical Engineering, Sahand University Road, P.O. Box 51335/1996, Tabriz, Iran

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Hafez Maghsoudi,

Corresponding Author

Hafez Maghsoudi

[email protected]

Sahand University of Technology, Faculty of Chemical Engineering, Sahand University Road, P.O. Box 51335/1996, Tabriz, Iran

Sahand University of Technology, Nanostructured Materials Research Center, Sahand University Road, P.O. Box 51335/1996, Tabriz, Iran

Correspondence: Hafez Maghsoudi ([email protected]), Faculty of Chemical Engineering, Sahand University of Technology, Sahand University Road, P.O. Box 51335/1996, Tabriz, Iran.Search for more papers by this author

Reza Yegani,

Reza Yegani

Sahand University of Technology, Faculty of Chemical Engineering, Sahand University Road, P.O. Box 51335/1996, Tabriz, Iran

Sahand University of Technology, Membrane Technology Research Center, Sahand University Road, P.O. Box 51335/1996, Tabriz, Iran

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Farahnaz Karamouz,

Farahnaz Karamouz

Sahand University of Technology, Faculty of Chemical Engineering, Sahand University Road, P.O. Box 51335/1996, Tabriz, Iran

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Hafez Maghsoudi,

Corresponding Author

Hafez Maghsoudi

[email protected]

Sahand University of Technology, Faculty of Chemical Engineering, Sahand University Road, P.O. Box 51335/1996, Tabriz, Iran

Sahand University of Technology, Nanostructured Materials Research Center, Sahand University Road, P.O. Box 51335/1996, Tabriz, Iran

Reza Yegani,

Reza Yegani

Sahand University of Technology, Faculty of Chemical Engineering, Sahand University Road, P.O. Box 51335/1996, Tabriz, Iran

Sahand University of Technology, Membrane Technology Research Center, Sahand University Road, P.O. Box 51335/1996, Tabriz, Iran

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First published: 27 June 2018

https://doi.org/10.1002/ceat.201800087

Citations: 17

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Abstract

This work deals with the incorporation of deca-dodecasil 3 rhombohedral (DD3R) zeolite as an inorganic filler into the Pebax®-1074-based polymer matrix to enhance the performance of the pure polymeric membrane in CO₂/CH₄ separation. The membranes were fabricated with different concentrations of DD3R. Separation performances of the membranes were investigated at various feed pressures and temperatures. Scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), and differential scanning calorimetry (DSC) analysis of the prepared membranes were performed. In the best case, selectivity for CO₂/CH₄ separation was improved, while the permeability decreased. Membranes with 1 and 5 wt % DD3R were located in the acceptable region beyond the Robeson plot (1991) for CO₂/CH₄ gas pairs.

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Volume41, Issue9

September 2018

Pages 1767-1775

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Synthesis of High-Performance Pebax®-1074/DD3R Mixed-Matrix Membranes for CO₂/CH₄ Separation

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Synthesis of High-Performance Pebax®-1074/DD3R Mixed-Matrix Membranes for CO2/CH4 Separation

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Synthesis of High-Performance Pebax®-1074/DD3R Mixed-Matrix Membranes for CO₂/CH₄ Separation