Layered Cobalt Hydroxide Nanocones: Microwave-Assisted Synthesis, Exfoliation, and Structural Modification†
Dr. Xiaohe Liu
International Center for Materials Nanoarchitectonics, National Institute for Materials Science, 1-1 Namiki, Tsukuba, Ibaraki 305-0044 (Japan), Fax: (+81) 29-854-9061
Permanent address: Department of Inorganic Materials, Central South University, Changsha, Hunan 410083 (China)
Search for more papers by this authorDr. Renzhi Ma
International Center for Materials Nanoarchitectonics, National Institute for Materials Science, 1-1 Namiki, Tsukuba, Ibaraki 305-0044 (Japan), Fax: (+81) 29-854-9061
Search for more papers by this authorProf. Yoshio Bando
International Center for Materials Nanoarchitectonics, National Institute for Materials Science, 1-1 Namiki, Tsukuba, Ibaraki 305-0044 (Japan), Fax: (+81) 29-854-9061
Search for more papers by this authorProf. Takayoshi Sasaki
International Center for Materials Nanoarchitectonics, National Institute for Materials Science, 1-1 Namiki, Tsukuba, Ibaraki 305-0044 (Japan), Fax: (+81) 29-854-9061
Search for more papers by this authorDr. Xiaohe Liu
International Center for Materials Nanoarchitectonics, National Institute for Materials Science, 1-1 Namiki, Tsukuba, Ibaraki 305-0044 (Japan), Fax: (+81) 29-854-9061
Permanent address: Department of Inorganic Materials, Central South University, Changsha, Hunan 410083 (China)
Search for more papers by this authorDr. Renzhi Ma
International Center for Materials Nanoarchitectonics, National Institute for Materials Science, 1-1 Namiki, Tsukuba, Ibaraki 305-0044 (Japan), Fax: (+81) 29-854-9061
Search for more papers by this authorProf. Yoshio Bando
International Center for Materials Nanoarchitectonics, National Institute for Materials Science, 1-1 Namiki, Tsukuba, Ibaraki 305-0044 (Japan), Fax: (+81) 29-854-9061
Search for more papers by this authorProf. Takayoshi Sasaki
International Center for Materials Nanoarchitectonics, National Institute for Materials Science, 1-1 Namiki, Tsukuba, Ibaraki 305-0044 (Japan), Fax: (+81) 29-854-9061
Search for more papers by this authorThis work was supported by CREST of the Japan Science and Technology Agency (JST) and the World Premier International Center Initiative (WPI Initiative) on Materials Nanoarchitectonics, MEXT, Japan.
Graphical Abstract
Layered cobalt hydroxide nanocones intercalated with dodecyl sulfate (DS) ions (see scheme; OH− blue, Co green dots, DS ions red) could be synthesized by the microwave-assisted rolling of lamellar structures. The cones could be exfoliated into cobalt hydroxide nanosheets and converted into CoOOH and Co3O4 nanocones.
Supporting Information
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