• Issue

    Journal of Synchrotron Radiation: Volume 28, Issue 3

    669-1030
    May 2021

research papers

A coherent harmonic generation method for producing femtosecond coherent radiation in a laser plasma accelerator based light source

  • Pages: 669-680
  • First Published: 22 March 2021
A coherent harmonic generation method for producing femtosecond coherent radiation in a laser plasma accelerator based light source

A new seed laser-assisted microbunching generation method has been proposed. This method can be used to produce femtosecond coherent radiation in a laser-plasma accelerator-based light source.

Numerical study of the second harmonic generation in FELs

  • Pages: 681-687
  • First Published: 22 March 2021
Numerical study of the second harmonic generation in FELs

A numerical study of the effect of betatron oscillations on the second harmonic generation in free-electron lasers (FELs) is presented. A program for FEL simulation with new analytical expressions is developed; the modeling of harmonics in LCLS and PAL-XFEL experiments is performed.

Open Access

The FEL in the SXL project at MAX IV

  • Pages: 707-717
  • First Published: 02 May 2021
The FEL in the SXL project at MAX IV

The design of a soft X-ray free-electron laser for the SXL project at the MAX IV Laboratory is presented.

Open Access

Commissioning and operation status of the MAX IV 3 GeV storage ring vacuum system

  • Pages: 718-731
  • First Published: 02 May 2021
Commissioning and operation status of the MAX IV 3 GeV storage ring vacuum system

The 3 GeV electron storage ring of the MAX IV laboratory is the first light source storage ring that has the inner surface of nearly all the vacuum chambers coated with non-evaporable getter (NEG) thin film. The vacuum and the accelerator performance have proven successful.

Open Access

Staircase array of inclined refractive multi-lenses for large field of view pixel super-resolution scanning transmission hard X-ray microscopy

  • Pages: 732-740
  • First Published: 19 March 2021
Staircase array of inclined refractive multi-lenses for large field of view pixel super-resolution scanning transmission hard X-ray microscopy

A new X-ray focusing device generates hundreds of thousands of line foci, periodically spaced in the sub-micrometre range, with centimetre length. It enables to achieve large FOV pixel super-resolution scanning transmission hard X-ray microscopy.

High-accuracy computation of hard X-ray focusing and imaging for refractive optics

  • Pages: 741-755
  • First Published: 19 March 2021
High-accuracy computation of hard X-ray focusing and imaging for refractive optics

A mathematical apparatus for solving problems of X-ray wave propagation through complex optical systems, when the lens thickness can change with jumps, is developed and presented.

Temperature-gradient analyzers for non-resonant inelastic X-ray scattering

  • Pages: 756-768
  • First Published: 19 March 2021
Temperature-gradient analyzers for non-resonant inelastic X-ray scattering

Temperature-gradient analyzers for medium resolution, 25–32 meV, non-resonant inelastic X-ray scattering are fabricated and evaluated.

Open Access

Spatial-frequency features of radiation produced by a step-wise tapered undulator

  • Pages: 769-777
  • First Published: 26 March 2021
Spatial-frequency features of radiation produced by a step-wise tapered undulator

Spatial frequency radiation properties from a step-wise magnetic structure of an undulator are studied. This magnetic scheme is the most suitable for the superconducting undulators and provides the radiation properties that facilitate developing future beamlines dedicated to micro-probing.

Open Access

A microfluidic dosimetry cell to irradiate solutions with poorly penetrating radiations: a step towards online dosimetry for synchrotron beamlines

  • Pages: 778-789
  • First Published: 02 May 2021
A microfluidic dosimetry cell to irradiate solutions with poorly penetrating radiations: a step towards online dosimetry for synchrotron beamlines

The application of a microfluidic cell, specifically optimized for low penetrating soft X-ray radiation, as a dosimetry cell is reported. An analysis of the important parameters of the microfluidic cell, as well as their influences over dosimetry, is also reported. Measurements at 1.28 keV led to the determination of a hydroxyl production yield, G(HO.), of 0.025 ± 0.004 µmol J−1.

Open Access

Observation of microstructure evolution during inertia friction welding using in-situ synchrotron X-ray diffraction

  • Pages: 790-803
  • First Published: 19 March 2021
Observation of microstructure evolution during inertia friction welding using in-situ synchrotron X-ray diffraction

The first reported in-situ synchrotron X-ray diffraction experiments for the inertia friction welding process are presented. The evolution of the microstructure around the weld interface has been quantified throughout the process.

Practical measurement of the energy resolution for meV-resolved inelastic X-ray scattering

  • Pages: 804-811
  • First Published: 09 April 2021
Practical measurement of the energy resolution for meV-resolved inelastic X-ray scattering

Several different methods of measuring the energy resolution for meV-resolved inelastic X-ray scattering are investigated. Quantitative determination of inelastic contributions to the scattering from plexiglass and borosilicate glass enables an efficient, single scan, approach to resolution determination for a large (4 × 7) array of analyzers.

Open Access

Anomalous SAXS at P12 beamline EMBL Hamburg: instrumentation and applications

  • Pages: 812-823
  • First Published: 02 May 2021
Anomalous SAXS at P12 beamline EMBL Hamburg: instrumentation and applications

Hardware and software for anomalous small-angle X-ray scattering on biological macromolecules in solution implemented at the P12 beamline of the EMBL (PETRA III storage ring, DESY, Hamburg) are described.

Open Access

Extending synchrotron SAXS instrument ranges through addition of a portable, inexpensive USAXS module with vertical rotation axes

  • Pages: 824-833
  • First Published: 02 May 2021
Extending synchrotron SAXS instrument ranges through addition of a portable, inexpensive USAXS module with vertical rotation axes

This compact, Creative-Commons-licensed ultra-SAXS module, augments existing high-performance SAXS/WAXS synchrotron instruments, so that larger structures may be measured. Its functionality is demonstrated at the I22 beamline at Diamond Light Source, where the combined USAXS/SAXS/WAXS range of an alumina membrane, a porous carbon catalyst and silica, covers over four decades in scattering angle.

Calculating absorption dose when X-ray irradiation modifies material quantity and chemistry

  • Pages: 834-848
  • First Published: 22 March 2021
Calculating absorption dose when X-ray irradiation modifies material quantity and chemistry

A general method for calculating the dose absorbed in X-ray irradiation of a material when the irradiation changes the physical properties of the material is presented. The method considers cases where X-ray irradiation alters the chemical structure, the amount of material in the irradiated area, the linear absorption coefficient and the density of the material.

In situ X-ray absorption spectroscopic studies of photocatalytic oxidation of As(III) to less toxic As(V) by TiO2 nanotubes

  • Pages: 849-853
  • First Published: 13 April 2021
In situ X-ray absorption spectroscopic studies of photocatalytic oxidation of As(III) to less toxic As(V) by TiO2 nanotubes

The photocatalytic oxidation of As(III) to less toxic As(V) by TiO2 nanotubes studied using in situ synchrotron X-ray absorption spectroscopy is presented.

Generalized reverse projection method for grating-based phase tomography

  • Pages: 854-863
  • First Published: 19 March 2021
Generalized reverse projection method for grating-based phase tomography

A generalized reverse projection method has been established analytically for grating-based phase tomography with non-uniform reference. The method combines the advantages of the high efficiency of the reverse projection method and the universal applicability of the phase-stepping method.

A new imaging concept in spin polarimetry based on the spin-filter effect

  • Pages: 864-875
  • First Published: 30 March 2021
A new imaging concept in spin polarimetry based on the spin-filter effect

The concept of an imaging-type 3D spin detector, based on the combination of spin-exchange interactions in the ferromagnetic film and spin selectivity of the electron–photon conversion effect (cathodoluminescence) in a semiconductor heterostructure, is proposed and demonstrated on a model system.

Open Access

Ring artifact reduction via multiscale nonlocal collaborative filtering of spatially correlated noise

  • Pages: 876-888
  • First Published: 02 May 2021
Ring artifact reduction via multiscale nonlocal collaborative filtering of spatially correlated noise

Here, streak noise is modeled in the sinogram domain as correlated noise, which is attenuated by the Block-Matching and 3-D (BM3D) filtering algorithm applied across multiple scales. The proposed procedure is fully automatic and attenuates streak noise and the corresponding ring artifacts without creating major distortions common to other streak removal algorithms.

Open Access

X-ray tomographic reconstruction and segmentation pipeline for the long-wavelength macromolecular crystallography beamline at Diamond Light Source

  • Pages: 889-901
  • First Published: 02 May 2021
X-ray tomographic reconstruction and segmentation pipeline for the long-wavelength macromolecular crystallography beamline at Diamond Light Source

Automatic segmentation methods developed for tomography data collected on macromolecular crystallography beamline I23, Diamond Light Source, to assist with absorption corrections for very long wavelengths X-ray diffraction data are presented.

Analysis of partially coherent light propagation through the soft X-ray interference lithography beamline at SSRF

  • Pages: 902-909
  • First Published: 14 April 2021
Analysis of partially coherent light propagation through the soft X-ray interference lithography beamline at SSRF

The effect of coherence properties on EUV-IL is analysed to obtain high-quality patterns using the mutual optical intensity model.

Estimation of trapezoidal-shaped overlapping nuclear pulse parameters based on a deep learning CNN-LSTM model

  • Pages: 910-918
  • First Published: 19 April 2021
Estimation of trapezoidal-shaped overlapping nuclear pulse parameters based on a deep learning CNN-LSTM model

A parameter estimation method based on the deep learning CNN-LSTM model is proposed for overlapping nuclear pulses shaped by several exponential decay nuclear pulses.

short communications

A refraction correction for buried interfaces applied to in situ grazing-incidence X-ray diffraction studies on Pd electrodes

  • Pages: 919-923
  • First Published: 19 March 2021
A refraction correction for buried interfaces applied to in situ grazing-incidence X-ray diffraction studies on Pd electrodes

A refraction correction for grazing-incidence X-ray diffraction has been developed that can be applied to buried interfaces, including liquid–solid interfaces, allowing for a more quantitative determination of d-spacing values.

Three-dimensional fast elemental mapping by soft X-ray dual-energy focal stacks imaging

  • Pages: 924-929
  • First Published: 30 March 2021
Three-dimensional fast elemental mapping by soft X-ray dual-energy focal stacks imaging

The presented 3D dual-energy focal stacks imaging method enables different elements in a sample to be quickly distinguished or certain elements of interest to be obtained.

beamlines

Open Access

The new X-ray absorption fine-structure beamline with sub-second time resolution at the Taiwan Photon Source

  • Pages: 930-938
  • First Published: 19 March 2021
The new X-ray absorption fine-structure beamline with sub-second time resolution at the Taiwan Photon Source

The new TPS 44A beamline at the Taiwan Photon Source is presented. The beamline is equipped with a new quick-scanning monochromator (Q-Mono), which can provide both conventional step-by-step scans and on-the-fly scans for XAFS spectroscopy experiments, including XANES and EXAFS spectral measurements.

Open Access

I22: SAXS/WAXS beamline at Diamond Light Source – an overview of 10 years operation

  • Pages: 939-947
  • First Published: 19 March 2021
I22: SAXS/WAXS beamline at Diamond Light Source – an overview of 10 years operation

Beamline I22, a versatile SAXS/WAXS beamline at Diamond Light Source, is presented, along with an overview of 10 years operation of the beamline.

Open Access

The time-resolved hard X-ray diffraction endstation KMC-3 XPP at BESSY II

  • Pages: 948-960
  • First Published: 19 March 2021
The time-resolved hard X-ray diffraction endstation KMC-3 XPP at BESSY II

The KMC-3 XPP endstation of the synchrotron BESSY II is dedicated to time-resolved studies of structural dynamics of matter upon optical and/or electrical excitation using hard X-ray diffraction with an accessible time range from 17 ps to several microseconds.

The lower energy diffraction and scattering side-bounce beamline for materials science at the Canadian Light Source

  • Pages: 961-969
  • First Published: 26 March 2021
The lower energy diffraction and scattering side-bounce beamline for materials science at the Canadian Light Source

A description of a new hard X-ray diffraction beamline for materials science at the Canadian Light Source is presented.

Open Access

PROXIMA-1 beamline for macromolecular crystallography measurements at Synchrotron SOLEIL

  • Pages: 970-976
  • First Published: 05 May 2021
PROXIMA-1 beamline for macromolecular crystallography measurements at Synchrotron SOLEIL

PROXIMA-1 at Synchrotron SOLEIL has been run for 12 years as an endstation dedicated to macromolecular crystallography experiments, optimized for anomalous data recording and diffraction studies of large unit-cell crystals.

Open Access

Development of the Soft X-ray AGM–AGS RIXS beamline at the Taiwan Photon Source

  • Pages: 977-986
  • First Published: 30 March 2021
Development of the Soft X-ray AGM–AGS RIXS beamline at the Taiwan Photon Source

The development of a high-resolution and highly efficient beamline for soft X-ray resonant inelastic X-ray scattering (RIXS) located at the Taiwan Photon Source is reported.

Open Access

A UHV MOKE magnetometer complementing XMCD-PEEM at the Elettra Synchrotron

  • Pages: 995-1005
  • First Published: 30 March 2021
A UHV MOKE magnetometer complementing XMCD-PEEM at the Elettra Synchrotron

A UHV-compatible MOKE magnetometer for in situ studies operating in tandem with the PEEM at the Nanospectroscopy beamline of the Elettra synchrotron.

Open Access

The Hard X-ray Nanoprobe beamline at Diamond Light Source

  • Pages: 1006-1013
  • First Published: 09 April 2021
The Hard X-ray Nanoprobe beamline at Diamond Light Source

The design and operational performance of beamline I14, the Hard X-ray Nanoprobe at Diamond Light Source, is presented.

teaching and education

Open Access

Synchrotron radiation and X-ray free-electron lasers (X-FELs) explained to all users, active and potential

  • Pages: 1014-1029
  • First Published: 02 May 2021
Synchrotron radiation and X-ray free-electron lasers (X-FELs) explained to all users, active and potential

A new teaching strategy presents synchrotron sources and free-electron lasers (FELs) in a form accessible to readers without a theoretical physics background. This specifically includes the microbunching and amplification mechanisms of FELs.