Volume 58, Issue 8 pp. o877-o878

A new polymorph of atranorin, a lichen paradepside

Yen-Hsiang Liu

Yen-Hsiang Liu

Department of Chemistry, Louisiana State University, Baton Rouge, LA 70803-1804, USA

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Steven L. Robbs

Steven L. Robbs

Department of Chemistry, Louisiana State University, Baton Rouge, LA 70803-1804, USA

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Frank R. Fronczek

Frank R. Fronczek

Department of Chemistry, Louisiana State University, Baton Rouge, LA 70803-1804, USA

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Steven F. Watkins

Steven F. Watkins

Department of Chemistry, Louisiana State University, Baton Rouge, LA 70803-1804, USA

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Nikolaus H. Fischer

Nikolaus H. Fischer

Department of Chemistry, Louisiana State University, Baton Rouge, LA 70803-1804, USA

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First published: 29 July 2004
Citations: 1
Frank R. Fronczek, e-mail: [email protected]

Abstract

In the title compound, methyl 4-(3-formyl-2,4-di­hydroxy-6-methyl-benzoyl­oxy)-2-hydroxy-3,6-di­methyl­benzoate, C19H18O8, there are three intramolecular O—H⋯O hydrogen bonds, with lengths 2.5515 (14), 2.5711 (15), and 2.5437 (13) Å. The two aromatic rings form a dihedral angle of 60.38 (3)°, differing from that in the previously reported Pbca polymorph, viz. 84 (1)°.

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