Time–Temperature-Transformation (TTT) Cure Diagram of an Epoxy–Amine System
Abstract
A time–temperature-transformation diagram is created for the curing reaction of a diglycidylether bisphenol A (DGEBA)-based epoxy resin. It results from a kinetic analysis performed by means of dynamical differential scanning calorimetry (DSC) measurements; a gelation curve determined with isothermal and dynamical rheological tests; and a vitrification curve obtained from temperature-modulated dynamic DSC measurements. The resulting diagram is validated by comparison of isothermal measurements with the corresponding calculated curves.
Conflict of Interest
The authors declare no conflict of interest.
Open Research
Data Availability Statement
The data that support the findings of this study are available from the corresponding author upon reasonable request.