Volume 33, Issue 6 2400039
Research Article

Time–Temperature-Transformation (TTT) Cure Diagram of an Epoxy–Amine System

Claire Strasser

Corresponding Author

Claire Strasser

NETZSCH-Gerätebau GmbH, Wittelsbacherstr. 42, 95100 Selb, Germany

E-mail: [email protected]

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Elena Moukhina

Elena Moukhina

NETZSCH-Gerätebau GmbH, Wittelsbacherstr. 42, 95100 Selb, Germany

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Jürgen Hartmann

Jürgen Hartmann

Institute Zero Carbon (IZEC), Technical University of Applied Sciences Würzburg-Schweinfurt (THWS), Ignaz-Schön-Straße 11, 97421 Schweinfurt, Germany

Center for Applied Energy Research e.V. (CAE), Magdalene-Schoch-Straße 3, 97074 Würzburg, Germany

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First published: 15 June 2024
Citations: 1

Abstract

A time–temperature-transformation diagram is created for the curing reaction of a diglycidylether bisphenol A (DGEBA)-based epoxy resin. It results from a kinetic analysis performed by means of dynamical differential scanning calorimetry (DSC) measurements; a gelation curve determined with isothermal and dynamical rheological tests; and a vitrification curve obtained from temperature-modulated dynamic DSC measurements. The resulting diagram is validated by comparison of isothermal measurements with the corresponding calculated curves.

Conflict of Interest

The authors declare no conflict of interest.

Data Availability Statement

The data that support the findings of this study are available from the corresponding author upon reasonable request.

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