Communication

Insertion of Polypyrrole Chains into Montmorillonite Galleries by a Solvent-Free Mechanochemical Route

Corresponding Author

Shoji Yoshimoto

[email protected]

Aichi Industrial Technology Institute, Nishishinwari, Hitotsugi-cho, Kariya, Aichi 448-0003, Japan

Aichi Industrial Technology Institute, Nishishinwari, Hitotsugi-cho, Kariya, Aichi 448-0003, Japan. Fax: +81-566-22-8033Search for more papers by this author

Fumihiko Ohashi,

Fumihiko Ohashi

Ceramics Research Institute, AIST Chubu, 2266-98 Shimo-Shidami, Moriyama, Nagoya 463-8560, Japan

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Tetsuya Kameyama,

Tetsuya Kameyama

Ceramics Research Institute, AIST Chubu, 2266-98 Shimo-Shidami, Moriyama, Nagoya 463-8560, Japan

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Shoji Yoshimoto,

Corresponding Author

Shoji Yoshimoto

[email protected]

Aichi Industrial Technology Institute, Nishishinwari, Hitotsugi-cho, Kariya, Aichi 448-0003, Japan

Aichi Industrial Technology Institute, Nishishinwari, Hitotsugi-cho, Kariya, Aichi 448-0003, Japan. Fax: +81-566-22-8033Search for more papers by this author

Fumihiko Ohashi,

Fumihiko Ohashi

Ceramics Research Institute, AIST Chubu, 2266-98 Shimo-Shidami, Moriyama, Nagoya 463-8560, Japan

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Tetsuya Kameyama,

Tetsuya Kameyama

Ceramics Research Institute, AIST Chubu, 2266-98 Shimo-Shidami, Moriyama, Nagoya 463-8560, Japan

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First published: 17 March 2005

https://doi.org/10.1002/marc.200400529

Citations: 35

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Abstract

Summary: Non-ionic pyrrole was directly intercalated into unmodified montmorillonite (MMT) and organically modified MMT galleries by adsorption, and subsequently polymerized within the interlamellar spaces by a mechanochemical route under solvent-free conditions. XRD analysis revealed the successful intercalation of pyrrole into unmodified MMT and organically modified MMT clay galleries by mechanochemical grinding. After in situ polymerization, the XRD and FT-IR analyses confirmed the insertion of polypyrrole chains between both MMT galleries.

X-ray powder diffraction patterns of (A) pyrrole-intercalated MMT and (B) pyrrole-intercalated C18-MMT.

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Volume26, Issue6

March 18, 2005

Pages 461-466

Insertion of Polypyrrole Chains into Montmorillonite Galleries by a Solvent-Free Mechanochemical Route

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Insertion of Polypyrrole Chains into Montmorillonite Galleries by a Solvent-Free Mechanochemical Route

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