Facile synthesis of graphene/polypyrrole 3D composite for a high-sensitivity non-enzymatic dopamine detection
Zhou Rui
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Search for more papers by this authorWei Huang
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Search for more papers by this authorYong Chen
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Search for more papers by this authorCorresponding Author
Kexi Zhang
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Correspondence to: K. Zhang (E-mail: [email protected]) and Yang Cao (E-mail: [email protected])Search for more papers by this authorCorresponding Author
Yang Cao
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Correspondence to: K. Zhang (E-mail: [email protected]) and Yang Cao (E-mail: [email protected])Search for more papers by this authorJinchun Tu
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Search for more papers by this authorZhou Rui
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Search for more papers by this authorWei Huang
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Search for more papers by this authorYong Chen
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Search for more papers by this authorCorresponding Author
Kexi Zhang
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Correspondence to: K. Zhang (E-mail: [email protected]) and Yang Cao (E-mail: [email protected])Search for more papers by this authorCorresponding Author
Yang Cao
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Correspondence to: K. Zhang (E-mail: [email protected]) and Yang Cao (E-mail: [email protected])Search for more papers by this authorJinchun Tu
State Key Laboratory of Marine Resource Utilization in South China Sea, Key Laboratory of Tropical Biological Resources of Ministry of Education, College of Materials and Chemical Engineering, Hainan University, Haikou, 570228 People's Republic of China
Search for more papers by this authorABSTRACT
One kind of nanocomposite consisting of graphene and polypyrrole was synthesized via a facile and mild way with the assistant of microwave irradiation. The synthesis route was embedding the polypyrrole into the graphene flakes to form a 3D structure, to achieve larger active surface and higher electro-catalysis property. Structures and components of the composite were measured by X-ray diffraction, field emission scanning electron microscopy, and Fourier transform infrared spectroscopy. A stronger electrochemical response of electrode with modified resultant was observed in the electrochemical test. Dopamine sensor based on the composite showed a sensitivity of 363 μA mM−1 cm−2, a linear range of 1 × 10−4 M to 1 × 10−3 M, and a detection limit of 2.3 × 10−6 M (S/N = 3). © 2017 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2017, 134, 44840.
REFERENCES
- 1 Schultz, W. Curr. Opin. Neurobiol. 1997, 7, 191.
- 2 Eki̇nci̇, E.; Erdoğdu, G.; Karagözler, A. E. J. Appl. Polym. Sci. 2001, 79, 327.
- 3 Lin, F.; Gui, C.; Wen, W.; Bao, T.; Zhang, X.; Wang, S. Talanta 2016, 158, 292.
- 4 Jackowska, K.; Krysinski, P. Anal. Bioanal. Chem. 2013, 405, 3753.
- 5 Roychoudhury, A.; Basu, S.; Jha, S. K. Biosens. Bioelectron. 2016, 84, 72.
- 6 Zhao, D.; Yu, G.; Tian, K.; Xu, C. Biosens. Bioelectron. 2016, 82, 119.
- 7 Liu, X.; Peng, Y.; Qu, X.; Ai, S.; Han, R.; Zhu, X. J. Electroanal. Chem. 2011, 654, 72.
- 8 Mao, H.; Liang, J.; Ji, C.; Zhang, H.; Pei, Q.; Zhang, Y.; Zhang, Y.; Hisaeda, Y.; Song, X. M. Mater. Sci. Eng. C 2016, 65, 143.
- 9 Hwang, S. H.; Kang, D.; Ruoff, R. S.; Shin, H. S.; Park, Y. B. ACS Nano 2014, 8, 6739.
- 10 Xue, P.; Yang, X.; Lai, X.; Xia, W.; Li, P.; Fang, J. Sci. Bull. 2015, 60, 1348.
- 11 Deng, S.; Tjoa, V.; Fan, H. M.; Tan, H. R.; Sayle, D. C.; Olivo, M.; Mhaisalkar, S.; Wei, J.; Sow, C. H. J. Am. Chem. Soc. 2012, 134, 4905.
- 12 Yoo, B. M.; Shin, H. J.; Yoon, H. W.; Park, H. B. J. Appl. Polym. Sci. 2014, 131, DOI: 10.1002/app.39628.
- 13 Lim, Y. S.; Tan, Y. P.; Lim, H. N.; Tan, W. T.; Mahnaz, M. A.; Talib, Z. A.; Huang, N. M.; Kassim, A.; Yarmo, M. A. J. Appl. Polym. Sci. 2013, 128, 224.
- 14 Ren, P. G.; Yan, D. X.; Chen, T.; Zeng, B. Q.; Li, Z. M. J. Appl. Polym. Sci. 2011, 121, 3167.
- 15 Wen, Y.; Wen, W.; Zhang, X.; Wang, S. Biosens. Bioelectron. 2016, 79, 894.
- 16 Shang, N. G.; Papakonstantinou, P.; McMullan, M.; Chu, M.; Stamboulis, A.; Potenza, A.; Dhesi, S. S.; Marchetto, H. Adv. Funct. Mater. 2008, 18, 3506.
- 17 Liu, S.; Wang, L.; Tian, J.; Lu, W.; Zhang, Y.; Wang, X.; Sun, X. J. Nanoparticle Res. 2011, 13, 4731.
- 18 Yujie, Z.; Wenbing, H.; Bo, L.; Cheng, P.; Chunhai, F.; Qing, H. Nanotechnology 2011, 22, 345601.
- 19 Kim, H.; Abdala, A. A.; Macosko, C. W. Macromolecules 2010, 43, 6515.
- 20 Das, I.; Agrawal, N. R.; Pandey, A. K.; Choudhary, R.; Pandey, P. C. J. Appl. Polym. Sci. 2015, 132, DOI: 10.100/app.42729.
- 21 Imran, S. M.; Shao, G. N.; Haider, M. S.; Abbas, N.; Hussain, M.; Kim, H. T. J. Appl. Polym. Sci. 2015, 132, DOI: 10.1002/app.41800.
- 22 Zhao, Y.; Liu, J.; Hu, Y.; Cheng, H.; Hu, C.; Jiang, C.; Jiang, L.; Cao, A.; Qu, L. Adv. Mater. 2013, 25, 591.
- 23 Liu, T.; Finn, L.; Yu, M.; Wang, H.; Zhai, T.; Lu, X.; Tong, Y.; Li, Y. Nano Lett. 2014, 14, 2522.
- 24 Sun, R.; Chen, H.; Li, Q.; Song, Q.; Zhang, X. Nanoscale 2014, 6, 12912.
- 25 Ulubay, Ş.; Dursun, Z. Talanta 2010, 80, 1461.
- 26 Zhang, D.; Zhang, X.; Chen, Y.; Yu, P.; Wang, C.; Ma, Y. J. Power Sources 2011, 196, 5990.
- 27 Stankovich, S.; Dikin, D. A.; Dommett, G. H. B.; Kohlhaas, K. M.; Zimney, E. J.; Stach, E. A.; Piner, R. D.; Nguyen, S. T.; Ruoff, R. S. Nature 2006, 442, 282.
- 28 Yan, J.; Wei, T.; Shao, B.; Fan, Z.; Qian, W.; Zhang, M.; Wei, F. Carbon 2010, 48, 487.
- 29 He, Y.; Bai, Y.; Yang, X.; Zhang, J.; Kang, L.; Xu, H.; Shi, F.; Lei, Z.; Liu, Z. H. J. Power Sources 2016, 317, 10.
- 30 Bose, S.; Kuila, T.; Uddin, M. E.; Kim, N. H.; Lau, A. K. T.; Lee, J. H. Polymer 2010, 51, 5921.
- 31 Wu, T. M.; Lin, S. H. J. Polym. Sci. Part A: Polym. Chem. 2006, 44, 6449.
- 32 Bissessur, R.; Liu, P. K. Y.; Scully, S. F. Synth. Met. 2006, 156, 1023.