Zeitschrift für anorganische und allgemeine Chemie

Short Communication

Facile Synthesis and Crystal Structure of 1,1,1,3-Tetranitro-3-azabutane^†

Corresponding Author

Thomas M. Klapötke Prof. Dr.

[email protected]

München, Department Chemie und Biochemie der Ludwig-Maximilians-Universität

Department Chemie und Biochemie der Ludwig-Maximilians-Universität, Butenandtstr. 5-13 (D), D-81377 München, Fax: -49-89-2180-77492Search for more papers by this author

Burkhard Krumm,

Burkhard Krumm

München, Department Chemie und Biochemie der Ludwig-Maximilians-Universität

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Matthias Scherr,

Matthias Scherr

München, Department Chemie und Biochemie der Ludwig-Maximilians-Universität

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Gunnar Spieß,

Gunnar Spieß

München, Department Chemie und Biochemie der Ludwig-Maximilians-Universität

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F. Xaver Steemann,

F. Xaver Steemann

München, Department Chemie und Biochemie der Ludwig-Maximilians-Universität

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Thomas M. Klapötke Prof. Dr.,

Corresponding Author

Thomas M. Klapötke Prof. Dr.

[email protected]

München, Department Chemie und Biochemie der Ludwig-Maximilians-Universität

Department Chemie und Biochemie der Ludwig-Maximilians-Universität, Butenandtstr. 5-13 (D), D-81377 München, Fax: -49-89-2180-77492Search for more papers by this author

Burkhard Krumm,

Burkhard Krumm

München, Department Chemie und Biochemie der Ludwig-Maximilians-Universität

Search for more papers by this author

Matthias Scherr,

Matthias Scherr

München, Department Chemie und Biochemie der Ludwig-Maximilians-Universität

Search for more papers by this author

Gunnar Spieß,

Gunnar Spieß

München, Department Chemie und Biochemie der Ludwig-Maximilians-Universität

Search for more papers by this author

F. Xaver Steemann,

F. Xaver Steemann

München, Department Chemie und Biochemie der Ludwig-Maximilians-Universität

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First published: 26 May 2008

https://doi.org/10.1002/zaac.200800061

Citations: 10

^†

Dedicated to Professor Heinrich Nöth on the Occasion of his 80^th Birthday

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Abstract

The synthesis of 1,1,1,3-tetranitro-3-azabutane is disclosed and compared with the known method. The structure of 1,1,1,3-tetranitro-3-azabutane is identified by multi-nuclear NMR spectroscopy and X-ray single crystal structure determination.

REFERENCES

1a I. S. Shvartz, M. M. Krayushkin, V. V. Sevost′yanova, V. N. Yarovenko, Russ. Chem. Bull., 1979, 28, 1000–1002.
10.1007/BF00963315
Web of Science® Google Scholar
1b H. Feuer, W. A. Swarts, J. Org. Chem., 1962, 27, 1455–1457.
10.1021/jo01051a515
CAS Web of Science® Google Scholar
2a M. J. Kamlet, 6^th Proc. Symp. Int. Detonation, Off. Nav. Res., Techn. Rep., ACR (US), 1976, 312–322.
Google Scholar
2b C. B. Storm, J. R. Stine, J. F. Cramer in Chemistry and Physics of Energetic Materials, (Ed.: ), Kluwer Academic, Dordrecht, 1990, p. 623.
Google Scholar
2c J. Edwards, C. Eybl, B. Johnson, Int. J. Quant. Chem., 2004, 100, 713–719.
10.1002/qua.20235
CAS Web of Science® Google Scholar
3a B. L. Korsounskii, V. G. Matveev, L. D. Nazina, G. M. Nazin, Russ. Chem. Bull., 1998, 47, 253–258.
10.1007/BF02498944
CAS Web of Science® Google Scholar
3b R. S. Stepanov, L. A. Kruglyakova, A. M. Astakhov, Russ. J. Org. Chem., 2001, 37, 1793.
10.1023/A:1013955430589
CAS Web of Science® Google Scholar
3c G. M. Nazin, V. G. Prokudin, G. B. Manelis, Russ. Chem. Bull., 2000, 49, 234–237.
10.1007/BF02494664
CAS Web of Science® Google Scholar
4 F. D. Chattaway, Chem. News J. Ind. Sci., 1910, 102, 307–308.
CAS Google Scholar
5 H. Bock, R. Dienelt, H. Schödel, Z. Havlas, J. Chem. Soc., Chem. Commun., 1993, 1792–1793.
10.1039/c39930001792
CAS Web of Science® Google Scholar
6 J. Denkstein, V. Kaderabek, Coll. Czech. Chem. Commun., 1960, 25, 2334–2340.
10.1135/cccc19602334
CAS Web of Science® Google Scholar
G. A. Gareev, L. P. Kirillova, V. M. Shulgina, S. R. Buzillova, L. P. Vologdina, L. I. Vereshchagin, J. Org. Chem. USSR (Engl. Transl.) 1988, 24, 2003–2007.
Google Scholar
7G. M. Sheldrick, Universität Göttingen, Germany, 1997.
Google Scholar
8a H. D. Flack, Acta Crystallogr., 1983, A 39, 876–881.
10.1107/S0108767383001762
CAS Web of Science® Google Scholar
8b H. D. Flack, G. Bernardinelli, J. Appl. Crystallogr., 2000, 33, 1143–1148.
10.1107/S0021889800007184
CAS Web of Science® Google Scholar

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Volume634, Issue8

July 2008

Pages 1244-1246

Facile Synthesis and Crystal Structure of 1,1,1,3-Tetranitro-3-azabutane^†

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Facile Synthesis and Crystal Structure of 1,1,1,3-Tetranitro-3-azabutane†

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Facile Synthesis and Crystal Structure of 1,1,1,3-Tetranitro-3-azabutane^†