Variations in surface fractal characteristics of coal subjected to liquid CO2 phase change fracturing
Corresponding Author
Xianfeng Liu
State Key Laboratory of Coal Mine Disaster Dynamics and Control, School of Resources and Safety Engineering, Chongqing University, Chongqing, China
State Key Laboratory Cultivation Base for Gas Geology and Gas Control, Henan Polytechnic University, Jiaozuo, China
Correspondence
Xianfeng Liu and Zepeng Wang, State Key Laboratory of Coal Mine Disaster Dynamics and Control, School of Resources and Safety Engineering, Chongqing University, Chongqing 400044, China.
Email: [email protected] (X. L.) and [email protected] (Z. W.)
Search for more papers by this authorCorresponding Author
Zepeng Wang
State Key Laboratory of Coal Mine Disaster Dynamics and Control, School of Resources and Safety Engineering, Chongqing University, Chongqing, China
Correspondence
Xianfeng Liu and Zepeng Wang, State Key Laboratory of Coal Mine Disaster Dynamics and Control, School of Resources and Safety Engineering, Chongqing University, Chongqing 400044, China.
Email: [email protected] (X. L.) and [email protected] (Z. W.)
Search for more papers by this authorDazhao Song
School of Civil and Resource Engineering, University of Science and Technology Beijing, Beijing, China
Search for more papers by this authorXueqiu He
School of Civil and Resource Engineering, University of Science and Technology Beijing, Beijing, China
Search for more papers by this authorTao Yang
School of Safety Engineering, North China Institute of Science and Technology, Beijing, China
Search for more papers by this authorCorresponding Author
Xianfeng Liu
State Key Laboratory of Coal Mine Disaster Dynamics and Control, School of Resources and Safety Engineering, Chongqing University, Chongqing, China
State Key Laboratory Cultivation Base for Gas Geology and Gas Control, Henan Polytechnic University, Jiaozuo, China
Correspondence
Xianfeng Liu and Zepeng Wang, State Key Laboratory of Coal Mine Disaster Dynamics and Control, School of Resources and Safety Engineering, Chongqing University, Chongqing 400044, China.
Email: [email protected] (X. L.) and [email protected] (Z. W.)
Search for more papers by this authorCorresponding Author
Zepeng Wang
State Key Laboratory of Coal Mine Disaster Dynamics and Control, School of Resources and Safety Engineering, Chongqing University, Chongqing, China
Correspondence
Xianfeng Liu and Zepeng Wang, State Key Laboratory of Coal Mine Disaster Dynamics and Control, School of Resources and Safety Engineering, Chongqing University, Chongqing 400044, China.
Email: [email protected] (X. L.) and [email protected] (Z. W.)
Search for more papers by this authorDazhao Song
School of Civil and Resource Engineering, University of Science and Technology Beijing, Beijing, China
Search for more papers by this authorXueqiu He
School of Civil and Resource Engineering, University of Science and Technology Beijing, Beijing, China
Search for more papers by this authorTao Yang
School of Safety Engineering, North China Institute of Science and Technology, Beijing, China
Search for more papers by this authorFunding information: Program for Changjiang Scholars and Innovative Research Team in University, Grant/Award Number: IRT_17R112; the State Key Laboratory Cultivation Base for Gas Geology and Gas Control (Henan Polytechnic University), Grant/Award Number: WS2019B08; National Natural Science Foundation of China, Grant/Award Numbers: U19B2009, 51974127, 51634001
Summary
Enhancement of coal permeability plays the key role in methane extraction underground coalmine. As the physical blasting method, liquid CO2 phase change fracturing (LCPCF) technique can effectively stimulate the coal reservoirs, further enhance the coal permeability. In this work, the combination of scanning electron microscopy (SEM) and mercury intrusion porosimetry (MIP) was adopted to quantitatively evaluate the variations in the pore/fracture structure and fractal characteristics of coal subjected to LCPCF. Fracture fractal dimension (DF) and pore fractal dimensions (DP1, DP2) are calculated based on the SEM images and MIP data, respectively. After conducting LCPCF, a large number of microfracture and macropore clusters are generated and observed in SEM images. The maximum fracture ratio in treated coal is enhanced by approximately 200% compared with that in raw coal. MIP results show that pore distribution within coal exhibits a nonlinear alteration with four stages and the pore connectivity of coal is improved after LCPCF. The impact of LCPCF on pore/microfracture characteristics of coal is closely correlated with the distance from the fracturing borehole. The maximum values of DF and DP1 are found at the distance of around 2.0 m, indicating the best fracturing effect at such distance. It has been found that the effective influence scope of LCPCF on coal is within 7.0 m. The evolution of coal pore/fracture structure during LCPCF is attributed to the new pore/fracture generation and the conversion of original micropores into larger ones. Knowledge of these properties is essential for the application LCPCF in methane drainage.
REFERENCES
- 1Salmachi A, Dunlop E, Rajabi M, et al. Investigation of permeability change in ultradeep coal seams using time-lapse pressure transient analysis: a pilot project in the Cooper Basin. Australia AAPG Bull. 2019; 103(1): 91-107.
- 2He X, Liu X, Nie B, Song D. FTIR and Raman spectroscopy characterization of functional groups in various rank coals. Fuel. 2017; 206: 555-563.
- 3Li X, Li Z, Wang E, et al. Pattern recognition of mine microseismic and blasting events based on wave fractal features. Fractals. 2018; 26(3):1850029.
- 4Kong X, Wang E, He X, Zhao E, Zhao C. Mechanical characteristics and dynamic damage evolution mechanism of coal samples in compressive loading experiments. Eng Fract Mech. 2019; 210: 160-169.
- 5Karacan CÖ, Goodman GVR. Probabilistic modeling using bivariate normal distributions for identification of flow and displacement intervals in longwall overburden. Int J Rock Mech Min Sci. 2011; 48(1): 27-41.
- 6Szlązak N, Obracaj D, Swolkień J. Methane drainage from roof strata using an overlying drainage gallery. Int J Coal Geol. 2014; 136: 99-115.
- 7Liu XF, Nie BS, Wang WX, Wang Z, Zhang L. The use of AFM in quantitative analysis of pore characteristics in coal and coal-bearing shale. Mar Petrol Geol. 2019; 105: 331-337.
- 8Schatzel SJ, Karacan CÖ, Dougherty H, Goodman GVR. An analysis of reservoir conditions and responses in longwall panel overburden during mining and its effect on gob gas well performance. Eng Geol. 2012; 127: 65-74.
- 9He X, Liu X, Song D, Nie B. Effect of microstructure on electrical property of coal surface. Appl Surf Sci. 2019; 483: 713-720.
- 10Goraya NS, Rajpoot N, Marriyappan SB. Coal bed methane enhancement techniques: a review. ChemistrySelect. 2019; 4(12): 3585-3601.
- 11Zagorščak R, Thomas HR. Dynamic transport and reaction behaviour of high-pressure gases in high-rank coal. J Nat Gas Sci Eng. 2019; 71: 102978.
- 12Liu SM, Li XL, Wang DK, Wu M, Yin G, Li M. Mechanical and acoustic emission characteristics of coal at temperature impact. Nat Resour Res. 2019; 29: 1-18. https://doi.org/10.1007/s11053-019-09562-w.
- 13Yang Y, Liu Z, Yao J, et al. Flow simulation of artificially induced microfractures using digital rock and lattice Boltzmann methods. Energies. 2018; 11(8): 2145.
- 14Durucan S, Edwards JS. The effects of stress and fracturing on permeability of coal. Mining Sci Tech. 1986; 3(3): 205-216.
10.1016/S0167-9031(86)90357-9 Google Scholar
- 15Lecampion B, Bunger A, Zhang X. Numerical methods for hydraulic fracture propagation: a review of recent trends. J Nat Gas Sci Eng. 2018; 49: 66-83.
- 16Barth-Naftilan E, Sohng J, Saiers JE. Methane in groundwater before, during, and after hydraulic fracturing of the Marcellus shale. Proc Natl Acad Sci. 2018; 115(27): 6970-6975.
- 17McIntosh JC, Ferguson G. Conventional oil–the forgotten part of the water-energy nexus. Groundwater. 2019; 57: 669-677. https://doi.org/10.1111/gwat.12917.
- 18Santos IC, Hildenbrand ZL, Schug KA. A review of analytical methods for characterizing the potential environmental impacts of unconventional oil and gas development. Anal Chem. 2018; 91(1): 689-703.
- 19Stringfellow WT, Domen JK, Camarillo MK, Sandelin WL, Borglin S. Physical, chemical, and biological characteristics of compounds used in hydraulic fracturing. J Hazard Mater. 2014; 275: 37-54.
- 20Faber AH, Annevelink MPJA, Schot PP, et al. Chemical and bioassay assessment of waters related to hydraulic fracturing at a tight gas production site. Sci Total Environ. 2019; 690: 636-646.
- 21Akyon B, Lipus D, Bibby K. Glutaraldehyde inhibits biological treatment of organic additives in hydraulic fracturing produced water. Sci Total Environ. 2019; 666: 1161-1168.
- 22Rogers JD, Burke TL, Osborn SG, Ryan JN. A framework for identifying organic compounds of concern in hydraulic fracturing fluids based on their mobility and persistence in groundwater. Environ Sci Tech Lett. 2015; 2(6): 158-164.
- 23Naik S, Yang S, Woolley M, Bedrikovetsky P. Analytical modelling of the water block phenomenon in hydraulically fractured wells. J Nat Gas Sci Eng. 2019; 67: 56-70.
- 24Zhang Y, Deng J, Deng H, Ke B. Peridynamics simulation of rock fracturing under liquid carbon dioxide blasting. Int J Damage Mech. 2019; 28(7): 1038-1052.
- 25Ke B, Zhou K, Xu C, Ren G, Jiang T. Thermodynamic properties and explosion energy analysis of carbon dioxide blasting systems. Mining Tech. 2019; 128(1): 39-50.
10.1080/25726668.2018.1527982 Google Scholar
- 26Singh SP. Non-explosive applications of the PCF concept for underground excavation. Tunnell Underground Space Tech. 1998; 13(3): 305-311.
- 27Wu F, Wei X, Chen Z, et al. Numerical simulation and parametric analysis for designing high energy gas fracturing. J Nat Gas Sci Eng. 2018; 53: 218-236.
- 28Vidanovic N, Ognjanovic S, Ilincic N, et al. Application of unconventional methods of underground premises construction in coal mines. Tech Technol Edu Manag. 2011; 6(4): 861-865.
- 29Vishal V. In-situ disposal of CO2: liquid and supercritical CO2 permeability in coal at multiple down-hole stress conditions. J Carbondioxide Util. 2017; 17: 235-242.
- 30Patrick V. CO2 blasting in Europe. Nuclear Eng Int. 1995; 40(448): 43-45.
- 31White CM, Smith DH, Jones KL, et al. Sequestration of carbon dioxide in coal with enhanced coalbed methane recovery a review. Energy Fuel. 2005; 19(3): 659-724.
- 32Liu X, Song D, He X, Wang Z, Zeng M, Wang L. Quantitative analysis of coal nanopore characteristics using atomic force microscopy. Powder Technol. 2019; 346: 332-340.
- 33Chen H, Wang Z, Chen X, Chen X, Wang L. Increasing permeability of coal seams using the phase energy of liquid carbon dioxide. J Carbondioxide Util. 2017; 19: 112-119.
- 34Isaka BLA, Ranjith PG, Rathnaweera TD, Wanniarachchi WAM, Kumari WGP, Haque A. Testing the frackability of granite using supercritical carbon dioxide: insights into geothermal energy systems. J Carbondioxide Util. 2019; 34: 180-197.
- 35Zhang Y, Lebedev M, Sarmadivaleh M, Barifcani A, Iglauer S. Swelling-induced changes in coal microstructure due to supercritical CO2 injection. Geophys Res Lett. 2016; 43: 9077-9083.
- 36Harpalani S, Mitra A. Impact of CO2 injection on flow behavior of coalbed methane reservoirs. Transp Porous Media. 2010; 82(1): 141-156.
- 37Wu D, Liu X, Liang B, Sun K, Xiao X. Experiments on displacing methane in coal by injecting supercritical carbon dioxide. Energy Fuel. 2018; 32(12): 12766-12771.
- 38Liu K, Sheng JJ. Experimental study of the effect of stress anisotropy on fracture propagation in eagle ford shale under water imbibition. Eng Geol. 2019; 249: 13-22.
- 39Kumari WGP, Ranjith PG, Perera MSA, et al. Hydraulic fracturing under high temperature and pressure conditions with micro CT applications: geothermal energy from hot dry rocks. Fuel. 2018; 230: 138-154.
- 40Liu X, Song D, He X, Nie B, Wang L. Insight into the macromolecular structural differences between hard coal and deformed soft coal. Fuel. 2019; 245: 188-197.
- 41Yang X, Wen G, Sun H, et al. Environmentally friendly techniques for high gas content thick coal seam stimulation—multi-discharge CO2 fracturing system. J Nat Gas Sci Eng. 2019; 61: 71-82.
- 42Ranathunga AS, Perera MSA, Ranjith PG, Zhang XG, Wu B. Super-critical carbon dioxide flow behaviour in low rank coal: a meso-scale experimental study. J Carbondioxide Util. 2017; 20: 1-13.
- 43Sampath K, Perera MSA, Li D, et al. Characterization of dynamic mechanical alterations of supercritical CO2-interacted coal through gamma-ray attenuation, ultrasonic and X-ray computed tomography techniques. J Petrol Sci Eng. 2019; 174: 268-280.
- 44Sampath K, Perera MSA, Ranjith PG, et al. Qualitative and quantitative evaluation of the alteration of micro-fracture characteristics of supercritical CO2-interacted coal. J Supercrit Fluids. 2019; 147: 90-101.
- 45Hu G, He W, Sun M. Enhancing coal seam gas using liquid CO2 phase-transition blasting with cross-measure borehole. J Nat Gas Sci Eng. 2018; 60: 164-173.
- 46Li H, Shi S, Lu J, Ye Q, Lu Y, Zhu X. Pore structure and multifractal analysis of coal subjected to microwave heating. Powder Technol. 2019; 346: 97-108.
- 47Kong X, Wang E, Li S, et al. Fractals and chaos characteristics of acoustic emission energy about gas-bearing coal during loaded failure. Fractals. 2019; 27(5): 1950072.
- 48Liu X, Nie B. Fractal characteristics of coal samples utilizing image analysis and gas adsorption. Fuel. 2016; 182: 314-322.
- 49Xia Y, Cai J, Perfect E, Wei W, Zhang Q, Meng Q. Fractal dimension, lacunarity and succolarity analyses on CT images of reservoir rocks for permeability prediction. J Hydrol. 2019; 579: 124198.
- 50Wen H, Li Z, Deng J, et al. Influence on coal pore structure during liquid CO2-ECBM process for CO2 utilization. J Carbondioxide Util. 2017; 21: 543-552.
- 51Gao F, Tang L, Zhou K, Zhang Y, Ke B. Mechanism analysis of liquid carbon dioxide phase transition for fracturing rock masses. Energies. 2018; 11(11): 2909.
- 52Li W, Ren T, Busch A, et al. Architecture, stress state and permeability of a fault zone in Jiulishan coal mine, China: implication for coal and gas outbursts. Int J Coal Geol. 2018; 198: 1-13.
- 53Alfonso I, Beltran A, Abatal M, et al. Fractal dimension determination of rock pores by multi-scale analysis of images obtained using OM. SEM XCT Fract. 2018; 26(5): 1850067.
- 54Li H, Shi S, Lin B, et al. Effects of microwave-assisted pyrolysis on the microstructure of bituminous coals. Energy. 2019; 187: 115986.
- 55Morales FA, Aristizábal LC. A discussion on the transmission conditions for saturated fluid flow through porous media with fractal microstructure. Fractals. 2019; 27(3): 1950033.
- 56Cai J, Zhang L, Ju Y, et al. An introduction to fractal-based approaches in unconventional reservoirs—part I. Fractals. 2018; 26(2): 1802001.
- 57Zhang L, Zhang X, Chai H, et al. Pore structure characterization for a continental lacustrine shale parasequence based on fractal theory. Fractals. 2019; 27(1): 1940006.
- 58Foroutan-pour K, Dutilleul P, Smith DL. Advances in the implementation of the box-counting method of fractal dimension estimation. Appl Math Comput. 1999; 105(2–3): 195-210.
- 59Panesar DK, Francis J. Influence of limestone and slag on the pore structure of cement paste based on mercury intrusion porosimetry and water vapour sorption measurements. Construct Build Mater. 2014; 52: 52-58.
- 60Friesen WI, Mikula RJ. Fractal dimensions of coal particles. J Colloid Interface Sci. 1987; 120(1): 263-271.
- 61Chen Y, Zhang H, Zhu Z, et al. A new shock-wave test apparatus for liquid CO2 blasting and measurement analysis. Meas Control. 2019; 52: 399-408.
- 62Zhu H, Ju Y, Huang C, et al. Pore structure variations across structural deformation of Silurian Longmaxi shale: An example from the Chuandong thrust-Fold Belt. Fuel. 2019; 241: 914-932.
- 63Yu K, Shao C, Ju Y, Qu Z. The genesis and controlling factors of micropore volume in transitional coal-bearing shale reservoirs under different sedimentary environments. Mar Petrol Geol. 2019; 102: 426-438.
- 64Luo C, Zhang D, Lun Z, et al. Displacement behaviors of adsorbed coalbed methane on coals by injection of SO2/CO2 binary mixture. Fuel. 2019; 247: 356-367.
- 65Yang Y, Zhang W, Gao Y, et al. Influence of stress sensitivity on microscopic pore structure and fluid flow in porous media. J Nat Gas Sci Eng. 2016; 36: 20-31.
- 66Zhu HJ, Ju YW, Qi Y, Huang C, Zhang L. Impact of tectonism on pore type and pore structure evolution in organic-rich shale: implications for gas storage and migration pathways in naturally deformed rocks. Fuel. 2018; 228: 272-289.
- 67Akhondzadeh H, Keshavarz A, Alyaseri AZ, et al. Pore-scale analysis of coal cleat network evolution through liquid nitrogen treatment: a micro-computed tomography investigation. Int J Coal Geol. 2020; 219: 103370.
- 68Liu X, Song D, He X, Wang Z, Zeng M, Deng K. Nanopore structure of deep-burial coals explored by AFM. Fuel. 2019; 246: 9-17.