Synthesis and Characterization of Ordered Mesoporous Aluminosilicate Molecular Sieves with High Stability in High-Temperature Steam
Yong-Ming Luo
Institute of Catalysis, Department of Chemistry, Zhejiang University (Xixi campus), Hangzhou, Zhejiang 310028, China
Faculty of Environmental Science and Engineering, Kunming University of Science and Technology, Kunming, Yunnan 650093, China
Search for more papers by this authorZhao-Yin Hou
Institute of Catalysis, Department of Chemistry, Zhejiang University (Xixi campus), Hangzhou, Zhejiang 310028, China
Search for more papers by this authorDing-Feng Jin
Institute of Catalysis, Department of Chemistry, Zhejiang University (Xixi campus), Hangzhou, Zhejiang 310028, China
Search for more papers by this authorXiao-Ming Zheng
Tel.: 0086-0571-88273272; Fax: 0086-0571-88273283
Search for more papers by this authorYong-Ming Luo
Institute of Catalysis, Department of Chemistry, Zhejiang University (Xixi campus), Hangzhou, Zhejiang 310028, China
Faculty of Environmental Science and Engineering, Kunming University of Science and Technology, Kunming, Yunnan 650093, China
Search for more papers by this authorZhao-Yin Hou
Institute of Catalysis, Department of Chemistry, Zhejiang University (Xixi campus), Hangzhou, Zhejiang 310028, China
Search for more papers by this authorDing-Feng Jin
Institute of Catalysis, Department of Chemistry, Zhejiang University (Xixi campus), Hangzhou, Zhejiang 310028, China
Search for more papers by this authorXiao-Ming Zheng
Tel.: 0086-0571-88273272; Fax: 0086-0571-88273283
Search for more papers by this authorAbstract
The ordered mesoporous aluminosilicate molecular sieve (MASMS-1) stable in the high-temperature steam has been successfully synthesized from the assembly of diluted ZSM-5-type precursor with mesoporous MCM-41. The material was characterized by XRD, N2 adsorption-desorption, FE-SEM, TEM, FT-IR spectroscopy and 27Al MAS NMR techniques. This mesoporous material shows high stability in the high-temperature steam [H2O (ψ=20%) in N2 at 800 °C for 4 h], which might be ascribed to the synergistic effect of both thick walls containing zeolite-like five-membered ring subunits and highly condensed surface silanol groups.
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