Article

Synthesis, optical, and thermal properties of polyimides containing flexible ether linkage

Corresponding Author

İsmet Kaya

[email protected]

orcid.org/0000-0002-9813-2962

Polymer Synthesis and Analysis Laboratory, Department of Chemistry, Faculty of Science and Arts, Çanakkale Onsekiz Mart University, Çanakkale 17020, Turkey

Correspondence to: İ. Kaya (E-mail: [email protected])Search for more papers by this author

Musa Kamacı,

Musa Kamacı

Polymer Synthesis and Analysis Laboratory, Department of Chemistry, Faculty of Science and Arts, Çanakkale Onsekiz Mart University, Çanakkale 17020, Turkey

Engineering of Faculty, Department of Machine Engineering, Piri Reis University, Tuzla, Istanbul 34940, Turkey

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İsmet Kaya,

Corresponding Author

İsmet Kaya

[email protected]

orcid.org/0000-0002-9813-2962

Polymer Synthesis and Analysis Laboratory, Department of Chemistry, Faculty of Science and Arts, Çanakkale Onsekiz Mart University, Çanakkale 17020, Turkey

Correspondence to: İ. Kaya (E-mail: [email protected])Search for more papers by this author

Musa Kamacı,

Musa Kamacı

Polymer Synthesis and Analysis Laboratory, Department of Chemistry, Faculty of Science and Arts, Çanakkale Onsekiz Mart University, Çanakkale 17020, Turkey

Engineering of Faculty, Department of Machine Engineering, Piri Reis University, Tuzla, Istanbul 34940, Turkey

Search for more papers by this author

First published: 23 April 2018

https://doi.org/10.1002/app.46573

Citations: 20

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ABSTRACT

The goal of this article was to synthesize a series of flexible polyimides containing ether linkage in main chain and clarified the effect of this ether linkage on some physical properties such as optical and thermal decomposition. Also, different functional group effects such as carbonyl (CO), hexa-fluoro-isopropylidene [C(CF₃)₂] and phenyl (C₆H₅) on these physical properties were evaluated. The structural characterization of poly(ether imide)s was performed using Fourier transform infrared, ¹H-nuclear magnetic resonance (NMR), and ¹³C-NMR techniques. Optical band gap of polyimides was calculated in the range from 2.57 to 2.81 eV. Thermal characterization of poly(ether imide)s was carried out using thermogravimetry–differential thermal analysis and differential scanning calorimetry. Thermal stability of poly(ether imide)s was evaluated by initial decomposition temperature (T_on) and char. T_on value of polymers was determined in the range from 100 to 195 °C. In addition, glass transition temperatures of poly(ether imide)s were found between 144 and 148 °C. © 2018 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2018, 135, 46573.

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Volume135, Issue31

August 15, 2018

46573

Synthesis, optical, and thermal properties of polyimides containing flexible ether linkage

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