Inorganic Syntheses

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About this book

The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Author Bios

Donald W. Murphy is the Editor-in-Chief of Inorganic Syntheses: Nonmolecular Solids, Volume 30, published by Wiley.

Leonard V. Interrante, PhD, is Professor of Chemistry at Rensselaer Polytechnic Institute. He is Editor of the ACS journal, Chemistry of Materials.

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Frontmatter (Pages: i-xvii)

Tungsten Dichloride (Pages: 1-6)

G. M. Ehrlich, P. E. Rauch, F. J. Disalvo, Robert E. Mccarley,

Zirconium Monochloride and Monobromide (Pages: 6-11)

Richard L. Daake, John D. Corbett, Donald W. Murphy,

Lanthanum Triiodide (and Other Rare-Earth Metal Triiodides) (Pages: 11-16)

John D. Corbett, Arndt Simon,

Lanthanum Diiodide (Pages: 17-19)

John D. Corbett, Arndt Simon,

Rare-Earth Sesquisulfides, Ln₂S₃ (Pages: 20-22)

A. W. Sleight, D. P. Kelly, R. Kershaw, A. Wold,

Group IV Sulfides (Pages: 22-27)

Lawrence E. Conroy, R. J. Bouchard,

Titanium Disulfide (Pages: 28-32)

M. J. Mckelvy, W. S. Claunsinger, G. Ouvrard,

Metathetical Precursor Route to Molybdenum Disulfide (Pages: 33-37)

Philippe R. Bonneau, John B. Wiley, Richard B. Kaner, Michael F. Mansuktto,

Lithium Nitride, Li₃N (Pages: 38-45)

E. Schönherr, A. Kohler, G. Pfrommer, K J. Fi Nielsen,

Aluminum Nitride (Pages: 46-50)

F. C. Sauls, L. V. Interrante, S. N. Shaikh, L. Carpenter Jr., Wayne L. Gladfelter,

Electrochemical Syntheses of Binary Silver Oxides (Pages: 50-55)

Peter Fischer, Martin Jansen, S. M. Zahurak,

Trisodium Heptaphosphide and Trisodium Undecaphosphide (Pages: 56-63)

Wolfgang Hönle, Hans Georg Von Schnering, D. W. Murphy,

Lead Ruthenium Oxide, Pb₂[Ru_2-XPb_X ⁴⁺]O_6.5 (Pages: 64-68)

H. S. Horowitz, J. M. Longo, J. T. Lewandowski, J. Murphy,

Calcium Manganese Oxide, Ca₂Mn₃O₈ (Pages: 68-72)

Harold S. Horowitz, John M. Longo, Carlye Booth, Christopher Case,

Ternary Chlorides and Bromides of the Rare-Earth Elements (Pages: 72-81)

Gerd Meyer, S.-J. Hwu, J. D. Corbett,

Cesium Scandium(II) Trichloride (Pages: 81-84)

K. R. Poeppelmeier, J. D. Corbett, Gerd Meyer,

A One-Dimensional Polychalcogenide, K₄Ti₃S₁₄ ¹ (Pages: 84-85)

Steven A. Sunshine, Doris Kang, James A. Ibers, Edward G. Gillan,

Synthesis of K₄M₃Te₁₇ (M =Zr, Hf)¹ and K₃Cunb₂Se₁₂ ² (Pages: 86-88)

Patricia M. Keane, Ying-Jie Lu, James A. Ibers, John B. Wiley,

Synthesis of Ternary Chalcogenides in Molten Polychalcogenide Salts: α-KCuQ₄, KAuS₅, NaBiS₂, KFeQ₂ (Q = S, Se) (Pages: 88-95)

Younbong Park, Timothy J. Mccarthy, Anthony C. Sutorlk, Mercouri G. Kanatzidis, Edward G. Gillan,

Single Crystals of Transition-Metal Dioxides (Pages: 96-104)

D. B. Rogers, S. R. Butler, R. D. Shannon, A. Wold, R. Kershaw,

Molybdenum(IV) Oxide and Tungsten(IV) Oxide Single Crystals (Pages: 105-107)

Lawrence E. Conroy, Lina Ben-Dor, R. Kershaw, A. Wold,

Niobium Monoxide (Pages: 108-110)

T. B. Reed, E. R. Pollard, L. E. Lonney, R. E. Loehman, J. M. Honig,

Barium Titanate, Batio₃ (Pages: 111-112)

Francis S. Galasso, Michael Kestigan,

Bismuth Titanate, Bi₄Ti₃O₁₂ (Pages: 112-113)

Francis S. Galasso, Michael Kestigan,

Sodium Tungsten Bronzes (Pages: 114-119)

C. T. Hauck, A. Wold, E. Banks, R. Seiver, H. A. Eick,

Potassium Molybdenum Oxide ‘Blue Bronze”: K_0.30MoO₃ (Pages: 119-124)

L. F. Schneemeyer, David Dicarlo,

Growth and Characterization of Single Crystals of Zinc Ferrites, Fe_3-X Zn_xO₄ (Pages: 124-132)

M. Wittenauer, P. Wang, P. Metcalf, Z. Ka̧kol, J. M. Honig, Bruce F. Collier, J. E. Greedan,

Congruent Growth of Single-Crystal La₂NiO₄ and Other Layered Nickelates by Radiofrequency Skull Melting (Pages: 133-142)

D. J. Buttrey, R. R. Schartman, J. M. Honig, Bruce F. Collier, J. E. Greedan,

Hydrothermal Synthesis and Crystal Growth of Potassium Titanyl Arsenate, Ktioaso₄ (Pages: 143-146)

Mark L. F. Phillips, Galen D. Stucky, John B. Ings,

Synthesis of La₂Ta₃Se₂O₈ Single Crystals (Pages: 146-148)

Theodore D. Brennan, James A. Ibers, L. F. Schneemeyer,

The Alkali Ternary Oxides, A_XCoO₂ and A_XCrO₂(A = Na, K) (Pages: 149-155)

C. Delmas, C. Fouassier, P. Hagenmuller, J. F. Ackerman,

Tantalum Disulfide (TaS₂) and Its Intercalation Compounds (Pages: 155-169)

J. F. Revelli, F. J. Disalvo,

Ammonia Solvated and Neat Lithium- Titanium Bisulfide Intercalates (Pages: 170-176)

M. J. Mckelvy, W. S. Glaunsinger, V. B. Cajipej,

Intercalation Compounds with Organic π-Donors: FeOCl(TTF)_1/8.5, FeOCI(TSF), _1/8.5, and FeOCi(Perylene)_1/9 (Pages: 177-180)

J. F. Bringley, B. A. Averill, David A. Cleary,

Synthesis of Tl₂Ba₂Ca_n-1Cu_nO_2n+4 (n = 1, 2, 3), (Tl,M)Sr₂Cuo_5±δ (M = Bi, Pb), and (Tl, Pb)Sr₂CaCu₂O_7+±δ (Pages: 201-207)

M. Greenblatt, L. E. H. Mcmills, S. Li, K. V. Ramanujachary, M. H. Pan, Z. Zhang, Thomas E. Sutto, Jian-Ming Zhu, Bruce, A. Averill,

Quaternary Chlorides and Bromides of the Rare-Earth Elements: Elpasolites A^I ₂ B^IRE^IIIX₆ [r (A^I) > r (B^I)] (Pages: 249-255)

Gerd Meyer, S.-J. Hwu, J. D. Corbett,

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Inorganic Syntheses: Nonmolecular Solids

About this book

Author Bios

Table of Contents

Frontmatter (Pages: i-xvii)

Part 1 : Chapter One BINARY COMPOUNDS

Tungsten Dichloride (Pages: 1-6)

Zirconium Monochloride and Monobromide (Pages: 6-11)

Lanthanum Triiodide (and Other Rare-Earth Metal Triiodides) (Pages: 11-16)

Lanthanum Diiodide (Pages: 17-19)

Rare-Earth Sesquisulfides, Ln2S3 (Pages: 20-22)

Group IV Sulfides (Pages: 22-27)

Titanium Disulfide (Pages: 28-32)

Metathetical Precursor Route to Molybdenum Disulfide (Pages: 33-37)

Lithium Nitride, Li3N (Pages: 38-45)

Aluminum Nitride (Pages: 46-50)

Electrochemical Syntheses of Binary Silver Oxides (Pages: 50-55)

Trisodium Heptaphosphide and Trisodium Undecaphosphide (Pages: 56-63)

Part 2 : Chapter Two TERNARY COMPOUNDS

Lead Ruthenium Oxide, Pb2[Ru2-XPbX 4+]O6.5 (Pages: 64-68)

Calcium Manganese Oxide, Ca2Mn3O8 (Pages: 68-72)

Ternary Chlorides and Bromides of the Rare-Earth Elements (Pages: 72-81)

Cesium Scandium(II) Trichloride (Pages: 81-84)

A One-Dimensional Polychalcogenide, K4Ti3S14 1 (Pages: 84-85)

Synthesis of K4M3Te17 (M =Zr, Hf)1 and K3Cunb2Se12 2 (Pages: 86-88)

Synthesis of Ternary Chalcogenides in Molten Polychalcogenide Salts: α-KCuQ4, KAuS5, NaBiS2, KFeQ2 (Q = S, Se) (Pages: 88-95)

Part 3 : Chapter Three CRYSTAL GROWTH

Single Crystals of Transition-Metal Dioxides (Pages: 96-104)

Molybdenum(IV) Oxide and Tungsten(IV) Oxide Single Crystals (Pages: 105-107)

Niobium Monoxide (Pages: 108-110)

Barium Titanate, Batio3 (Pages: 111-112)

Bismuth Titanate, Bi4Ti3O12 (Pages: 112-113)

Sodium Tungsten Bronzes (Pages: 114-119)

Potassium Molybdenum Oxide ‘Blue Bronze”: K0.30MoO3 (Pages: 119-124)

Growth and Characterization of Single Crystals of Zinc Ferrites, Fe3-X ZnxO4 (Pages: 124-132)

Congruent Growth of Single-Crystal La2NiO4 and Other Layered Nickelates by Radiofrequency Skull Melting (Pages: 133-142)

Hydrothermal Synthesis and Crystal Growth of Potassium Titanyl Arsenate, Ktioaso4 (Pages: 143-146)

Synthesis of La2Ta3Se2O8 Single Crystals (Pages: 146-148)

Part 4 : Chapter Four INTERCALATION COMPOUNDS

The Alkali Ternary Oxides, AXCoO2 and AXCrO2(A = Na, K) (Pages: 149-155)

Tantalum Disulfide (TaS2) and Its Intercalation Compounds (Pages: 155-169)

Ammonia Solvated and Neat Lithium- Titanium Bisulfide Intercalates (Pages: 170-176)

Intercalation Compounds with Organic π-Donors: FeOCl(TTF)1/8.5, FeOCI(TSF), 1/8.5, and FeOCi(Perylene)1/9 (Pages: 177-180)

Layered Intercalation Compounds (Pages: 181-184)

Lithium Insertion Compounds (Pages: 185-191)

Part 5 : Chapter Five OXIDE SUPERCONDUCTORS AND RELATED COMPOUNDS

Synthesis of Superconducting Oxides (Pages: 192-201)

Synthesis of Tl2Ba2Can-1CunO2n+4 (n = 1, 2, 3), (Tl,M)Sr2Cuo5±δ (M = Bi, Pb), and (Tl, Pb)Sr2CaCu2O7+±δ (Pages: 201-207)

Preparation of Ba4Bipb2 Tio12, A 10.7 K Superconductor (Pages: 208-210)

Barium Yttrium Copper Oxide Crystals (Pages: 210-218)

Synthesis of the Perovskite Series Lacuo3-δ (Pages: 218-222)

Lithium Niobium Oxide: LiNbo2 and Superconducting LiXNbO2 (Pages: 222-226)

Part 6 : Chapter Six MISCELLANEOUS SOLID-STATE COMPOUNDS

Zeolite Molecular Sieves (Pages: 227-234)

Substituted β-Aluminas (Pages: 234-241)

Vanadyl Phosphates and Organylphosphonates (Pages: 241-248)

Quaternary Chlorides and Bromides of the Rare-Earth Elements: Elpasolites AI 2 BIREIIIX6 [r (AI) > r (BI)] (Pages: 249-255)

Preparation of Ta2S2C (Pages: 255-257)

Scandium Strontium Borate, Aluminum Strontium Yttrium Borate, and Lanthanum Magnesium Strontium Borate (Pages: 257-262)

Preparation of ZrO2, Zno, and Zns Thin Films (Pages: 262-267)

Contributer Index (Pages: 269-270)

Subject Index (Pages: 271-276)

Formula Index (Pages: 277-296)

Chemical Abstracts Service Registry Number Index (Pages: 297-302)

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