Inorganic Syntheses

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About this book

The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Author Bios

Henry F. Holtzclaw Jr. is the author of Inorganic Syntheses, Volume 8, published by Wiley.

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Frontmatter (Pages: i-xv)

Alkali Metal Compounds (Page: 1)

Bis(4-imino-2-pentanonato)copper(II) and Bis(3-phenylimino-1-Phenyl-1-butanonato)Copper(II) (Pages: 2-4)

Arthur W. Struss, Dean F. Martin, Norman E. Griswold,

Complex Carbonates of Beryllium (Pages: 5-9)

A. K. Sengupta, S. Von Winbush,

Dichloro(2,2′-iminodipyridine)zinc, Diacetato(2,2′-iminodipyridine)zinc, and Dicyano(2,2′-iminodipyridine)zinc (Pages: 10-12)

Joseph Simkin, B. P. Block, John A. Broomhead,

Sodium Bis(trimethylsilyl)amide and Tris(trimethylsilyl)amine (Pages: 13-19)

Carl R. Krüger, Hans Niederprüm, Max Schmidt, O. Scherer,

Lithium Bis(trimethylsilyl)amide and Tris(trimethylsilyl)amine (Pages: 19-22)

E. H. Amonoo-Neizer, R. A. Shaw, D. O. Skovlin, B. C. Smith, Joel W. Rosenthal, William L. Jolly,

Silicon Tetraisocyanate and Methylsilicon Isocyanates (Pages: 23-27)

Roy G. Neville, John J. Mcgee, Constance Wright, Earl L. Muetterties,

Silicon Tetraisothiocyanate and Methylsilicon Isothiocyanates (Pages: 27-31)

Roy G. Neville, John J. Mcgee, Constance Wright, Earl L. Muetterties,

Tetraphenylgermane and Hexaphenyldigermane (Pages: 31-34)

Frank Glockling, K. A. Hooton, John C. Kotz, A. W. Laubengayer,

Potassium Trioxalatogermanate(IV) (Pages: 34-36)

Peter Arvedson, E. M. Larsen, George B. Kauffman, Leslie W. Michael,

Dichlorobis(2,4-pentanedionato)titanium(IV): (Correction): [Dichlorobis(acetylacetonato)Titanium (IV)] (Page: 37)

John P. Fackler Jr.,

Tris(2,4-pentanedionato)zirconium(IV) Chloride: [Tris(acetylacetonato)zirconium(IV) Chloride] (Pages: 38-40)

Vera Doron, R. K. Belitz, Stanley Kirschner, J. H. Craddock, M. M. Jones,

Potassium Tetraoxalatozirconate(IV), -Hafnate(IV), and -Thorate(IV) (Pages: 40-44)

Frederic A. Johnson, Edwin M. Larsen, Carl L. Rollinson, James Lindsay,

Metal Derivatives of β-Keto Imines (β-Imino Ketones) (Pages: 45-52)

Dean F. Martin, Edward J. Olszewski,

Ammonium Azide (Pages: 53-56)

C. O. Obenland, D. J. Mangold, M. P. Marino, T. R. Musgrave, R. N. Keller,

Phenyllead(IV) Azides (Pages: 56-63)

Eugene Lieber, Francis M. Keane, John P. Fackler Jr., James Marini, Victor Wroobel,

Tetraphosphorus Hexamethylhexaimide (Pages: 63-68)

R. R. Holmes, J. A. Forstner, C. O. Mcarthur, R. S. Drago,

Diphenyl Phosphorochloridite (Diphenyl Monochlorophosphite) (Pages: 68-71)

W. Hewertson, B. C. Smith, R. A. Shaw, R. L. Lintvedt,

Diphenylphosphinic Acid (Pages: 71-74)

L. R. Ocone, C. W. Schaumann, B. P. Block, E. N. Walsh,

(2,2-Dimethylhydrazino)-Diphenylphosphine (Pages: 74-76)

Harry H. Sisler, R. P. Nielsen, T. H. Dexter, D. J. Jaszka,

Alkoxy- and Aryloxycyclophosphazenes (Pages: 77-84)

B. W. Fitzsimmons, R. A. Shaw, George M. Nichols,

Mercapto Derivatives of Chlorocyclophosphazenes (Pages: 84-92)

A. P. Carroll, R. A. Shaw,

(Trichlorophosphoranylidene)amidophosphoryl dichloride: [Trichlorophosphazophosphorus (V) Oxychloride] (Pages: 92-94)

Margot Becke-Goehring, Ekkehard Fluck, Piero Nannelli, Therald Moeller,

Trichloro[(trichlorophosphoranylidene)amino]phosphorus (V) Hexachlorophosphate (Pages: 94-97)

Margot Becke-Goehring, Ekkehard Fluck, Morris L. Nielsen,

Hexaatomic Sulfur (Pages: 100-103)

Paul D. Bartlett, William R. Roderick, William C. Andersen,

Heptasulfur Imide (Pages: 103-105)

Margot Becke-Goehring, Ekkehard Fluck, Amedeo Failli, Therald Moeller,

Imidodisulfuric Acid Chloride (Pages: 105-107)

Margot Becke-Goehring, Ekkehard Fluck, Amedeo Failli, Therald Moeller,

Dialkylsulfamoyl Chlorides (Pages: 108-111)

Antonio Vandi, Therald Moeller, Elmer Schlemper, Henry Grote, Doyle Britton,

N- and N,N′-Substituted Sulfamides (Pages: 111-116)

Antonio Vandi, Therald Moeller, Elmer Schlemper, Doyle Britton,

Dialkylamides of (Trichlorophosphoranylidene)sulfamic Acid (Pages: 116-119)

Antonio Vandi, Therald Moeller, Sherman Thomas, Doyle Britton,

Bis(trichlorophosphoranylidene)sulfamide (Pages: 119-121)

Antonio Vandi, Therald Moeller, Henry Grote, George Grimm, Doyle Britton,

Aminomethanesulfonic Acid (Pages: 121-124)

G. Schlessinger, C. J. Nyman,

Anyhdrous Chromium(II) Acetate, Chromium(II) Acetate 1-Hydrate, and Bis(2,4-Pentanedionato)Chromium (II) (Pages: 125-132)

L. R. Ocone, B. P. Block, James P. Collman, David A. Buckingham,

Diperoxotriamminechromium(IV) (Pages: 132-135)

George B. Kauffman, Guillermo Acero, E. A. V. Ebsworth,

Tris(1,3-diphenyl-1,3-propanedionato)chromium(III) (Pages: 135-138)

Robert G. Charles, R. F. Trimble,

Tris(1,1,1-trifluoro-2,4-pentanedionato)(III) (Pages: 138-140)

Robert G. Charles, Irvin C. Brandt,

Tris(1,3-Propanedialato)chromium(III) (Pages: 141-143)

James P. Collman, Edyund T. Kittleman, William S. Hurt, Ned A. Moore, Eiichi Sekido,

cis- and trans-Tris (3-oxobutanalato)Chromium(III) (Pages: 144-148)

James P. Collyan, Eumund T. Kittleman, William S. Hurt, Ned A. Moore, Glenn Wilkes, Chin Hsuan Wei, Lawrence F. Dahl,

tris(4-p-toluidino-3-penten-2-onato)chromium(III) (Pages: 149-153)

James P. Collman, E. T. Kittleman, Norman E. Griswold,

Tris(2,4-pentanedionato)molybdenum (III) (Pages: 153-156)

Melvin L. Larson, Fred W. Moore, James Waller, Burl E. Bryant,

Potassium Tetraoxalatouranate(IV) (Pages: 157-158)

Frederic A. Johnson, Edwin M. Larsen, Carl L. Rollinson, Betty Wallace,

Sulfur Chloride Pentafluoride (Pages: 160-165)

F. Nyman, H. L. Roberts, T. Seaton, John W. George,

Trifluoromethyl Hypofluorite (Pages: 165-170)

George H. Cady, Saadideen I. Khayat, K. S. Willson,

Ammonium Perrhenate (Pages: 171-173)

Richard J. Thompson, Tung-Ch'Ing Wang, Jacob Kleinberg, George M. Adams, Burl E. Bryant,

Bis(ethylenediamine)dioxorhenium(V) Chloride, Bis(ethylenediamine)oxohydroxorhenium(V) Perchlorate, and Bis(ethylenediamine)dihydroxorhenium(V) Hexachloroplatinate(IV) (Pages: 173-177)

R. Kent Murmann, C. J. L. Lock, G. Wilkinson,

Diiron Enneacarbonyl (Pages: 178-181)

E. H. Braye, W. Hübel, Marvin D. Rausch, Thomas M. Wallace,

Triiron Dodecacarbonyl (Pages: 181-183)

W. Mcfarlane, G. Wilkinson, W. Hübel,

Tricarbonyl(cyclooctatetraene)iron (Pages: 184-185)

W. Mcfarlane, G. Wilkinson, W. Hübel,

Iron Carbonyl Complexes of Triphenylphosphine, Triphenylarsine, and Triphenylstibine (Pages: 185-191)

A. F. Clifford, A. K. Mukherjee, Donald C. Jicha, Forrest C. Hentz Jr.,

Nitrosylpentaamminecobalt(II) Chloride (Pages: 191-195)

Ole Bostrup, R. S. Tobias, Sister Sigrid Hutcheson O.S.B., W. H. Englemann,

cis-Dinitrobis(ethylenediamine)cobalt(III) Nitrite and Nitrate (Pages: 196-198)

Edward P. Harbulak, Marvin J. Albinak, Richard L. Lintvedt, Robert C. Henney, Henry F. Holtzclaw Jr.,

cis-Bromoamminebis(ethylenediamine)cobalt(III) Bromide, cis- and trans-Aquoamminebis(ethylenediamine)cobalt(III) Bromide, and cis- and trans-Aquoamminebis(ethylenediamine)cobalt(III) Nitrate (Pages: 198-202)

M. L. Tobe, Dean F. Martin, A. A. Thelen, L. Hilo, George Glover, John P. Fackler Jr.,

Sodium Tricarbonatocobaltate(III) 3-Hydrate (Pages: 202-204)

H. F. Bauer, W. C. Drinkard, Richard J. Thompson,

Potassium Tetraoxalato-Di-μ-Hydroxo-Dicobaltate(III) 3-Hydrate (Durrant's Salt) and Sodium Tetraoxalato-Di-μ-Hydroxodicobaltate(III) 5-Hydrate (Pages: 204-207)

A. M. Sargeson, I. K. Reid, John H. Bouqhton, R. N. Keller,

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