Design and Control for the Dimethyl Adipate Process with a Side-Reactor Column Configuration
Guowen Zhang
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorLe Wang
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorCorresponding Author
Jihai Tang
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Jiangsu National Synergetic Innovation Center for Advanced Materials (SICAM), 211816 Nanjing, China
Correspondence: Jihai Tang ([email protected]), Xu Qiao ([email protected]), State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, Nanjing Tech University, Nanjing, 211816, China.Search for more papers by this authorHao Jin
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorZhuxiu Zhang
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorZhaoyang Fei
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorQing Liu
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorXian Chen
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorMifen Cui
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorCorresponding Author
Xu Qiao
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Jiangsu National Synergetic Innovation Center for Advanced Materials (SICAM), 211816 Nanjing, China
Correspondence: Jihai Tang ([email protected]), Xu Qiao ([email protected]), State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, Nanjing Tech University, Nanjing, 211816, China.Search for more papers by this authorGuowen Zhang
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorLe Wang
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorCorresponding Author
Jihai Tang
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Jiangsu National Synergetic Innovation Center for Advanced Materials (SICAM), 211816 Nanjing, China
Correspondence: Jihai Tang ([email protected]), Xu Qiao ([email protected]), State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, Nanjing Tech University, Nanjing, 211816, China.Search for more papers by this authorHao Jin
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorZhuxiu Zhang
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorZhaoyang Fei
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorQing Liu
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorXian Chen
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorMifen Cui
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Search for more papers by this authorCorresponding Author
Xu Qiao
Nanjing Tech University, State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, 211816 Nanjing, China
Jiangsu National Synergetic Innovation Center for Advanced Materials (SICAM), 211816 Nanjing, China
Correspondence: Jihai Tang ([email protected]), Xu Qiao ([email protected]), State Key Laboratory of Materials-Oriented Chemical Engineering, College of Chemical Engineering, Nanjing Tech University, Nanjing, 211816, China.Search for more papers by this authorAbstract
A side-reactor column (SRC) configuration, which integrates vacuum distillation with atmospheric reaction, was developed for dimethyl adipate (DMA) production. The sequential optimization method was applied to optimize the design parameters including side stream drawn stage, reactor numbers, and catalyst loading with total annual cost (TAC) as objective function in order to realize the economical design. The best economic performance was achieved as the result of the specific SRC configuration featuring one column with 20 stages where DMA was drawn from the 5th stage and one side-reactor was equipped in the bottom. Moreover, a proportion-temperature cascade control structure was successfully developed which avoids the disturbance of inlet flow rate and composition.
Supporting Information
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