Influence of Solution Composition and Temperature on the Crystal Form of Sodium Dehydroacetate
Xia Zhang
Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China
The University of Western Ontario, Department of Chemical and Biochemical Engineering, Thompson Engineering Building, Room TEB 457, N6A 5B9 ON London, Canada
Search for more papers by this authorCorresponding Author
Qiuxiang Yin
Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China
Collaborative Innovation Center of Chemical Science and Chemical Engineering, No. 92 Weijin Road, 300072 Tianjin, China
Correspondence: Qiuxiang Yin ([email protected]), Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China; Sohrab Rohani ([email protected]) The University of Western Ontario, Department of Chemical and Biochemical Engineering, Thompson Engineering Building, Room TEB 457, London, N6A 5B9 ON, Canada.Search for more papers by this authorBaohong Hou
Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China
Collaborative Innovation Center of Chemical Science and Chemical Engineering, No. 92 Weijin Road, 300072 Tianjin, China
Search for more papers by this authorYing Bao
Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China
Collaborative Innovation Center of Chemical Science and Chemical Engineering, No. 92 Weijin Road, 300072 Tianjin, China
Search for more papers by this authorJunbo Gong
Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China
Collaborative Innovation Center of Chemical Science and Chemical Engineering, No. 92 Weijin Road, 300072 Tianjin, China
Search for more papers by this authorCorresponding Author
Sohrab Rohani
The University of Western Ontario, Department of Chemical and Biochemical Engineering, Thompson Engineering Building, Room TEB 457, N6A 5B9 ON London, Canada
Correspondence: Qiuxiang Yin ([email protected]), Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China; Sohrab Rohani ([email protected]) The University of Western Ontario, Department of Chemical and Biochemical Engineering, Thompson Engineering Building, Room TEB 457, London, N6A 5B9 ON, Canada.Search for more papers by this authorXia Zhang
Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China
The University of Western Ontario, Department of Chemical and Biochemical Engineering, Thompson Engineering Building, Room TEB 457, N6A 5B9 ON London, Canada
Search for more papers by this authorCorresponding Author
Qiuxiang Yin
Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China
Collaborative Innovation Center of Chemical Science and Chemical Engineering, No. 92 Weijin Road, 300072 Tianjin, China
Correspondence: Qiuxiang Yin ([email protected]), Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China; Sohrab Rohani ([email protected]) The University of Western Ontario, Department of Chemical and Biochemical Engineering, Thompson Engineering Building, Room TEB 457, London, N6A 5B9 ON, Canada.Search for more papers by this authorBaohong Hou
Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China
Collaborative Innovation Center of Chemical Science and Chemical Engineering, No. 92 Weijin Road, 300072 Tianjin, China
Search for more papers by this authorYing Bao
Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China
Collaborative Innovation Center of Chemical Science and Chemical Engineering, No. 92 Weijin Road, 300072 Tianjin, China
Search for more papers by this authorJunbo Gong
Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China
Collaborative Innovation Center of Chemical Science and Chemical Engineering, No. 92 Weijin Road, 300072 Tianjin, China
Search for more papers by this authorCorresponding Author
Sohrab Rohani
The University of Western Ontario, Department of Chemical and Biochemical Engineering, Thompson Engineering Building, Room TEB 457, N6A 5B9 ON London, Canada
Correspondence: Qiuxiang Yin ([email protected]), Tianjin University, State Key Laboratory of Chemical Engineering, School of Chemical Engineering and Technology, No. 92 Weijin Road, 300072 Tianjin, China; Sohrab Rohani ([email protected]) The University of Western Ontario, Department of Chemical and Biochemical Engineering, Thompson Engineering Building, Room TEB 457, London, N6A 5B9 ON, Canada.Search for more papers by this authorAbstract
The slurry transformation of sodium dehydroacetate monohydrate with different compositions of water and methanol was investigated. The water content and temperature did not only affect the solubility but also the crystal form of the precipitated material. A new needle hydrate form of sodium dehydroacetate appeared on the surface of the anhydrate when the water content was between 2 % and the critical transformation values which varied with temperature. The results revealed that the needle hydrate was a new form of sodium dehydroacetate monohydrate. A possible explanation for these observations was found in the relationship between the change of water content, the interaction between solute and solvent, and the influence of supersaturation.
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