Research Article

Adjustment of Process Conditions in Seeded Batch Cooling Crystallization

Corresponding Author

J. Prlic Kardum

[email protected]

University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, Croatia

University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, CroatiaSearch for more papers by this author

M. Hrkovac,

M. Hrkovac

University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, Croatia

Search for more papers by this author

M. Leskovac,

M. Leskovac

University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, Croatia

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J. Prlic Kardum,

Corresponding Author

J. Prlic Kardum

[email protected]

University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, Croatia

University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, CroatiaSearch for more papers by this author

M. Hrkovac,

M. Hrkovac

University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, Croatia

Search for more papers by this author

M. Leskovac,

M. Leskovac

University of Zagreb, Faculty of Chemical Engineering and Technology, Zagreb, Croatia

Search for more papers by this author

First published: 04 July 2013

https://doi.org/10.1002/ceat.201300221

Citations: 8

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Abstract

The influence of seed addition temperature, seed surface area, and seeds of different origin on granulometric characteristics and polymorphism of glycine was examined. At sufficient surface seed area, a regular and narrow crystal size distribution (CSD) was obtained. Polymorphism was investigated by differential scanning calorimetry and X-ray diffraction analysis. Differences in seed size and seed mass couple affected the granulometric properties but did not cause changes in polymorphic structure. Four experiments with different origin seeds were carried out under optimal process conditions determined by preliminary experiments. Various seed origins caused differences in supersaturation level and CSD but the structure of the obtained crystals remained the same as the loaded seed.

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Volume36, Issue8

Special Issue:Industrial Crystallization

August, 2013

Pages 1347-1354

Adjustment of Process Conditions in Seeded Batch Cooling Crystallization

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Adjustment of Process Conditions in Seeded Batch Cooling Crystallization

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