Alumina – Stabilized SEI and CEI in Potassium Metal Batteries
Corresponding Author
Pengcheng Liu
Materials Science and Engineering Program & Texas Materials Institute (TMI), The University of Texas at Austin, Austin, TX 78712–1591 USA
Contribution: Conceptualization (lead), Data curation (lead), Methodology (lead), Visualization (lead), Writing - original draft (lead), Writing - review & editing (equal)
Search for more papers by this authorCorresponding Author
Hongchang Hao
Materials Science and Engineering Program & Texas Materials Institute (TMI), The University of Texas at Austin, Austin, TX 78712–1591 USA
Contribution: Data curation (supporting), Formal analysis (supporting)
Search for more papers by this authorAditya Singla
School of Mechanical Engineering, Purdue University, West Lafayette, IN 47907 USA
Contribution: Data curation (supporting), Software (supporting), Visualization (supporting)
Search for more papers by this authorBairav S. Vishnugopi
School of Mechanical Engineering, Purdue University, West Lafayette, IN 47907 USA
Contribution: Data curation (equal), Software (equal), Visualization (supporting), Writing - original draft (supporting)
Search for more papers by this authorJohn Watt
Center for Integrated Nanotechnologies, Los Alamos National Laboratory, Los Alamos, NM 87545 USA
Contribution: Data curation (equal), Funding acquisition (supporting), Resources (equal)
Search for more papers by this authorPartha P. Mukherjee
School of Mechanical Engineering, Purdue University, West Lafayette, IN 47907 USA
Contribution: Funding acquisition (supporting), Software (lead)
Search for more papers by this authorCorresponding Author
David Mitlin
Materials Science and Engineering Program & Texas Materials Institute (TMI), The University of Texas at Austin, Austin, TX 78712–1591 USA
Contribution: Funding acquisition (lead), Project administration (lead), Supervision (lead), Writing - review & editing (lead)
Search for more papers by this authorCorresponding Author
Pengcheng Liu
Materials Science and Engineering Program & Texas Materials Institute (TMI), The University of Texas at Austin, Austin, TX 78712–1591 USA
Contribution: Conceptualization (lead), Data curation (lead), Methodology (lead), Visualization (lead), Writing - original draft (lead), Writing - review & editing (equal)
Search for more papers by this authorCorresponding Author
Hongchang Hao
Materials Science and Engineering Program & Texas Materials Institute (TMI), The University of Texas at Austin, Austin, TX 78712–1591 USA
Contribution: Data curation (supporting), Formal analysis (supporting)
Search for more papers by this authorAditya Singla
School of Mechanical Engineering, Purdue University, West Lafayette, IN 47907 USA
Contribution: Data curation (supporting), Software (supporting), Visualization (supporting)
Search for more papers by this authorBairav S. Vishnugopi
School of Mechanical Engineering, Purdue University, West Lafayette, IN 47907 USA
Contribution: Data curation (equal), Software (equal), Visualization (supporting), Writing - original draft (supporting)
Search for more papers by this authorJohn Watt
Center for Integrated Nanotechnologies, Los Alamos National Laboratory, Los Alamos, NM 87545 USA
Contribution: Data curation (equal), Funding acquisition (supporting), Resources (equal)
Search for more papers by this authorPartha P. Mukherjee
School of Mechanical Engineering, Purdue University, West Lafayette, IN 47907 USA
Contribution: Funding acquisition (supporting), Software (lead)
Search for more papers by this authorCorresponding Author
David Mitlin
Materials Science and Engineering Program & Texas Materials Institute (TMI), The University of Texas at Austin, Austin, TX 78712–1591 USA
Contribution: Funding acquisition (lead), Project administration (lead), Supervision (lead), Writing - review & editing (lead)
Search for more papers by this authorAbstract
Aluminum oxide (Al2O3) nanopowder is spin-coated onto both sides of commercial polypropene separator to create artificial solid-electrolyte interphase (SEI) and artificial cathode electrolyte interface (CEI) in potassium metal batteries (KMBs). This significantly enhances the stability, including of KMBs with Prussian Blue (PB) cathodes. For example, symmetric cells are stable after 1,000 cycles at 0.5 mA/cm2–0.5 mAh/cm2 and 3.0 mA/cm2–0.5 mAh/cm2. Alumina modified separators promote electrolyte wetting and increase ionic conductivity (0.59 vs. 0.2 mS/cm) and transference number (0.81 vs. 0.23). Cryo-stage focused ion beam (cryo-FIB) analysis of cycled modified anode demonstrates dense and planar electrodeposits, versus unmodified baseline consisting of metal filaments (dendrites) interspersed with pores and SEI. Alumina-modified CEI also suppresses elemental Fe crossover and reduces cathode cracking. Mesoscale modeling of metal – SEI interactions captures crucial role of intrinsic heterogeneities, illustrating how artificial SEI affects reaction current distribution, conductivity and morphological stability.
Conflict of interests
The authors declare no conflict of interest.
Open Research
Data Availability Statement
The data that support the findings of this study are available from the corresponding author upon reasonable request.
Supporting Information
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