• Issue

    Acta Crystallographica Section C: Volume 40, Issue 5

    715-904
    May 1984
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inorganic compounds

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Structure of dierbium decavanadate 25-hydrate, Er2V10O28.25H2O

B. E. Rivero,  G. Rigotti,  G. Punte,  A. Navaza, 
  • Pages: 715-718
  • First Published: 15 May 1984
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Structure of monoclinic rubidium dideuteriumphosphate, RbD2PO4, in the intermediate phase

T. Hagiwara,  K. Itoh,  E. Nakamura,  M. Komukae,  Y. Makita, 
  • Pages: 718-720
  • First Published: 15 May 1984
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Structure of ammonium dihydrogenphosphite, NH4H2PO3

Z. Melichar,  B. Kratochvíl,  J. Podlahová,  V. Petříček,  K. Malý,  I. Císařová, 
  • Pages: 720-722
  • First Published: 15 May 1984
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Structure of a second form of 1,2;2,3-di-μ-hydrido-μ3-tetracarbonylferrio-cyclo-tris(tricarbonylruthenium)(3Ru–Ru), H2FeRu3(CO)13

L.-Y. Hsu,  A. A. Bhattacharyya,  S. G. Shore, 
  • Pages: 722-725
  • First Published: 15 May 1984
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Structures of mercury dichloride–dipotassium dichromate (1/1), HgCl2.K2Cr2O7, and mercury dichloride–diammonium dichromate (1/1), HgCl2.(NH4)2Cr2O7

M. T. Averbuch-Pouchot,  N. El-Horr,  J. C. Guitel, 
  • Pages: 725-728
  • First Published: 15 May 1984
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Structure du triphosphate de cuivre(II) et de trisodium dodécahydraté, CuNa3P3O10.12H2O

O. Jouini,  M. Dabbabi,  M. T. Averbuch-Pouchot,  A. Durif,  J. C. Guitel, 
  • Pages: 728-730
  • First Published: 15 May 1984
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Two-layer structure of tricalcium germanate, Ca3−x[GeO4](O1−2x,F2x) with X∝0.275

F. Nishi,  Y. Takéuchi, 
  • Pages: 730-733
  • First Published: 15 May 1984
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Location and anisotropic refinement of deuterium atoms in deuterium sodium silicate–deuterium oxide (1/8) Na2D2SiO4.8D2O by neutron diffraction; hydrogen bonding at 173 K

R. L. Schmid,  J. Felsche,  G. J. McIntyre, 
  • Pages: 733-736
  • First Published: 15 May 1984

metal-organic compounds

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Structure of calcium thymidine 5'-phosphate dihydrate, Ca2+.C10H13N2O8P2−.2H2O

T. Sato, 
  • Pages: 736-738
  • First Published: 15 May 1984
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Structure of calcium 2'-deoxyadenosine 5'-phosphate pentahydrate, Ca2+.C10H12N5O6P2−.5H2O

T. Sato, 
  • Pages: 738-740
  • First Published: 15 May 1984
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Dipotassium salt of 3-hydroxy-4-mercapto-2-thioxo-3-cyclobuten-1-one dihydrate (potassium 1,3-dithiosquarate dihydrate), K2[C4O2S2].2H2O, at 140 K

R. Mattes,  G. Johann, 
  • Pages: 740-742
  • First Published: 15 May 1984
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Structures of azidobis(dimethylglyoximato)(triphenylphosphine)cobalt(III), C26H29CoN7O4P, and [4,5-bis(methoxycarbonyl)-1,2,3-triazolato]bis(dimethylglyoximato)(triphenylphosphine)cobalt(III), C32H35CoN7O8P

J. H. Nelson,  N. E. Takach,  N. Bresciani-Pahor,  L. Randaccio,  E. Zangrando, 
  • Pages: 742-746
  • First Published: 15 May 1984
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Structure of trans-bis(dimethylphenylphosphine)bis(pyrazole)platinum, [Pt(C3H4N2)2{P(CH3)2(C6H5)}2]

J. D. Oliver,  D. F. Mullica,  D. A. Grossie,  W. O. Milligan,  H. O. Perkins, 
  • Pages: 746-748
  • First Published: 15 May 1984
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trans-Chloro(dimethylamine-N)bis[dimethylglyoximato-(1–)-N,N']cobalt(III), [CoCl(C4H7N2O2)2{NH(CH3)2}]

A. T. H. Lenstra,  H. J. Geise,  S. K. Tyrlik, 
  • Pages: 749-751
  • First Published: 15 May 1984
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Structure of (5,10,15,20-tetraphenyl-21H,23H-porphinato)platinum(II), C44H28N4Pt

A. C. Hazell, 
  • Pages: 751-753
  • First Published: 15 May 1984
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Structure of bis(tetraphenylphosphonium) (dichlorodithioferrato-S,S')disulphidooxomolybdate(2–) methyl cyanide solvate, [P(C6H5)4]2.[FeCl2{MoO(S2)}(S2)].C2H3N

W. Clegg,  C. D. Garner,  P. A. Fletcher, 
  • Pages: 754-756
  • First Published: 15 May 1984
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Copper(I)–olefin complexes. Structure of 1-chloro-2-(1-2-η-cyclohexene)-μ-[hydrotri(1-pyrazolyl)borato-N:N',N'']-dicopper(I), C15H20BClCu2N6

J. S. Thompson,  J. F. Whitney, 
  • Pages: 756-759
  • First Published: 15 May 1984
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The structure of μ3-thio-μ3-tris(disulfido)-chlorato-cyclo-tris[(diethyl dioxodithiophosphato-S,S')molybdenum](3Mo–Mo), C12H30ClMo3O6P3S13

M.-Y. Shang,  J.-L. Huang,  J.-X. (C.-S. ) Lu, 
  • Pages: 759-761
  • First Published: 15 May 1984
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The structure of bis(tetraethylammonium) bis(μ-acetato-O,O')-tri-μ-chloro-pentachloro-μ3-oxo-cyclo-trimolybdate(3Mo–Mo), 2C8H20N+.C4H6Cl8Mo3O52−

M.-Y. Shang,  J.-L. Huang,  J.-X. (C.-S. ) Lu, 
  • Pages: 761-762
  • First Published: 15 May 1984
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Structure of diaquabis(4-methyl-N-8-quinolylbenzenesulphonamide-N,N')cobalt(II)–acetone (1/1), [Co(C16H13N2O2S)2(H2O)2].C3H6O

J. M. Castresana,  M. P. Elizalde,  J. M. Arrieta,  G. Germain,  J.-P. Declercq, 
  • Pages: 763-765
  • First Published: 15 May 1984
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Bis(succinimido-N,N')argentate(I) de sodium pentahydraté, Na[Ag(C4H4NO2)2].5H2O

W. Khayata,  D. Baylocq,  F. Pellerin,  N. Rodier, 
  • Pages: 765-767
  • First Published: 15 May 1984
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Structure of tetrakis(N-methylimidazole-N')copper(I) perchlorate, [Cu(C4H6N2)4][ClO4]

W. Clegg,  S. R. Acott,  C. D. Garner, 
  • Pages: 768-769
  • First Published: 15 May 1984
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The ribbon structure of catena-{μ4-(dihydrogen mellitato)-bis[bis(oxamide oxime-N,N')nickel(II)]} tetrahydrate, [Ni2(C12H2O12)(C2H6N4O2)2].4H2O

H. Endres,  A. Knieszner, 
  • Pages: 770-772
  • First Published: 15 May 1984
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Structure of bis(9-methylhypoxanthine)silver(I) nitrate dihydrate, [Ag(C6H6N4O)2](NO3).2H2O

K. Aoki,  W. Saenger, 
  • Pages: 772-775
  • First Published: 15 May 1984
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Structure of (1-methyluracilato)silver(I), [Ag(C5H5N2O2)]

K. Aoki,  W. Saenger, 
  • Pages: 775-778
  • First Published: 15 May 1984
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Structure of the copper(II) dichloride complex of 1,4,10,13-tetraoxa-7,16-diazacyclooctadecane-7,16-diacetatocopper(II) methanol solvate, [Cu(C16H28N2O8)].CuCl2.CH3OH

P. Gluziński,  J. W. Krajewski,  Z. Urbańczyk-Lipkowska,  G. D. Andreetti,  G. Bocelli, 
  • Pages: 778-781
  • First Published: 15 May 1984
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The structures of the lanthanide ethyl sulfate enneahydrates, M(C2H5SO4)3.9H2O [M = La–Lu (except Pm)], at 171 K

R. E. Gerkin,  W. J. Reppart, 
  • Pages: 781-786
  • First Published: 15 May 1984
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Structure of tricarbonylbis(triphenylphosphine)ruthenium(0)–tetrahydrofuran (2/1), [Ru(CO)3{P(C6H5)3}2].1/2C4H8O

F. Dahan,  S. Sabo,  B. Chaudret, 
  • Pages: 786-788
  • First Published: 15 May 1984
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Tetramethylammonium diiodoargentate(I), [N(CH3)4][AgI2]

K. Peters,  H. G. Von Schnering,  W. Ott,  H.-M. Seidenspinner, 
  • Pages: 789-790
  • First Published: 15 May 1984
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The structure of 1,2;3,4-bis{μ-[bis(diphenylphosphino)methane]-P,P'}-1,2;2,4;4,1-tri-μ-carbonyl-1,2,3,3,4-pentacarbonyl-tetrahedro-tetrairidium(0), C58H44Ir4O8P4

M. M. Harding,  B. S. Nicholls,  A. K. Smith, 
  • Pages: 790-793
  • First Published: 15 May 1984
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trans-Dichloro(dimethyl sulfoxide)(isopropylamine)platinum(II), C5H15Cl2NOPtS

R. Melanson,  F. D. Rochon, 
  • Pages: 793-795
  • First Published: 15 May 1984
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Trinitrato-(O,O')(triethylene glycol)europium(III), Eu(NO3)3(C6H14O4)

E. Forsellini,  U. Casellato,  G. Tomat,  R. Graziani,  P. Di Bernardo, 
  • Pages: 795-797
  • First Published: 15 May 1984
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Structures du tris(nitroso-1 éthanal oximato-N,O')ferrate(II) de tétraphénylphosphonium, [P(C6H5)4][Fe(C2H3N2O2)3], et du tris(nitroso-1 éthanal oximato-N,O')ferrate(II) de tétraphénylarsonium, [As(C6H5)4][Fe(C2H3N2O2)3]: deux exemples de dédoublement spontané des isomères optiques lors de la cristallisation

P. Gouzerh,  Y. Jeannin,  E. Miler-Srenger,  F. Valentini, 
  • Pages: 797-801
  • First Published: 15 May 1984
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Structure of disodium 1,4-piperazinedicarbodithioate hexahydrate, 2Na+.C6H8N2S42−.6H2O

J.-P. Legros,  D. Troy,  J. Galy, 
  • Pages: 801-804
  • First Published: 15 May 1984
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Digold(III) strontium octaacetate dihydrate, Au2Sr(C2H3O2)8.2H2O

P. G. Jones, 
  • Pages: 804-805
  • First Published: 15 May 1984
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The structure of two yellow tris(2,2'-bipyridine)iridium(III) complexes: bis(2,2'-bipyridine-N,N')(NH+-2,2'-bipyridinium-3-yl-N')iridium(III) trisperchlorate–water(1/1), [Ir(C10H8N2)3](ClO4)3.H2O, and tris(2,2'-bipyridine-N,N')iridium(III) trisperchlorate–water(1/2.33), [Ir(C10H8N2)3](ClO4)3.2.33H2O

A. C. Hazell,  R. G. Hazell, 
  • Pages: 806-811
  • First Published: 15 May 1984
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Structure of hexaaquairon(II) bis{tris[1,3-dimethyl-2,4,5,6(1H,3H)-pyrimidinetrone 5-oximato]ferrate(II)} dodecahydrate, [Fe(H2O)6]2+.2[Fe(C6H6N3O4)3]−.12H2O

C. Ruiz-Valero,  A. Monge,  E. Gutiérrez-Puebla,  E. Gutiérrez-Rios, 
  • Pages: 811-812
  • First Published: 15 May 1984

organic compounds

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Structure of 3,3'-(trimethylenediimino)bis(3-methyl-2-butanone oxime), C13H28N4O2

M. S. Hussain,  Mazhar-ul-Haque,  J. Ahmed, 
  • Pages: 813-816
  • First Published: 15 May 1984
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Structures of the cis and trans isomers of 2,4,6-tri-tert-butyl-2,4,6-trifluorocyclotrisilazane, C12H30F3N3Si3

W. Clegg,  G. M. Sheldrick,  D. Stalke, 
  • Pages: 816-818
  • First Published: 15 May 1984
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Structure of the 1:1 adduct of di-tert-butylfluorosilanol and pyridine N-oxide, C8H19FOSi.C5H5NO

W. Clegg,  G. M. Sheldrick,  U. Klingebiel,  D. Bentmann,  G. Henkel,  B. Krebs, 
  • Pages: 819-820
  • First Published: 15 May 1984
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Structure of sucrose octaacetate, C28H38O19, at 173 K

J. D. Oliver,  L. C. Strickland, 
  • Pages: 820-824
  • First Published: 15 May 1984
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(R,R)-Labetalol hydrochloride: determination of the absolute configuration of the high-melting polymorph, C19H25N2O3+.Cl−

P. Murray-Rust,  J. Murray-Rust,  D. Hartley,  P. Hallett,  J. Clifton, 
  • Pages: 825-828
  • First Published: 15 May 1984
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Pyridin-bortrifluorid (1/1), C5H5N.BF3

K. Töpel,  K. Hensen,  J. W. Bats, 
  • Pages: 828-830
  • First Published: 15 May 1984
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3-Chlorobiphenyl-4-carbonitrile, C13H8ClN

H. H. Sutherland,  A. Rawas, 
  • Pages: 830-832
  • First Published: 15 May 1984
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Garuganin-I, an antibiotic, C22H24O5

V. Pattabhi,  S. Krishnaswami,  E. J. Gabe, 
  • Pages: 832-834
  • First Published: 15 May 1984
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Structure of 4-(p-chlorobenzoyl)pyridine, C12H8ClNO

A. Syed,  L. I. Foss,  E. D. Stevens, 
  • Pages: 834-836
  • First Published: 15 May 1984
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β-Modifikation von Naphtho[2,3-c][1,2,5]thiadiazol-4,9-dion, C10H4N2O2S

A. Gieren,  T. Hübner,  V. Lamm, 
  • Pages: 836-839
  • First Published: 15 May 1984
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Structural studies of colchicine derivatives. III. Structure of 7-deacetamidocolchiceine, C19H20O5

J. Rius,  E. Molins,  C. Miravitlles,  A. Bladé-Font, 
  • Pages: 839-842
  • First Published: 15 May 1984
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9-Methylthioxanthenium-10-bis(methoxycarbonyl)methylide 10-oxide, C19H18O5S

I. Vicković,  W. H. Watson,  A. L. Ternay Jnr, 
  • Pages: 842-844
  • First Published: 15 May 1984
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N1-Phenylsulphanilamide, C12H12N2O2S

C. J. Brown,  D. S. Cook,  L. Sengier, 
  • Pages: 844-846
  • First Published: 15 May 1984
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Structure of 1-diphenylmethyl-3-hydroxyazetidinium chloride, C16H18NO+.Cl−

K. R. Acharya,  S. S. Tavale,  T. N. Guru Row,  K. Venkatesan, 
  • Pages: 846-848
  • First Published: 15 May 1984
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Structure of 8-chloro-1-[(dimethylamino)methyl]-6-phenyl-4H-imidazo[1,2-a][1,4]benzodiazepine, C20H19ClN4

H. J. Butcher,  T. A. Hamor, 
  • Pages: 848-850
  • First Published: 15 May 1984
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Stereochemical aspects of narcotic action. II. 9-(m-Hydroxyphenyl)-9α-methoxy-3-methyl-3-azoniabicyclo[3.3.1]nonane p-toluenesulfonate monohydrate, C16H24NO2+.C7H7O3S−.H2O

G. Hite,  P. Salva,  J. B. Anderson,  M. Rapposch,  M. Mangion,  M. Froimowitz, 
  • Pages: 850-853
  • First Published: 15 May 1984
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Methyl 8-oxotricyclo[5.4.0.02,6]undecane-1-carboxylate, C13H18O3

G. Ferguson, 
  • Pages: 853-855
  • First Published: 15 May 1984
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Covalently linked purine–pyrimidine analogs. Structure of 7-(4,6-dioxo-5-pyrimidinyl)theophylline dihydrate, C11H10N6O4.2H2O

E. Gavuzzo,  F. Mazza,  A. Tamburrini,  G. Casini,  A. Carotti, 
  • Pages: 856-858
  • First Published: 15 May 1984
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(E)-1-(2-Bromo-4,5-dimethoxyphenyl)-2-(2-hydroxy-3,4-dimethoxyphenyl)ethylene, C18H19BrO5

J. M. Arrieta,  E. Domínguez,  E. Lete,  M. J. Villa,  G. Germain, 
  • Pages: 859-861
  • First Published: 15 May 1984
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1,2,2a,4a,5,6,7,8-Octahydro-5,8-methanocyclobut[c]indene-1,1,2,2-tetracarbonitrile, C16H12N4

C. Wu,  R. P. Kashyap,  W. H. Watson,  P. D. Bartlett, 
  • Pages: 861-863
  • First Published: 15 May 1984
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rel-(1R,4S,5S,8R)-1,2,3,4,5,6,7,8-Octahydro-1,4:5,8-dimethanonaphthalene-2,2,3,3-tetracarbonitrile, C16H12N4

W. H. Watson,  R. P. Kashyap,  P. D. Bartlett,  C. Wu, 
  • Pages: 863-866
  • First Published: 15 May 1984
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rel-(1R,4S,4aR,7R)- (1) and rel-(1R,4S,4aS,7S)- (2) isomers of 1,2,3,4,4a,5,6,7-octahydro-1,4:4a,7-dimethanonaphthalene-5,5,6,6-tetracarbonitrile, C16H12N4

W. H. Watson,  R. P. Kashyap,  C. Wu,  P. D. Bartlett, 
  • Pages: 866-869
  • First Published: 15 May 1984
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Structure of 1,2-dipiperidinoethane mono-N-oxide monoperchlorate monohydrate, (C12H25N2O)+.ClO4−.H2O

M. Jaskólski,  Z. Kosturkiewicz, 
  • Pages: 869-871
  • First Published: 15 May 1984
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Structure of 1,3-di-tert-butyl-2,2,4,4-tetraisopropylcyclodisilazane, C20H46N2Si2

W. Clegg,  M. Haase,  G. M. Sheldrick,  N. Vater, 
  • Pages: 871-873
  • First Published: 15 May 1984
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Structure of 2-(1,2-dihydro-1-methyl-2-pyridylidene)-3-(4-ethoxyphenyl)-3-oxopropanenitrile, C17H16N2O2

K. R. Acharya,  S. S. Tavale,  T. N. Guru Row, 
  • Pages: 873-875
  • First Published: 15 May 1984
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Structure of 2-chloro-5-methyl-6-phenyl-3-(p-tolyl)perhydro-1,3,2λ5-oxazaphosphorine 2-oxide, C17H19ClNO2P

K. R. Acharya,  S. S. Tavale,  T. N. Guru Row, 
  • Pages: 875-877
  • First Published: 15 May 1984
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Structure of bis(trifluoroacetato)(phenyl)iodine(III), C10H5F6IO4

G. A. Stergioudis,  S. C. Kokkou,  A. P. Bozopoulos,  P. J. Rentzeperis, 
  • Pages: 877-879
  • First Published: 15 May 1984
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Structure of 2'-deoxyadenosine, C10H13N5O3

T. Sato, 
  • Pages: 880-882
  • First Published: 15 May 1984
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Structure of (3aS)-7-chloro-4-(2-dimethylaminoethyl)-8-methyl-2,3,3a,4-tetrahydro-1H-pyrrolo[2,1-c][1,2,4]benzothiadiazine 5,5-dioxide, C15H22ClN3O2S

R. Oberti,  M. T. Bernabei,  F. Forni,  R. Cameroni,  E. Galli, 
  • Pages: 882-884
  • First Published: 15 May 1984
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Structure of 2',3'-O-cyclohexylidene-4'-C-(2-methyl-2-propenyl)uridine, C19H26N2O6

W. J. Cook,  S. E. Ealick,  J. A. III. Secrist, 
  • Pages: 885-887
  • First Published: 15 May 1984
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Structureof methyl 3,3-dimethyl-7-phenylsulfinyl-1,5-dioxaspiro[5.5]undecane-9-carboxylate, C19H26O5S

M. Soriano-García,  R. A. Toscano,  G. García,  M. I. Larraza,  I. H. Sánchez, 
  • Pages: 887-889
  • First Published: 15 May 1984
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Structure of 2-(4,6-dimethyl-2-pyridyliminomethyl)phenol, C14H14N2O

C. Escobar,  M. T. Garland, 
  • Pages: 889-891
  • First Published: 15 May 1984
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Low-temperature (163 K) structure of 1,8-naphthyridine, C8H6N2

P. Dapporto,  C. A. Ghilardi,  C. Mealli,  A. Orlandini,  S. Pacinotti, 
  • Pages: 891-894
  • First Published: 15 May 1984
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Structure of the dimethylsilylamine pentamer, (C2H9NSi)5. A redetermination

A. J. Blake,  E. A. V. Ebsworth,  A. J. Welch, 
  • Pages: 895-897
  • First Published: 15 May 1984
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Structure of 1'-(p-bromophenyl)-3'-ethyl-1',3',4',5'-tetrahydro-1,2-dideoxy-d-glycero-d-gulo-heptofuranoso[1,2-d]imidazole-2'-thione, C16H21BrN2O5S

M. D. Estrada,  A. Conde,  R. Márquez, 
  • Pages: 898-901
  • First Published: 15 May 1984

short communications

Free Access

Structure of 2-amino-3,5-dibromo-N-cyclohexyl-N-methylbenzenemethanamine–salicylic acid (1:1): corrigendum

R. E. Marsh, 
  • Page: 901
  • First Published: 15 May 1984
Free Access

Structure of 2-amino-3,5-dibromo-N-cyclohexyl-N-methylbenzenemethanamine–salicylic acid (1:1) (ABCMBMA–SALA), C14H20Br2N2.C7H6O3: errata

N. Shimizu,  S. Nishigaki,  Y. Nakai,  K. Osaki, 
  • Page: 902
  • First Published: 15 May 1984
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Structure of diaqua-bis[μ-(N-salicylidene-l-phenylalaninato)-O,N,μ-O']-dicopper(II), C32H30Cu2N2O8: a reappraisal

J. E. Davies, 
  • Pages: 903-904
  • First Published: 15 May 1984