Volume 46, Issue 1 pp. 310-324
ORIGINAL ARTICLE
Open Access

An experimental study on residual stress relaxation in low-cycle fatigue of Inconel 718Plus

Vito Dattoma

Vito Dattoma

Department of Engineering for Innovation, University of Salento, Lecce, Italy

Search for more papers by this author
Marta De Giorgi

Marta De Giorgi

Department of Engineering for Innovation, University of Salento, Lecce, Italy

Search for more papers by this author
Riccardo Nobile

Corresponding Author

Riccardo Nobile

Department of Engineering for Innovation, University of Salento, Lecce, Italy

Correspondence

Riccardo Nobile, Department of Engineering for Innovation, University of Salento, Via per Monteroni, 73100 Lecce, Italy.

Email: [email protected]

Search for more papers by this author
First published: 12 October 2022

Funding information: This study received no funding.

Abstract

Residual stress relaxation induced by the application of mechanical loads is determined by the nature of residual stress, the elasto-plastic material properties, and the type of applied load. Despite the importance of the first load cycle, analytical models available in the literature generally assumed residual stress relaxation as a continuous process. Residual stress induced by machining on Inconel 718Plus superalloy cylindrical specimens was measured before and after the application of load cycles under strain control. Low-cycle fatigue tests were carried out at room temperature for different strain amplitudes, and X-ray diffraction measurements were performed before and after 10 and 100 cycles. A comprehensive analytical model was derived to describe the relaxation process associated with the initial cycles and that associated with the continuous application of load cycle, which is based on the plastic strain energy per cycle W and requires the evaluation of parameters that are only dependent on the material and not on the strain amplitude.

1 INTRODUCTION

The residual stress induced by machining is essentially caused by the mechanical and thermal effects associated with the severe plastic deformations experienced by the material. When these effects are particularly relevant, the phase and metallurgical transformations are non-negligible. The interaction and level of these factors determine the resulting residual stress field.1 Two competitive phenomena result in a wide range of residual stress fields. The first one is a mechanical effect, which is essentially governed by strain hardening, whereas the second one can be considered a thermal effect, which originates from material softening at increasing temperature. By distinguishing the two effects and ignoring the thermal aspect, we can simplify the problem and better understand why residual stress occurs during machining. Considering only the mechanical effect, the material in the vicinity of the tip is initially deformed in compression during machining and then partially moved beneath the tool, resulting in superficial tensile plastic deformation. Consequently, the surrounding material tends to limit its inelastic deformation, generating a compressive residual stress state highly localized in the superficial layer. The thermal effect originating from the dissipative phenomena associated with the relevant plastic strain is also considered, which essentially consists of heat generation and the consequent local increase in the material temperature. Because plastic deformation determines a high thermal output in a thin superficial layer, the material suffers a relevant increase in temperature. If the temperature variation is particularly high and the mechanical properties are softened by the temperature, the material exhibits plastic deformation at high temperatures. When the temperature returns to room temperature, the thermal shrinkage generates a predominantly tensile residual stress.

No consensus has been reached in the literature regarding the relative contributions of mechanical and thermal effect during cutting. Several authors2-5 have shown that the mechanical effect is predominant, and the thermal effect becomes relevant at higher cutting speeds.6 However, by limiting the observation to high strength metallic materials, it can be found that the superficial residual stress induced by machining is tensile in some cases7-10 and compressive in others,11, 12 confirming that the final nature of the superficial residual stress is the result of contrasting phenomena.2, 13

The initial residual stress state can undergo relaxation due to the mechanical loads. Understanding and accurately quantifying residual stress redistribution under cyclic mechanical loads remains an important technical challenge.

The importance of relaxation after the first load cycle (quasi-static loading) was reported in the comprehensive literature reviews by James14 and McClung.15 When the initial residual stress was relaxed, specifically after the first load cycle, the application of further cycles may produce only a gradual relaxation, as reported in previous studies.16-18 In these cases, quasi-static and cyclic relaxation occur according to the von Mises yield criterion; the superposition of the initial residual stress and external load exceeds the local monotonic or cyclic yield stress of the material.19-21 These considerations derived from experimental measurements are consistent with the results obtained by the finite element method numerical models of the relaxation phenomenon. 22-24 In particular, the effect of the plasticization behavior of the material on the residual stress relaxation was found to be particularly evident after the first load cycle and negligible in subsequent load cycles. In certain cases,25-29 residual stress measured after load application was found to be higher than the initial residual stress, and in others, the compressive residual stress became tensile. This effect is mainly observed when bending fatigue loads are applied.23, 25, 27 Other studies have considered the residual stress relaxation originating from constant and variable amplitude fatigue loads30 and determined how the process is affected by the material characteristics and surface hardening state.17, 31 The importance of the relaxation near the crack tip was also considered.32, 33

This phenomenon was analyzed also from a microscopic perspective by Qian et al. in three different types of steel.34 The authors proposed a relaxation model based on the principle of creep dislocation movement individuating the three relaxation regimes as a function of the applied stress. Xie et al.,35 in agreement with Morrow and Sinclair,36 attributed the amount of relaxation to the plastic strain accumulation with the number of cycles. Concerning this aspect, relaxation can only occur if there is some degree of plasticity in the reverse loading, both in tension and compression.37 In a recent study,38 the authors analyzed the circumstances under which continuous relaxation could arise. They concluded that a continuous residual stress modification is possible if the production of new plastic strain takes place in both the loading and reverse loading parts of a cyclic loading. They further determined that the relaxation at a small load is limited to the first cycle depending on whether the stress ratio is positive or negative. In contrast, continuous relaxation occurs if the load is sufficiently high and the stress ratio is negative.

The significance of considering the influence of the cold working rate on different volumes of material and its influence on the local material properties and therefore on the role of gradient properties on the relaxation mechanism has been demonstrated in previous studies.39, 40 This is particularly true for all residual stress fields concentrated in a superficial layer, such as those introduced by shot peening, general surface mechanical treatments, and machining. These treatments and manufacturing phases introduce cold work in the surface layer, producing a local yield strength gradient. In particular, tensile cold working increases the tensile yield strength on the surface but reduces the compressive yield strength owing to the Bauschinger effect. Consequently, the surface layer, where compressive residual stress is introduced, easily reaches the yield limit and relaxes the residual stress.

This study focuses on the phenomenon of relaxation of residual stress induced by machining in a nickel-based superalloy, characterized by superior mechanical properties at room and at elevated temperature. This class of materials is widely used to realize high-value components subjected to particularly heavy thermal and mechanical load conditions. An improvement in the mechanical behavior of such components could lead to valuable economical and technical advantages.

This study aims to describe how the chip-forming residual stress induced by machining in a nickel-based superalloy is modified by applying a fatigue load cycle under strain control at different amplitudes. Based on experimental observations, a two-stage process has been proposed for the evaluation of the residual stress relaxation. Furthermore, identifying in plastic strain energy per cycle is a suitable parameter to define an analytical model for predicting the phenomenon in the considered class of material.

1.1 Residual stress relaxation models

Semi-empirical models have been developed to predict residual stress relaxation based on experimental assessments.16, 36, 41, 42 Relaxation is considered a continuous and gradual process that ideally occurs for the entire life of the component. In several cases, the authors recognized the importance of relaxation during the first load cycle but explicitly declared that this phenomenon was not covered by their proposed model.16, 36 Relaxation models are characterized by a common framework consisting of relatively simple analytical formulations, in which the main relevant parameters (initial residual stress, applied stress/strain amplitude, number of cycles, and cyclic hardening/softening behavior) are arranged with empirical factors to obtain a good fit with the experimental data. Therefore, the need to determine these empirical factors produces a lack of generality in these relaxation models, which are not directly applicable to cases that differ from those used for developing them.

Several models maintain a general approach and therefore could be suitable for application in different cases. Morrow and Sinclair36 conducted fatigue tests on strain control. Considering the residual stress as the mean stress, they proposed the following relationship:
σ mN σ m 1 = σ y σ a σ m 1 σ a σ y b log N (1)
where σmN is the mean stress in the Nth cycle, σm1 is the mean stress in the first cycle, σa is the stress amplitude, σy is the yield stress, and b is a constant that depends on the material hardening and applied strain. This model is suitable only for a stress ratio R = −1, because in this case the residual stress can be considered the mean stress.
Similarly, Jhansale and Topper41 proposed a simple relationship between the mean stress relaxation and the number of cycles in strain control, given by
σ mN σ m 1 = N B (2)
where the symbols assume the same meaning as in Equation (1). Landgraf and Chernenkoff42 used this approach to evaluate the empirical factor B and introduced the concept of a threshold strain range for the mean stress relaxation.
Kodama16 performed residual stress measurements using X-ray diffraction on shot-peened specimens. Analyzing the results for different number of cycles, he obtained the following rule:
σ N re = A + m log N (3)
where σNre is the residual stress after N cycles, and A and m are material constants that depend on the load amplitude σa. Experimental data show that this relation is only true after the first cycle; therefore, it is not suitable for cases where residual stress relaxation occurs immediately after the first load cycle, which is typically the case.

These few examples are based on simple analytical relations; however, they lead to prediction that could be very different. Moreover, a common framework does not exist, and it is difficult to define a general model of the residual stress relaxation, which is still a complex phenomenon. In several cases, only qualitative indications can be derived, and the proposed models are often inapplicable to different experimental conditions. To overcome these difficulties, the use of plastic strain energy per cycle as an indicator of residual stress relaxation was considered in this study.

2 MATERIALS AND METHODS

Superalloys are extensively used in the aeronautical and aerospace fields, mainly for turbines and compressors production, because of their high resistance at operating temperature. The polycrystalline superalloy Inconel 718Plus could be used for turbine disk applications, because of its high-temperature strength, good corrosion resistance, and excellent workability.

Inconel 718Plus is a precipitation-hardened nickel-based material that is normally subjected to thermal treatment, which consists of double vacuum melting or triple melting. The first process ensures a good degree of microcleanliness and tight compositional control. Triple melting minimizes the possibility of macrosegregation and enhances microcleanliness.43-45

The analyzed specimens were obtained from a larger part of the forged disk using Electric Discharge Machining. After having cut three circumferential blocks, each block has been used to obtain a certain number of cylindrical bars having a diameter of 14 mm (Figure 1A). Finally, the bars were chip formed to obtain the typical geometry of the Low-Cycle Fatigue specimens, according to the ASTM E606 standard (Figure 1B). In this manner, all specimens were oriented in the circumferential direction with respect to the original forged disk. The specimens had a final diameter of 5 mm and a gauge length of 12.7 mm to prevent elastic instability. As the specimens were obtained from an Inconel 718Plus bar by turning, a residual stress state was introduced on the surface layer.

Details are in the caption following the image
(A) Disposition of specimens in the forged disk; (B) geometry of LCF specimens [Colour figure can be viewed at wileyonlinelibrary.com]

Low-cycle fatigue tests were performed using a servo-hydraulic test machine MTS810, with a load capacity of 100 kN. Triangular ramps were imposed in strain control at a frequency of 0.1 Hz to prevent specimen overheating. An axial extensometer with a gauge length of 10 mm was used to measure the longitudinal strain during tests. During the tests, the load and applied strain were acquired at 50 Hz to reconstruct hysteresis cycles. The level of the applied strain εa ranged from 0.76% to 1.33%. All tests were suspended after 10 and 100 cycles to measure the residual stress using X-ray diffraction. Finally, the test was continued up to failure, identified by a 10% drop of the maximum load of the stabilized cycle.

Residual stress in the longitudinal and circumferential directions was evaluated using X-ray diffraction in the as-machined specimens and after the application of 10 and 100 fatigue cycles to determine the residual stress relaxation. The X-ray diffraction measurement technique was selected because it is a non-destructive technique that allows the mechanical test to be suspended, and residual stress measurements can be carried out without introducing any change in the specimen geometry. The limitation of this technique is that measurement is possible only on the surface of the specimen.46 The evaluation of the in-depth residual stress is, however, a feasible means to remove a thin layer of the material by electropolishing, without altering the surroundings residual stress. This possibility has not been considered in this study because the relevant residual stress introduced by machining is on the surface, and second, the residual stress profile over depth, independent of its surface value, goes rapidly to zero.9, 47

A Rigaku ULTIMA IV diffractometer was used in the iso-inclination configuration with a Cu source (λ = 1.540562 ang.), spot size of 1 mm, voltage of 40 kV, and amperage of 40 mA. A collimator with a diameter of 1 mm was used to reduce the error induced in the circumferential direction by specimen curvature. Using a Cu source on Inconel 718, the Bragg angle 2θ = 90.4°, and the microscopic elastic constant (E/[1 + ν]) = 140 GPa.41 Under these measurement conditions, the residual stress measurement must be referred to a superficial layer of approximately 0.005 mm. For each measurement, six scans were performed for six different ψ angles, chosen in the range 0° to 30° to ensure that the values of sin2ψ are evenly spaced. The diffraction peak position was evaluated using the center of gravity method, followed by filtering and reduction of data scatter.

3 RESULTS

3.1 Static and fatigue results

A static mechanical test was performed to determine monotonic mechanical properties at room temperature (Figure 2A). Moreover, the material behavior under repeated plastic strain was evaluated. In this case, a single specimen was loaded in the strain control using blocks of 10 cyclic loads at increasing strain amplitudes up to failure. The data for the stabilized hysteresis cycle of each block were used to determine the cyclic curve (Figure 2B). The Ramberg–Osgood model was adopted for both static and cyclic behavior, which can be expressed as48
ε = ε e + ε p = σ E + σ K 1 n , (4)
ε 2 = ε e 2 + ε p 2 = σ 2 E + σ 2 K 1 n , (5)
The parameters that describe the resultant monotonic and cyclic mechanical properties could be determined (Table 1), which are consistent with the values reported in the literature.45
Details are in the caption following the image
Mechanical properties of Inconel 718Plus: (A) tensile curve; (B) cyclic curve
TABLE 1. Monotonic and cyclic mechanical properties of Inconel 718Plus
Tensile strength σR [MPa] Yield stress σy [MPa] Elastic modulus E [MPa] Elongation at break A [%] Strength coefficient K [MPa] Strain hardening exponent n Cyclic strength coefficient K′ [MPa] Cyclic strain hardening exponent n
1462 1136 219,160 23.5 1666.2 ± 1.00 0.0742 ± 0.0003 2079.1 ± 1.05 0.127 ± 0.0104
Finally, fatigue tests were outperformed by applying a constant strain amplitude. Data of all the tests are reported in Table 2, whereas Figure 3 shows the hysteresis cycles for specimens subjected to strain amplitudes of 0.9% and 1.33%. It can be observed that the experimental behavior was not affected by the test interruption. The hysteresis cycles show that the material exhibits a cyclic softening behavior, which is typical of this class of high-strength materials. The results of the fatigue tests were used to determine the strain-life curve. The Manson–Coffin relationship49, 50 accurately described the fatigue life behavior of the material, enabling the determination of the corresponding parameters (Figure 4):
ε 2 = ε e 2 + ε p 2 = σ f E 2 N f b + ε f 2 N f c , (6)
TABLE 2. Detail of low-cycle fatigue tests of Inconel 718Plus
Specimen Strain amplitude εa [%] Number of cycles to failure Nf Stress amplitude σa [MPa] Mean stress σm [MPa] Tangent modulus ENT [MPa] Elastic strain amplitude εael [%] Plastic strain amplitude εapl [%]
29G 0.760 2111 1034.4 21.1 207,364 0.472 0.288
27G 0.900 645 1110.7 −25.0 220,936 0.507 0.393
21F 1.000 337 1142.3 −37.8 205,819 0.521 0.479
22F 1.100 269 1189.5 −24.1 207,560 0.543 0.557
23F 1.200 374 1216.1 2.8 175,538 0.555 0.645
24F 1.250 374 1164.1 4.6 188,151 0.531 0.719
25G 1.330 167 1242.7 −3.9 187,290 0.567 0.763
Static 6.2239 1 0.8143 5.4096
Details are in the caption following the image
Hysteresis cycles for different strain amplitudes: (A) εa = 0.9%; (B) εa = 1.33%
Details are in the caption following the image
Strain-life curve of Inconel 718Plus at room temperature

3.2 Residual stress results

Residual stress measurements in the longitudinal direction were characterized by a very low data dispersion of the sin2ψ straight line, confirming the reliability of the measurements, although the surface was not flat owing to the curvature of the specimen. As the effect of curved surface produces an asymmetry of the diffraction peak,51 the peak position evaluated by the center of gravity method differs from the maximum peak intensity. In the longitudinal direction, the difference between the two estimated peaks fell within 0.5%, which is considered acceptable. On the contrary, the high curvature of the specimen surface in the circumferential direction determined the difference in the peak position higher than 0.5% in a limited number of cases. Therefore, these data were discarded during the data-elaboration process. Table 3 lists the longitudinal and circumferential residual stress values σL(N) and σC(N) for each specimen, where the parameters N = 0, 10, and 100 indicate the number of load cycles applied before the residual stress evaluation. The scatter of the residual stress measurements was acceptable, considering the experimental difficulty in carrying out a correct measurement on the curved surface of the specimen. The NR (Not Reliable) measurement indicates the uncorrected evaluation of the sin2ψ straight line. The initial residual stress was compressive in both the longitudinal and circumferential directions suggesting that the residual stress field that originated from machining, as a result of the material properties and typical cutting parameters adopted, was dominated by the mechanical effect, as discussed in the section 1. The residual stress was higher in the longitudinal direction with exceptions in two cases. In general, the initial residual stress, especially in the longitudinal direction, can be considered fairly uniform between different specimens, which is a preferable prerequisite for the scope of this work.

TABLE 3. Longitudinal and circumferential residual stress
Specimen Strain amplitude εa [%] Longitudinal residual stress after N cycles σL (N) [MPa] Circumferential residual stress after N cycles σC (N) [MPa]
σL(0) σL (10) σL(100) σC(0) σC (10) σC(100)
29G 0.76 −414 (±189) −545 (±73) NR −213 (±219) NR NR
27G 0.90 −437 (±163) −563 (±116) −357 (±139) −650 (±56) −245 (±88) −649 (±72)
21F 1.00 −507 (±140) −475 (±95) −585 (±157) −646 (±54) −220 (±83) N.R.
22F 1.10 −673 (±270) −364 (±27) −267 (±141) −402 (±40) −541 (±71) −715 (±104)
23F 1.20 −796 (±85) −163 (±77) −164 (±50) −314 (±44) −277 (±73) −317 (±61)
24F 1.25 −615 (±133) −29 (±65) −56 (±61) −186 (±78) −367 (±47) NR
25G 1.33 −665 (±165) −185 (±48) −2 (±54) NR −188 (±104) NR

4 DISCUSSION

The analysis of the relaxation phenomenon was restricted to the longitudinal residual stress, which is directly involved in the relaxation phenomenon because it is aligned with the direction of the applied load. In fact, the circumferential residual stress did not show a particular evolution trend with respect to the number of cycles. This is an expected behavior, as it is evident that applying a tensile load could produce a relaxation of the residual stress especially in the longitudinal direction. On the other hand, the circumferential residual stress measurements do not provide sufficient reliability to derive valid observations from a curved surface.

Despite the limited amount of experimental data, the relaxation phenomenon was observed only when the applied strain amplitude is above a threshold value εa,th, which is in agreement with the observation reported previously.42 This is evident if the longitudinal residual stresses are plotted against the number of cycles (Figure 5). In this figure, residual stress data have been presented in two separated graphs to improve readability and better interpret the data. Specimens subjected to strain amplitudes lower than 1% (Figure 5A) have been separated from those higher than 1% (Figure 5B). Thus, it is possible to ascertain that relaxation is practically absent if the applied strain amplitude is lower than the threshold value of approximately 1%. However, for the specimens subjected to a lower strain amplitude (εa < εa,th), the applied strain amplitude was sufficiently high to determine the cyclic plasticization of the material, as shown by the data reported in Table 2. Nevertheless, with cycle-by-cycle plasticization, the residual stress amount seemed to be stable against the number of cycle and did not change continuously (Figure 5A). From an empirical point of view and without any specific claim, it can be observed that the strain amplitude threshold is in good agreement with the value of the strain amplitude that corresponds to the yield stress, as described by the Ramberg–Osgood model, which has been previously suggested for the static behavior of the material.
ε a , th = σ y E + σ y K 1 n = 1.09 % , (7)
This behavior was different (Figure 5B) when a strain amplitude higher than 1% was applied (εa > εa,th). Relaxation occurred, with the majority of it concentrated in the first 10 cycles. According to the findings present in the literature,15, 16 a large amount of this relaxation can be attributed to the first load cycle, even if no measurement has been carried out to support this statement. The application of further cycles after the first 10 cycles produces a slightly change in residual stress, which is significant in cases where it exceeds the inherent scatter of the measurement process.
Details are in the caption following the image
Relaxation of residual stress against number of cycles: (A) strain amplitude lower than 1%; (B) strain amplitude higher than 1%
The percentage variation in the residual stress after N cycles was calculated to quantify the relaxation phenomenon:
σ L N = σ L N σ L 0 σ L 0 · 100 , (8)
where σL(N) is the residual stress after N load cycles (N = 10, 100 cycles) and σL(0) is the initial residual stress. A general indication of the influence of the applied load on the residual stress relaxation can be derived by relating ΔσL(N) to the applied strain amplitude εa (Figure 6). The curves show that the longitudinal residual stress was completely relaxed in specimens subjected to high strain amplitudes, particularly for strain amplitudes higher than 1.2%. For lower values of strain amplitude, but not lower than 1%, residual stress drops by approximately 50% without any relevant difference between 10 and 100 cycles. Finally, for strain amplitude lower than 1%, the relaxation falls into the scatter of the measurement and therefore must be considered as not significant.
Details are in the caption following the image
Percentage variation in the longitudinal residual stress versus the applied strain amplitude
Based on the experimental behavior described above and observations made in the past by other researchers (briefly reported in section 1), three hypotheses have been considered to formulate a model that could describe the complexity of the relaxation phenomenon.
  1. Residual stress relaxation appears only if the applied load condition is above a threshold value, expressed by a threshold strain amplitude εa,th, which has been previously identified and derived from the static behavior of the material (Equation 7).
  2. Residual stress relaxation is concentrated in the first 10 cycles, most likely in the first cycle, as observed in several works in literature.
  3. Residual stress relaxation continues after the first 10 cycles, even if this phenomenon is minimal with respect to the initial one, and the continuous relaxation after the first 10 cycles cannot be neglected especially for higher strain amplitudes.
Regarding the first statement, in a recent study,52 static four-point bending tests were performed to induce residual stresses in flat-bending specimens. Subsequently, specimens were subject to several constant cyclic strain-controlled bending loads, and the tests revealed almost cyclic stability of residual stresses for such loading, considering that the maximum strain amplitude applied was relatively low (0.20%).

Consequently, residual stress relaxation must be regarded as a two-stage evolution, activated only if a threshold stress–strain state is achieved. Moreover, each stage of relaxation can potentially be governed by different load cycle parameters.

The model proposed in this study describes this two-stage process based on the evolution of hysteresis cycles against the number of cycles. The availability of the complete fatigue data of each specimen, which allows the reconstruction of all hysteresis cycles, makes it possible to discuss the relaxation phenomenon from an energy perspective. Considering a specific load cycle, the hysteresis area can be obtained by plotting the measured stress against the applied strain. The area W represents the plastic strain energy of a unitary material volume, which is evaluated through a numerical integration of the 500 experimental stress–strain datasets available per cycle. This value is averaged over the cylindrical volume corresponding to the gauge length of the extensometer and is referred to as the specific cycle considered. The plastic strain energy per cycle W has a relatively long tradition as a damage parameter to determine the fatigue behavior in several conditions.53 In addition, the specific thermal energy per cycle Q was proposed by Meneghetti et al.54 as a fatigue damage parameter.

Figure 7 shows the parameter versus the number of cycles for each specimen, excluding the data corresponding to the first and last cycles of the test block (cycles 1, 10, 11, 100, and 101) affected by transient effects due to the testing rig control system. Moreover, the need to stop the fatigue test for carrying the X-ray measurement introduces a step in the trends (Figure 7), because the repositioning of the extensometer always results in a change in the effective gage length. This change in the plastic strain energy is particularly significant in the case of 1.25% after 100 cycles. These data must be used with caution. Despite of these experimental effects, which potentially introduce errors in the evaluation of the energy parameter, W, three notable general behaviors were observed.
  1. Specimens tested at higher strain amplitudes revealed an important reduction of the plastic strain energy W concentrated in the first 10 cycles. The reduction was quite regular and uniform; however, in two cases, the reduction was concentrated between two subsequent cycles, not necessarily in the initial phase.
  2. The trend of the plastic strain was regular and uniform between 10 and 100 cycles. Furthermore, a reduction was associated with specimens tested at higher strain amplitudes, which seemed to disappear at lower strain amplitudes. Finally, the rate of decay was proportional to the applied strain amplitude.
  3. The slope of the intermediate curves between 10 and 100 cycles was high at the maximum strain amplitude and decreased with a decrease in the strain amplitude εa.
These qualitative observations suggest the existence of a possible relationship between relaxation and plastic strain energy W: if the area of the hysteresis cycle does not change, no relaxation occurs. On the other hand, in cases in which relaxation occurs, a reduction in the hysteresis cycle is observed. Although the existence of a relationship is evident, it is not possible to establish whether the cause of the relaxation is a change in the hysteresis area or vice versa. Consequently, the plastic strain energy W can be used as an indicator to establish whether relaxation occurs. However, the experimental error associated with the measurement of the plastic strain energy W could be potentially high because its uncertainty is the product of the uncertainty of the measured stress and strain. Considering that a further error is introduced by the numerical integration of the hysteresis cycle, the values of the plastic strain energy W must be considered carefully in comparison with the stress and strain data.
Details are in the caption following the image
Plastic strain energy versus number of cycles [Colour figure can be viewed at wileyonlinelibrary.com]
Based on these considerations, parameter W was used to describe the residual stress relaxation. As previously assumed, residual stress relaxation must be considered a two-stage process. The first stage occurs primarily during the initial cycles. For this purpose, several authors have suggested that relaxation occurs primarily in the first cycle. However, a more convenient hypothesis is that this stage is concentrated in one of the initial cycles, not necessarily the first one. This phase is mainly governed by the absolute intensity of the stress–strain state. A corresponding alternative parameter is the absolute amount of plastic strain energy that characterizes the initial cycles, Win. In particular, a linear trend is assumed between the relaxation amount of the first 10 cycles and the plastic strain energy of the initial cycle:
σ L 10 σ L 0 = p W in + q , (9)
where parameters p and q solely depend on the material.

This hypothesis was confirmed by the experimental data reported in this study, as shown in Figure 8. However, Equation (9) was obtained using the data from cycle 2, which ignore the transient effect of the test control; however, the relaxation is governed by the plastic strain energy associated with the first reliable cycle.

Details are in the caption following the image
Residual stress relaxation in the initial cycles against the initial plastic strain energy Win

The second stage corresponds to the continuous relaxation associated with the application of several cycles. Practically, all the models proposed in the literature are concerned with this stage. In this phase, the amount of relaxation can be associated with the rate of change in the hysteresis cycles. As previously observed, the slope of the intermediate curves between 10 and 100 cycles (Figure 8) was high at the maximum strain amplitude. Moreover, it decreased with a decrease in the strain amplitude εa until the trend appeared horizontal for the test performed below the threshold value εa,th. This behavior can be quantified by calculating the absolute value of the plastic strain energy variation over 10 and 100 cycles (Figure 9). Accepting the hypothesis that the relaxation mechanism could be activated above a threshold value of the strain amplitude, it is reasonable to consider that the other mechanical parameters associated with that specific strain level, such as the plastic strain energy W, could act as a threshold value. Relaxation is absent when this parameter falls below the threshold value, whereas a higher relaxation amount corresponds to a higher variation in plastic strain energy. A threshold value for plastic strain energy can be determined by fixing the value of the plastic strain energy W10th measured in correspondence with the test with strain amplitude εa = 1%, which is the nearest to the threshold value εa,th = 1.09% derived from the Ramberg–Osgood model (Equation 7). This choice allows the establishment of a threshold value for the plastic strain energy that can be evaluated simply by determining the monotonic curve of the material.

Details are in the caption following the image
Identification of a threshold value for the plastic strain energy
This threshold value W10th can be used to calculate a normalized parameter for the reduction of plastic strain energy after 100 cycles as follows:
w 100 = W 100 W 10 W 10 th , (10)
The parameter w100 represents the normalized reduction in the hysteresis cycle measured between 10 and 100 cycles. Using an exponential law, a simple relationship for the calculation of the amount of residual stress relaxation after N cycles can be obtained as follows:
σ L N σ L 0 = A e β w N , (11)
where A and β are parameters depending on the material.

Applying Equation (11) to the experimental data reported in this study and considering only the specimens that were tested above the threshold strain amplitude, a good correlation of the data was obtained (Figure 10).

Details are in the caption following the image
Residual stress relaxation against normalized variation in plastic strain energy w100

5 COMPARISON WITH ALTERNATIVE RESIDUAL STRESS RELAXATION MODELS

The experimental data reported in this study were used to validate the alternative models proposed in the literature. This allows comparison of the approaches especially with respect to their generality and the effective possibility of evaluating the material parameters involved. The models reported in the literature have been developed using theoretical considerations and experimental data that differ in terms of material, nature of residual stress, and applied load. Therefore, direct application of these models to general cases is not feasible. Another complication is the need to calculate specific parameters, which are often used in the models to obtain good agreement with the experimental data. However, the aim is to highlight the peculiarities and disadvantages of the most common models.

Let us firstly consider the model proposed by Morrow and Sinclair.36 The application of the model requires the determination of the parameter b of Equation (1), which is dependent not only on the material properties but also on the applied strain. By adopting the notation used in this study to indicate the residual stress before and after N cycles, it is possible to rearrange Equation (1) to derive the analytical expression of the parameter b:
b = log 1 log N σ y σ a σ L 0 σ L N σ L 0 log σ a σ y , (12)
By substituting the experimental data into Equation (12), the value of b is obtained for each strain amplitude εa and for N = 10 and 100. The values of parameter b vary randomly with respect to εa and N (Figure 11). Therefore, we conclude that this model does not correspond with the experimental data reported in this study and it is, at least in this case, not verified.
Details are in the caption following the image
Application of the model proposed by Morrow and Sinclair: distribution of parameter b against strain amplitude εa and number of cycles N
The second model considered for the comparison was proposed by Jhansale and Topper.41 The analytical formulation of the model is expressed by Equation (2) and is particularly simple. Using the experimental data reported in this study, parameter B can be easily calculated for each strain amplitude. Plotting the values of B against the applied strain amplitude shows that B is equal to zero below a strain amplitude threshold, which indicates that no relaxation occurs (Figure 12A). This behavior was observed and proposed by Landgraf and Chernenkoff42 and is now confirmed by the experimental data of this study. Using the threshold value of strain amplitude εa,th = 1.09%, which has been calculated previously, it is possible to derive the expression of B, as shown in Figure 12B.
B = 4.8972 · ε a ε a , th 1 , (13)
Details are in the caption following the image
Evaluation of parameter B in the model proposed by Jhansale and Topper: (A) all data; (B) interpolation of data higher than strain amplitude threshold

After determining parameter B, the model proposed by Jhansale and Topper can be used to predict residual stress relaxation for the experimental data of this study, with the strain amplitude threshold considered. Figure 13 clearly shows that the prediction values of this model were comparable to the experimental values. In this case, parameter B is dependent not only on the material but also on the strain amplitude, even if a simple correlation with the applied strain exists.

Details are in the caption following the image
Prediction of residual stress relaxation using the model proposed by Jhansale and Topper

In summary, the residual stress relaxation reported in this study cannot be described using the model proposed by Morrow and Sinclair but is coherent with the model proposed by Jhansale and Topper, which was modified to consider the existence of a strain amplitude threshold for activating the relaxation process. However, both models require the derivation of experimental parameters for each applied strain amplitude, resulting in a poor generality.

6 CONCLUSIONS

In this study, the residual stress relaxation phenomenon, following the application of cyclic load in the low-cycle fatigue regime, was analyzed based on data derived from a series of experimental tests carried out on Inconel 718Plus round specimens.

Based on experimental data, the following conclusions can be drawn.
  • Relaxation occurs only if the threshold value of the stress–strain state is reached. This threshold condition can be evaluated based on the static curve of the material.
  • A two-stage relaxation process was observed owing to the availability of residual stress data after 10 and 100 cycles. The existence of two distinct relaxation stages was assumed as a starting point for defining a unique coherent model based on the evolution of the plastic energy per cycle W. The two-stage relaxation process has the merit of appropriately considering all the qualitative factors reported in the literature. Relaxation was considered a continuous phenomenon, governed by analytical formulation depending on the number of cycles N, integrated by the ascertainment that the relaxation is mainly concentrated in the initial cycles.
  • The two-stage relaxation model was successfully described using the plastic strain energy per cycle W, relating the amount of the residual stress relaxation to the initial extension of the hysteresis cycle Win through a linear relation in the first stage and to the normalized decay of plastic strain energy w100 in the second stage.
  • The proposed model has been proven to provide an accurate quantification of the residual stress relaxation by adopting parameters that are only dependent on the material and not on the strain amplitude.

ACKNOWLEDGEMENTS

Open Access Funding provided by Universita del Salento within the CRUI-CARE Agreement.

    CONFLICT OF INTEREST/COMPETING INTEREST

    The authors have no conflicts of interest to declare.

    AUTHOR CONTRIBUTIONS

    Conceptualization and methodology R.N.; experimental test M. De G. and R.N.; resources and supervision V.D.; data curation R.N.; writing—original draft preparation M. De G. and R.N.; writing—review and editing R.N.

    All authors declare that the work described has not been published before; it is not under consideration for publication anywhere else, and its publication has been approved by all co-authors, as well as by the responsible authorities—tacitly or explicitly—at the institute where the work has been carried out.

    Nomenclature

  1. A, m
  2. parameters of the Kodama model
  3. A, β
  4. parameters of the proposed model
  5. b
  6. parameter of the Morrow–Sinclair model
  7. b, c
  8. parameters of the Manson–Coffin relationship
  9. B
  10. parameter of the Jhansale–Topper model
  11. E
  12. Young's modulus
  13. ENT
  14. tangent modulus
  15. K
  16. strength coefficient
  17. K
  18. cyclic strength coefficient
  19. n
  20. strain hardening exponent
  21. n
  22. cyclic strain hardening exponent
  23. N
  24. number of applied cycles
  25. Nf
  26. number of cycles to failure
  27. p, q
  28. parameters of the proposed relaxation model
  29. Q
  30. specific thermal energy
  31. R
  32. load ratio
  33. sin2ψ
  34. angular orientation of diffraction peaks
  35. w100
  36. normalized plastic strain energy at the 100th cycle
  37. W
  38. plastic strain energy per cycle
  39. W10
  40. plastic strain energy at the 10th cycle
  41. W100
  42. plastic strain energy at the 100th cycle
  43. W10th
  44. threshold plastic strain energy of the 10th cycle
  45. Win
  46. plastic strain energy of initial cycles
  47. Bragg angle
  48. Δεe
  49. elastic strain range
  50. Δεp
  51. plastic strain range
  52. Δσ
  53. stress range
  54. ε
  55. strain
  56. εa
  57. strain amplitude
  58. εael
  59. elastic strain amplitude
  60. εapl
  61. plastic strain amplitude
  62. εa,th
  63. threshold strain amplitude
  64. εe
  65. elastic strain
  66. εf
  67. true strain fracture
  68. εp
  69. plastic strain
  70. σa
  71. stress amplitude
  72. σC(0), σC(10), σC(100), σC(N)
  73. circumferential residual stress at 0, 10, 100, and N cycles
  74. σL(0), σL(10), σL(100), σL(N)
  75. longitudinal residual stress at 0, 10, 100, and N cycles
  76. σf
  77. fatigue strength coefficient
  78. σm
  79. mean stress
  80. σm1
  81. mean stress during the first cycle
  82. σmN
  83. mean stress during the Nth cycle
  84. σNre
  85. residual stress after N cycles
  86. σR
  87. tensile strength
  88. σy
  89. yield stress
  90. ν
  91. Poisson's ratio
  92. DATA AVAILABILITY STATEMENT

    The experimental data presented in this study are available upon request from the corresponding author.

      The full text of this article hosted at iucr.org is unavailable due to technical difficulties.