High temperature gas chromatography – atomic emission detection of metalloporphyrins in crude oils

Yadi Zeng,

Yadi Zeng

Department of Chemistry, Lederle Research Tower A, University of Massachusetts, Amherst, MA 01003, USA

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Peter C. Uden,

Corresponding Author

Peter C. Uden

Department of Chemistry, Lederle Research Tower A, University of Massachusetts, Amherst, MA 01003, USA

Department of Chemistry, Lederle Research Tower A, University of Massachusetts, Amherst, MA 01003, USASearch for more papers by this author

Yadi Zeng,

Yadi Zeng

Department of Chemistry, Lederle Research Tower A, University of Massachusetts, Amherst, MA 01003, USA

Search for more papers by this author

Peter C. Uden,

Corresponding Author

Peter C. Uden

Department of Chemistry, Lederle Research Tower A, University of Massachusetts, Amherst, MA 01003, USA

Department of Chemistry, Lederle Research Tower A, University of Massachusetts, Amherst, MA 01003, USASearch for more papers by this author

First published: April 1994

https://doi.org/10.1002/jhrc.1240170407

Citations: 33

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Abstract

High temperature gas chromatography-atomic emission spectroscopy is used for the detection of vanadyl, nickel, and iron porphyrins in crude oils. The operational variables are investigated with regard to the effects on performance in high temperature GC-AED. Under optimal conditions, the method provides charactersitic metal distributions for oils from different sources. The method is also advantageous in the study of decomposition of petroleum metal species. Several crude oils were analyzed for the content of the distillable metals in comparison with total metals as determined by a direct spectroscopic method.

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Volume17, Issue4

April 1994

Pages 223-229

High temperature gas chromatography – atomic emission detection of metalloporphyrins in crude oils

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High temperature gas chromatography – atomic emission detection of metalloporphyrins in crude oils

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