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The assignment of the 1H-NMR and 13C-NMR spectra of 5H-dibenz[b,f]azepine and 10,11-dihydro-5H-dibenz[b,f]azepine
Abstract
The total assignments of the 1H-nmr and 13C-nmr spectra of 5H-dibenz[b,f]azepine [1] and 10,11-dihydro-5H-dibenz[b,f]azepine (2) have been made based on comparison with the corresponding 4,6-dideuterated derivatives 3, and 4. These compounds were prepared via repeated lithiations and subsequent deuterations of 1 and 2.
