Volume 22, Issue 3-4 pp. 294-300

Research Article

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Hydrogen bonding networks in [(η⁶-arene)Cr(CO)₃] complexes^†

Balasubramanian Murugesapandian,

Balasubramanian Murugesapandian

Institut für Anorganische Chemie, Karlsruher Institut für Technologie, Engesserstr. 15, 76131 Karlsruhe, Germany

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Peter W. Roesky,

Corresponding Author

Peter W. Roesky

[email protected]

Institut für Anorganische Chemie, Karlsruher Institut für Technologie, Engesserstr. 15, 76131 Karlsruhe, Germany

Institut für Anorganische Chemie, Karlsruher Institut für Technologie, Engesserstr. 15, 76131 Karlsruhe, GermanySearch for more papers by this author

Balasubramanian Murugesapandian,

Balasubramanian Murugesapandian

Institut für Anorganische Chemie, Karlsruher Institut für Technologie, Engesserstr. 15, 76131 Karlsruhe, Germany

Search for more papers by this author

Peter W. Roesky,

Corresponding Author

Peter W. Roesky

[email protected]

Institut für Anorganische Chemie, Karlsruher Institut für Technologie, Engesserstr. 15, 76131 Karlsruhe, Germany

Institut für Anorganische Chemie, Karlsruher Institut für Technologie, Engesserstr. 15, 76131 Karlsruhe, GermanySearch for more papers by this author

First published: 29 March 2011

https://doi.org/10.1002/hc.20679

Citations: 6

^†

Dedicated to Professor Kin-ya Akiba on the occasion of his 75th birthday.

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Abstract

The four different [(η⁶-arene)chromium tricarbonyl] complexes [(η⁶-C₆H₅CH₂COOH) Cr(CO)₃], [{η⁶-(1,2-C₆H₄(NH₂)COOEt)}Cr(CO)₃], [η⁶ -{2,6-C₆H₄(i-Pr)₂NH₂}Cr(CO)₃], and [{η⁶ -(1,4-C₆H₄(NH₂)CH₃)}Cr(CO)₃] were synthesized and structurally characterized by single crystal X-ray diffraction. All compounds form hydrogen bonds in the solid state, leading to dimeric or polymeric networks. The hydrogen bonds are an essential part of the network. The connectivity is influenced by the groups on which the protons are bound (COOH vs. NH₂) and by the steric demand of the ligand. © 2011 Wiley Periodicals, Inc. Heteroatom Chem 22:294–300, 2011; View this article online at wileyonlinelibrary.com. DOI 10.1002/hc.20679

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