Mixed Ligand Palladium(II) Complex with NS-Bidentate S-Allyldithiocarbazate Schiff Base: Synthesis, Spectral Characterization, Crystal Structure and Decoding Intermolecular Interactions with Hirshfeld Surface Analysis
Rozita Takjoo
Shirvan Azad University-Shirvan Branch, Shirvan, Iran
Search for more papers by this authorMohammad Yazdanbakhsh
Department of Chemistry, School of Sciences, Ferdowsi University of Mashhad, Mashhad 91779-1436, Iran
Search for more papers by this authorAmir Aghaei kaju
Department of Chemistry, Research Institute of Sciences & Food Technology, Khorasan Science & Technology Park, Mashhad, 91735-139, Iran
Search for more papers by this authorYaguang Chen
Faculty of Chemistry, Northeast Normal University, 138 Renmin Street, Changchun 130024, China
Search for more papers by this authorRozita Takjoo
Shirvan Azad University-Shirvan Branch, Shirvan, Iran
Search for more papers by this authorMohammad Yazdanbakhsh
Department of Chemistry, School of Sciences, Ferdowsi University of Mashhad, Mashhad 91779-1436, Iran
Search for more papers by this authorAmir Aghaei kaju
Department of Chemistry, Research Institute of Sciences & Food Technology, Khorasan Science & Technology Park, Mashhad, 91735-139, Iran
Search for more papers by this authorYaguang Chen
Faculty of Chemistry, Northeast Normal University, 138 Renmin Street, Changchun 130024, China
Search for more papers by this authorAbstract
A new mixed ligand palladium(II) complex with bidentate NS-donor chelate, [PdCl(PPh3)L] (L: S-allyl β-N-(benzylidene)dithiocarbazate), has been prepared and characterized using single crystal X-ray diffraction and spectroscopic (electronic, IR, 1H NMR and 13C NMR) techniques. The shorter PdP bond distance, 2.255(7) Å, than the sum of the single bond radii for palladium and phosphorus (2.41 Å), showed partial double bond character. Visualizing and exploring the crystal structure using Hirshfeld surface analysis showed the presence of π··· π, N··· π, CH··· π, Cl···H and weak CH···S interactions as most important intermolecular interactions in the crystal lattice, which are responsible to extension of the supramolecular network of the compound and stabilization of the crystal structure.
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