Volume 27, Issue 23
Natural Products
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ChemInform Abstract: Synthesis of 1-O-5-Substituted-deoxy-β-D-ribofuranosides with ( CH3)2As and (CH3)2As=O as Substituents at the 5-Position and a Methyl or 2′,3′-Dihydroxypropyl Group as the Aglycone in the 1-Position.

J. LIU

J. LIU

Dep. Chem., Tex. A&M Univ., College Station, TX 77843-3255, USA

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D. H. O'BRIEN

D. H. O'BRIEN

Dep. Chem., Tex. A&M Univ., College Station, TX 77843-3255, USA

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K. J. IRGOLIC

K. J. IRGOLIC

Dep. Chem., Tex. A&M Univ., College Station, TX 77843-3255, USA

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First published: June 4, 1996

Abstract

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ChemInform Abstract

The multi-step reaction sequence described provides a viable route for the preparation of multigram quantities of arsenic-containing ribofuranosides such as (IV) and (VIII) starting with the inexpensive D-ribose (I) and employing tetramethyldiarsine (III). Dimethyl(ribosyl) arsine oxides are the major arsenic compounds from marine algae species.

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