Volume 18, Issue 38
Organoelement Compounds
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ChemInform Abstract: Reaction of Phosphorus Pentachloride with Enamides. A New Access to 1,4-Azaphosphorinanes.

V. G. ROZINOV

V. G. ROZINOV

Irkutskii gos. univ. im. Zhdanova

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L. P. IZHBOLDINA

L. P. IZHBOLDINA

Irkutskii gos. univ. im. Zhdanova

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V. I. DONSKIKH

V. I. DONSKIKH

Irkutskii gos. univ. im. Zhdanova

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A. V. KALABINA

A. V. KALABINA

Irkutskii gos. univ. im. Zhdanova

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First published: September 22, 1987

Abstract

Reaction of N-butyl-N-allylacetamide (I) with phosphorus pentachloride gives the cyclic salt (II) which is treated with sulfur dioxide, forming the azaphosphorinane (III).

ChemInform Abstract

Reaction of N-butyl-N-allylacetamide (I) with phosphorus pentachloride gives the cyclic salt (II) which is treated with sulfur dioxide, forming the azaphosphorinane (III). (1H-, 31P-NMR-data).

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