Scientific advice by Jacco van Beek, René Verel, and Urban Meier and financial support by the Schweizerischer Nationalfonds, the ETH Zurich, and the Kommission für Technologie und Innovation is acknowledged.

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At the micrometer scale: Chemical interactions at the atomic level have been characterized with localized spectroscopy by using magnetic-resonance force microscopy to locate slices of 2.0 μm thickness in a heterogeneous sample (see picture). To recover the chemical-shift information, the field gradient was temporarily switched off by removing its source mechanically. This technique allows high-resolution one- and two-dimensional NMR spectra to be recorded.

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Volume47, Issue46

November 3, 2008

Pages 8961-8963

One- and Two-Dimensional NMR Spectroscopy with a Magnetic-Resonance Force Microscope^†

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One- and Two-Dimensional NMR Spectroscopy with a Magnetic-Resonance Force Microscope†

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One- and Two-Dimensional NMR Spectroscopy with a Magnetic-Resonance Force Microscope^†