Volume 162, Issue 2 pp. 623-630
Research Article

Preparation of Nd2O3 Thin Films by a Novel Sol–Gel Dipping Process

Chengyun Wang

Chengyun Wang

Department of Chemistry, University of Science and Technology of China, Hefei, Anhui 230026, People's Republic of China

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Xueguang Shao

Xueguang Shao

Department of Chemistry, University of Science and Technology of China, Hefei, Anhui 230026, People's Republic of China

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Qingde Su

Qingde Su

Department of Chemistry, University of Science and Technology of China, Hefei, Anhui 230026, People's Republic of China

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Zhiwen Cheng

Zhiwen Cheng

Structure Research Laboratory, University of Science and Technology of China, Hefei, Anhui 230026, People's Republic of China

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Guiwen Zhao

Guiwen Zhao

Department of Chemistry, University of Science and Technology of China, Hefei, Anhui 230026, People's Republic of China

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Abstract

A novel sol–gel dipping process is adopted to prepare Nd2O3 thin films with Nd(NO3)3 · 6H2O as precursor and collodion as viscosity-increasing agent. The annealing temperature of gel films is 600 °C and the thickness of Nd2O3 thin films increases linearly with the number of dippings at a rate of about 20 nm per dipping. This novel dip-coating process provides a good reproducibility of the homogeneous Nd2O3 thin films. The function of collodion is discussed. The spectral and crystal properties of the thin films are studied and the results indicate that the color of the thin films mainly results from interference.

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