Volume 11, Issue 4 pp. 276-280
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New methods of syntheses of silyl derivatives of phosphorus(V) thioacids on the basis of tetraphosphorus decasulfide, 1,3,2,4-dithiadiphosphetane-2,4-disulfides, and bis(trimethylsilyl)acetamide

Il'yas S. Nizamov

Corresponding Author

Il'yas S. Nizamov

A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Arbuzov Str. 8, 420088 Kazan, Russia

A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Arbuzov Str. 8, 420088 Kazan, RussiaSearch for more papers by this author
Alexey E. Popovich

Alexey E. Popovich

A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Arbuzov Str. 8, 420088 Kazan, Russia

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Elvira S. Batyeva

Elvira S. Batyeva

A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Arbuzov Str. 8, 420088 Kazan, Russia

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Vladimir A. Alfonsov

Vladimir A. Alfonsov

A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Arbuzov Str. 8, 420088 Kazan, Russia

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Abstract

Mixed O,S-bis- and tris(trimethylsilyl) esters of dithiophosphoric, aryldithiophosphonic and trithiophosphoric acids, 3, 7a–c, and 9, respectively, were obtained by the reactions of tetraphosphorus decasulfide 1 and 1,3,2,4-dithiadiphosphetane-2,4-disulfides 6a–c and 8 with bis(trimethylsilyl)acetamide 2. © 2000 John Wiley & Sons, Inc. Heteroatom Chem 11:276–280, 2000

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