Experimental Research on Supercritical Carbon Dioxide Fracturing of Sedimentary Rock: A Critical Review
Bowen ZHENG
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorCorresponding Author
Shengwen QI
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Corresponding author. E-mail: [email protected]Search for more papers by this authorWei LU
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorSongfeng GUO
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorZan WANG
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorXin YU
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorYan ZHANG
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorBowen ZHENG
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorCorresponding Author
Shengwen QI
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Corresponding author. E-mail: [email protected]Search for more papers by this authorWei LU
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorSongfeng GUO
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorZan WANG
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorXin YU
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorYan ZHANG
Key Laboratory of Shale Gas and Geoengineering, Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing, 100029 China
Innovation Academy for Earth Science, Chinese Academy of Sciences, Beijing, 100029 China
College of Earth and Planetary Sciences, University of Chinese Academy of Sciences, Beijing, 100029 China
Search for more papers by this authorAbout the first author:
ZHENG Bowen, male, born in 1987 in Laoting, Hebei Province, senior engineer at the Institute of Geology and Geophysics, Chinese Academy of Sciences in Beijing. His research interests focus on engineering geomechanics of rock mass and CO2 storage. E-mail: [email protected].
About the Corresponding author:
QI Shengwen, male, born in 1975 in Pengyang, Ningxia Province, professor at the Institute of Geology and Geophysics, Chinese Academy of Sciences in Beijing. His research interests focus on engineering geomechanics of rock mass and CO2 storage. E-mail: [email protected].
Abstract
Supercritical carbon dioxide (ScCO2) fracturing has great advantages and prospects in both shale gas exploitation and CO2 storage. This paper reviews current laboratory experimental methods and results for sedimentary rocks fractured by ScCO2. The breakdown pressure, fracture parameters, mineral composition, bedding plane angle and permeability are discussed. We also compare the differences between sedimentary rock and granite fractured by ScCO2, ultimately noting problems and suggesting solutions and strategies for the future. The analysis found that the breakdown pressure of ScCO2 was reduced 6.52%–52.31% compared with that of using water. ScCO2 tends to produce a complex fracture morphology with significantly higher permeability. When compared with water, the fracture aperture of ScCO2 was decreased by 4.10%–72.33%, the tortuosity of ScCO2 was increased by 5.41%–70.98% and the fractal dimension of ScCO2 was increased by 4.55%–8.41%. The breakdown pressure of sandstone is more sensitive to the nature of the fracturing fluid, but fracture aperture is less sensitive to fracturing fluid than for shale and coal. Compared with granite, the tortuosity of sedimentary rock is more sensitive to the fracturing fluid and the fracture fractal dimension is less sensitive to the fracturing fluid. Existing research shows that ScCO2 has the advantages of low breakdown pressure, good fracture creation and environmental protection. It is recommended that research be conducted in terms of sample terms, experimental conditions, effectiveness evaluation and theoretical derivation in order to promote the application of ScCO2 reformed reservoirs in the future.
References
- Al-Khulaifi, Y., Lin, Q., Blunt, M., and Bijeljic, B., 2018. Reservoir-condition pore-scale imaging of dolomite reaction with supercritical CO2 acidified brine: Effect of pore-structure on reaction rate using velocity distribution analysis. International Journal of Greenhouse Gas Control, 68: 99–111.
- Andrew, M., Bijeljic, B., and Blunt, M., 2014. Pore-scale contact angle measurements at reservoir conditions using X-Ray microtomography. Advances in Water Resources, 68: 24–31.
- Brown, D., 2000. A hot dry rock geothermal energy concept utilizing supercritical CO2 instead of water. Twenty-Fifth Workshop on Geothermal Reservoir Engineering, 1–6.
- Brunet, J.P., Li, L., Karpyn, Z., and Huerta, N., 2016. Fracture opening or self-sealing: Critical residence time as a unifying parameter for cement-CO2-brine interactions. International Journal of Greenhouse Gas Control, 47: 25–37.
- Cai, B., Li, Q., and Zhang, X., 2021. China carbon dioxide capture utilization and storage (CCUS) annual report (2021)–China CCUS pathway study. Institute of Environmental Planning, Ministry of Ecology and Environment, Wuhan Institute of Geotechnics, Chinese Academy of Sciences, The Administrative Center for China's Agenda 21 (in Chinese).
- Chen, R., Zhang, P., Qin, Y., Wei, C., and Wang, L., 2018. New discovery on methane adsorption change of coal due to ScCO2 extraction during CO2-ECBM. Acta Geologica Sinica (English Edition), 92(6): 2438–2439.
- Chen, H., Hu, Y., Kang, Y., Cai, C., Liu, J., and Liu, Y., 2019. Fracture initiation and propagation under different perforation orientation angles in supercritical CO2 fracturing. Journal of Petroleum Science and Engineering, 183: 106403.
- Chen, H., Hu, Y., Kang, Y., Wang, X., Liu, F., and Liu, Y., 2021a. Advantages of supercritical CO2 compound fracturing in shale on fracture geometry, complexity and width. Journal of Natural Gas Science and Engineering, 93(5): 104033.
- Chen, H., Hu, Y., Liu, J., Liu, F., Liu, Z., Kang, Y., and Wang, X., 2021b. Surface characteristics analysis of fractures induced by supercritical CO2 and water through three-dimensional scanning and scanning electron micrography. Journal of Rock Mechanics and Geotechnical Engineering, 13(5): 1047–1058.
- Chen, Y., Nagaya, Y., and Ishida, T., 2015. Observations of fractures induced by hydraulic fracturing in anisotropic granite. Rock Mechanics and Rock Engineering, 48(4): 1455–1461.
- Deng, B., Yin, G., Li, M., Zhang, D., Lu, J., Liu, Y., and Chen, J., 2018. Feature of fractures induced by hydrofracturing treatment using water and L-CO2 as fracturing fluids in laboratory experiments. Fuel, 226: 35–46.
- Dong, K., Jiang, M., Li, J., and Zhang, D., 2020. Research progresses in formation mechanism of complex fracture network for unconventional reservoir. Arabian Journal of Geosciences, 13(15): 1–10.
- Fang, C., Chen, W., and Amro, M., 2014. Simulation study of hydraulic fracturing using super critical CO2 in shale. Abu Dhabi International Petroleum Exhibition and Conference.
- Fujioka, M., Yamaguchi, S., and Nako, M., 2010. CO2-ECBM field tests in the Ishikari coal basin of Japan. International Journal of Coal Geology, 82(3): 287–298.
- Gan, M., Zhang, L., Miao, X., Oladyshkin, S., Cheng, X., Wang, Y., Shu, Y., Su, X., and Li, X., 2020. Application of computed tomography (CT) in geologic CO2 utilization and storage research: A critical review. Journal of Natural Gas Science and Engineering, 83: 103591.
- Gandossi, L., 2013. An overview of hydraulic fracturing and other formation stimulation technologies for shale gas production. European Commission's Joint Research Centre, 26347, Doi: 10.2790/99937.
10.2790/99937 Google Scholar
- Garing, C., Voltolini, M., Ajo-Franklin, J., and Benson, S., 2017. Pore-scale evolution of trapped CO2 at early stages following imbibition using micro-CT imaging. Energy Procedia, 114: 4872–4878.
- Guo, S., and Qi, S., 2015. Numerical study on progressive failure of hard rock samples with an unfilled undulate joint. Engineering Geology, 193: 173–182.
- Guo, S., Qi, S., Zhan, Z., Ma, L., Gure, E.G., and Zhang, S., 2020. Numerical study on the progressive failure of heterogeneous geomaterials under varied confining stresses. Engineering Geology, 269: 105556.
- Guo, S., Qi, S., Zhan, Z., and Zheng, B., 2017. Plastic-strain-dependent strength model to simulate the cracking process of brittle rocks with an existing non-persistent joint. Engineering Geology, 231: 114–125.
- Gupta, S., Jackson, T., Hlavinka, G., Evans, J., Le, H., Batrashkin, A., and Shaefer, M., 2009. Development and field application of a low pH, efficient fracturing fluid for tight gas fields in the greater Green River Basin, Wyoming. SPE Production & Operations, 24(4): 602–610.
- Ha, S.J., Kim, Y., and Yun, T.S., 2021. Development of microcracks in granitic rock by liquid CO2 fracturing. International Journal of Rock Mechanics and Mining Sciences, 146(8): 104876.
10.1016/j.ijrmms.2021.104876 Google Scholar
- Haimson, B., and Fairhurst, C., 1967. Initiation and extension of hydraulic fractures in rocks. Society of Petroleum Engineers Journal, 7(3): 310–318.
10.2118/1710-PA Google Scholar
- He, J., Afolagboye, L.O., Lin, C., and Wan, X., 2018. An experimental investigation of hydraulic fracturing in shale considering anisotropy and using freshwater and supercritical CO2. Energies, 11(3): 1–13.
- He, J., Zhang, Y., Li, X., and Wan, X., 2019. Experimental investigation on the fractures induced by hydraulic fracturing using freshwater and supercritical CO2 in shale under uniaxial stress. Rock Mechanics and Rock Engineering, 52(10): 3585–3596.
- He, Z., Li, G., Tian, S., Wang, H., Shen, Z., and Li, J., 2016. SEM analysis on rock failure mechanism by supercritical CO2 jet impingement. Journal of Petroleum Science and Engineering, 146: 111–120.
- Holditch, S., 2007. Hydraulic fracturing: Overview, trends, issues. Drilling Contractor, 63: 116–118.
- Hu, Y., Liu, F., Hu, Y., Kang, Y., Chen, H., and Liu, J., 2019. Propagation characteristics of supercritical carbon dioxide induced fractures under true tri-axial stresses. Energies, 12 (22): 4299.
- Hubbert, M.K., and Willis, D.G., 1957. Mechanics of hydraulic fracturing. Transactions of the AIME, 210(1): 153–168.
10.2118/686-G Google Scholar
- Isaka, B.L.A., Ranjith, P.G., Rathnaweera, T.D., Wanniarachchi, W.A.M., Kumari, W.G.P., and Haque, A., 2019. Testing the frackability of granite using supercritical carbon dioxide: Insights into geothermal energy systems. Journal of CO2 Utilization, 34(4): 180–197.
- Ishida, T., Aoyagi, K., Niwa, T., Chen, Y., Murata, S., Chen, Q., and Nakayama, Y., 2012. Acoustic emission monitoring of hydraulic fracturing laboratory experiment with supercritical and liquid CO2. Geophysical Research Letters, 39(16): 1–6.
10.1029/2012GL052788 Google Scholar
- Ishida, T., Chen, Y., Bennour, Z., Yamashita, H., Inui, S., Nagaya, Y., Naoi, M., Chen, Q., Nakayama, Y., and Nagano, Y., 2016. Features of CO2 fracturing deduced from acoustic emission and microscopy in laboratory experiments. Journal of Geophysical Research: Solid Earth, 121(11): 8080–8098.
- Islam, R., Sohel, R., and Hasan, F., 2022. Role of oil and gas industry in meeting climate goals through carbon capture, storage and utilization CCUS. SPE Western Regional Meeting.
- Jia, Y., Lu, Y., Elsworth, D., Fang, Y., and Tang, J., 2018. Surface characteristics and permeability enhancement of shale fractures due to water and supercritical carbon dioxide fracturing. Journal of Petroleum Science and Engineering, 165: 284–297.
- Jia, Y., Lu, Z., Liu, H., Wang, J., Cheng, Y., and Zhang, X., 2020. Fracture propagation and morphology due to non-aqueous fracturing: Competing roles between fluid characteristics and in situ stress state. Minerals, 10(5): 428.
- Jiang, Y., Qin, C., Kang, Z., Zhou, J., Li, Y., Liu, H., and Song, X., 2018. Experimental study of supercritical CO2 fracturing on initiation pressure and fracture propagation in shale under different triaxial stress conditions. Journal of Natural Gas Science and Engineering, 55: 382–394.
- Kang, J., Wei, Y., Liu, L., and Wang, J., 2021. Observing technology reserves of carbon capture and storage via patent data: Paving the way for carbon neutral. Technological Forecasting and Social Change, 171: 120933.
- Kang, S.M., Fathi, E., Ambrose, R.J., Akkutlu, I.Y., and Sigal, R.F., 2011. Carbon dioxide storage capacity of organic-rich shales. SPE Journal, 16(4): 842–855.
- Kim, K.Y., Oh, J., Han, W.S., Park, K.G., Shinn, Y., and Park, E., 2018. Two-phase flow visualization under reservoir conditions for highly heterogeneous conglomerate rock: A core-scale study for geologic carbon storage. Scientific Reports, 8(1): 4869.
- Kizaki, A., Tanaka, H., Ohashi, K., Sakaguchi, K., and Matsuki, K., 2013. Hydraulic fracturing in Inada granite and Ogino tuff using super critical carbon dioxide and water as fracturing fluids. Journal of MMIJ, 129(7): 461–466.
- Kolle, J., 2000. Coiled-tubing drilling with supercritical carbon dioxide. SPE/CIM International Conference on Horizontal Well Technology.
- Kumar, H., Elsworth, D., Mathews, J.P., and Marone, C., 2016. Permeability evolution in sorbing media: Analogies between organic-rich shale and coal. Geofluids, 16(1): 43–55.
- Kumari, W.G.P., Beaumont, D.M., Ranjith, P.G., Perera, M.S.A., Avanthi Isaka, B.L., and Khandelwal, M., 2019. An experimental study on tensile characteristics of granite rocks exposed to different high-temperature treatments. Geomechanics and Geophysics for Geo-Energy and Geo-Resources, 5(1): 47–64.
- Li, C., Liang, W., Hou, D., Yao, H., and Song, X., 2019. Comparison of fracturing features and permeability enhancement of coal fractured by water and supercritical CO2. Journal of Taiyuan University of Technology, 50: 485–491 (in Chinese with English abstract).
- Li, C., Chen, G., Li, C., Tian, B., Sun, R., Su, L., Lu, Y., and Wang, L., 2021. Experimental study on water–rock reactions with CO2 fluid in a deep sandstone formation under high temperature and pressure. Acta Geologica Sinica (English Edition), 95(1): 268–279.
- Li, Q., Chen, M., Jin, Y., Wang, M., and Zhang, H., 2012. Application of new fracturing technologies in shale gas development. Special Oil and Gas Reservoirs, 19: 1–7 (in Chinese with English abstract).
- Li, Q., Xing, H., Liu, J., and Liu, X., 2015. A review on hydraulic fracturing of unconventional reservoir. Petroleum, 1(1): 8–15.
- Li, S., Zhang, S., Ma, X., Zou, Y., Li, N., Chen, M., Cao, T., and Bo, Z., 2019. Hydraulic fractures induced by water-/carbon dioxide-based fluids in tight sandstones. Rock Mechanics and Rock Engineering, 52(9): 3323–3340.
- Li, X., Feng, Z., Han, G., Elsworth, D., Marone, C., Saffer, D., and Cheon, D.S., 2016. Breakdown pressure and fracture surface morphology of hydraulic fracturing in shale with H2O, CO2 and N2. Geomechanics and Geophysics for Geo-Energy and Geo-Resources, 2(2): 63–76.
- Liu, H., Wang, F., Zhang, J., Meng, S., and Duan, Y., 2014. Fracturing with carbon dioxide: Application status and development trend. Petroleum Exploration and Development, 41: 466–472.
- Lu, Y., Zheng, J., Ge, Z., Zhou, Z., Wang, H., and Zhang, L., 2022. A study of variation in the initiation pressure and fracture distribution patterns of raw coal in SC-CO2 fracturing under the true tri-axial system. Rock Mechanics and Rock Engineering, 55(6): 3425–3438.
- Ma, D., Cheng, C., Ding, C., Song, J., Hu, D., and Zhou, H., 2021. Comparisons of fracturing mechanism of tight sandstone using liquid CO2 and water. Journal of Natural Gas Science and Engineering, 94: 104–108.
- Meng S. M., Liu H., and Yang Q., 2019. Exploration and practice of carbon sequestration realized by CO2 waterless fracturing. Exploration and practice of carbon sequestration realized by CO2 waterless fracturing Energy Procedia, 158: 4586–4591.
- Qi, S., Lan, H., Martin, D., and Huang, X., 2020a. Factors controlling the difference in Brazilian and direct tensile strengths of the Lac du Bonnet granite. Rock Mechanics and Rock Engineering, 53(3): 1005–1019.
- Qi, S., Zheng, B., Wu, F., Huang, X., Guo, S., Zhan, Z., Zou, Y., and Barla, G., 2020b. A new dynamic direct shear testing device on rock joints. Rock Mechanics and Rock Engineering, 53(10): 4787–4798.
- Qin, T., and Cheng, H., 2010. International law issues on the technology using carbon capture and sequestration. Journal of China University of Geosciences (Social Sciences Edition), 10(5): 36–40 (in Chinese with English abstract).
- Ranjith, P.G., Zhang, C.P., and Zhang, Z.Y., 2019. Experimental study of fracturing behaviour in ultralow permeability formations: A comparison between CO2 and water fracturing. Engineering Fracture Mechanics, 217: 106541.
- Reynolds, M., Ku, R., Vertz, J., and Stashko, Z., 2013. First field application in Canada of carbon dioxide separation for hydraulic fracture flow back operations. SPE Unconventional Resources Conference Canada.
- Rodhe, H., 1990. A comparison of the contribution of various gases to the greenhouse effect. Science, 248(4960): 1217–1219.
- Saidian, M., and Prasad, M., 2015. Effect of mineralogy on nuclear magnetic resonance surface relaxivity: A case study of Middle Bakken and Three Forks formations. Fuel, 161: 197–206.
- Soong, Y., Howard, B., Dilmore, R., Haljasmaa, I., Crandall, D., Zhang, L., Zhang, W., Lin, R., Irdi, G., Romanov, V., and Mclendon, T., 2016. CO2/brine/rock interactions in Lower Tuscaloosa Formation. Greenhouse Gases: Science and Technology, 6(6): 824–837.
- Suekane, T., Soukawa, S., Iwatani, S., Tsushima, S., and Hirai, S., 2005. Behavior of supercritical CO2 injected into porous media containing water. Energy, 30(11): 2370–2382.
- Verdon, J.P., Kendall, J.M., and Maxwell, S.C., 2010. A comparison of passive seismic monitoring of fracture stimulation from water and CO2 injection. Geophysics, 75(3): 1–7.
- Wamock Jr., W.E., Harris, P., and King, D., 1985. Successful field applications of CO2-foam fracturing fluids in the Arkansas-Louisiana-Texas Region. Journal of Petroleum Technology, 37(1): 80–88.
10.2118/11932-PA Google Scholar
- Wang, H., Lun, Z., Lv, C., Lang, D., Ji, B., Luo, M., Pan, W., Wang, R., and Gong, K., 2017. Measurement and visualization of tight rock exposed to CO2 using NMR relaxometry and MRI. Scientific Reports, 7(1): 1–10.
- Wang, H., Rezaee, R., and Saeedi, A., 2015. Evaporation process and pore size distribution in tight sandstones: A study using NMR and MICP. Procedia Earth and Planetary Science, 15: 767–773.
- Wang, J., Liu, J., Li, Z., Li, H., Zhang, J., Li, W., Zhang, Y., Ping, Y., Yang, H., and Wang, P., 2020. Synchronous injection-production energy replenishment for a horizontal well in an ultra-low permeability sandstone reservoir: A case study of Changqing oilfield in Ordos Basin, NW China. Petroleum Exploration and Development, 47(4): 827–835.
- Wang, L., Yao, B., Xie, H., Winterfeld, P.H., Kneafsey, T.J., Yin, X., and Wu, Y.S., 2017. CO2 injection-induced fracturing in naturally fractured shale rocks. Energy, 139: 1094–1110.
- Wang, L., and Liang, W., 2019. Experimental study on fracture initiation and growth in coal using hydraulic fracturing with supercritical CO2 and normal water. Chinese Journal of Rock Mechanics and Engineering, 38: 2680–2689.
- Wang, X., Dang, H., and Gao, T., 2018. Method of moderate water injection and its application in ultra-low permeability oil reservoirs of Yanchang Oilfield, NW China. Petroleum Exploration and Development, 45(6): 1026–1034.
- Wu, B., Jiang, L., Liu, Y., Lv, P., Wang, D., Xingbo, L., and Song, Y., 2017. An experimental study on the influence of CO2 containing N2 on CO2 sequestration by X-ray CT scanning. Energy Procedia, 114: 4119–4128.
- Xie, H., Liu, H., and Wu, G., 2012. China's carbon dioxide emissions technology should be developed in the direction of CCU. Energy of China, 34: 15–18 (in Chinese with English abstract).
- Xu, C., Bai, B., and Liu, M., 2019. Experimental study of the fracture characteristics of granite under CO2 injection condition. Rock and Soil Mechanics, 40(4): 1474–1482.
- Yan, H., Zhang, J., Li, B., and Zhu, C., 2021. Crack propagation patterns and factors controlling complex crack network formation in coal bodies during tri-axial supercritical carbon dioxide fracturing. Fuel, 286: 119381.
- Yang, B., Wang, H., Wang, B., Shen, Z., Zheng, Y., Jia, Z., and Yan, W., 2021. Digital quantification of fracture in full-scale rock using micro-CT images: A fracturing experiment with N2 and CO2. Journal of Petroleum Science and Engineering, 196: 107682.
- Yang, B., Wang, H., Wang, B., Yi, Y., Zhao, C., and Tian, G., 2022. Effect of supercritical CO2-water/brine-rock interaction on microstructures and mechanical properties of tight sandstone. Transport in Porous Media, 1–29, Doi: 10.1007/s11242-022-01834-z">10.1007/s11242-022-01834-z.
- Yang, J., Lian, H., and Li, L., 2020. Fracturing in coals with different fluids: An experimental comparison between water, liquid CO2, and supercritical CO2. Scientific Reports, 10(1): 1–15.
- Ye, L., Zou, Y., Zhao, Q., Li, S., Ding, Y., and Ma, X., 2018. Experiment research on the CO2 fracturing fracture propagation laws of tight sandstone. Oil Drilling and Production Technology, 40: 361–368 (in Chinese with English abstract).
- Yu, Z., Liu, L., Yang, S., Li, S., and Yang, Y., 2012. An experimental study of CO2-brine-rock interaction at in situ pressure-temperature reservoir conditions. Chemical Geology, 326: 88–101.
- Zhang, J., Wang, Z., Kang, J., Song, X., and Xu, D., 2022. Several key issues for CCUS development in China targeting carbon neutrality. Carbon Neutrality, 1(1): 1–20.
- Zhang, M., He, Y., Ye, G., Lange, D., and Breugel, K., 2012. Computational investigation on mass diffusivity in Portland cement paste based on X-ray computed microtomography (μCT) image. Construction and Building Materials, 27(1): 472–481.
- Zhang, W., Sun, Q., Hao, S., Geng, J., and Lv, C., 2016. Experimental study on the variation of physical and mechanical properties of rock after high temperature treatment. Applied Thermal Engineering, 98: 1297–1304.
- Zhang, X., Lu, Y., and Tang, J., 2017. Experimental study on fracture initiation and propagation in shale using supercritical carbon dioxide fracturing. Fuel, 190: 370–378.
- Zhang, X., Li, Y., Ma, Q., and Liu, L., 2021. Development of carbon capture, utilization and storage technology in China. Strategic Study of CAE, 23: 70–80 (in Chinese with English abstract).
- Zhang, X., Zhu, W., Xu, Z., Liu, S., and Wei, C., 2022. A review of experimental apparatus for supercritical CO2 fracturing of shale. Journal of Petroleum Science and Engineering, 208: 109515.
- Zhang, Y., He, J., Li, X., and Lin, C., 2019. Experimental study on the supercritical CO2 fracturing of shale considering anisotropic effects. Journal of Petroleum Science and Engineering, 173(10): 932–940.
- Zhao, H., and Zu, E., 2017. Mineralogical characteristic and mechanical tensile strength of Xiu Yu and Lantian Yu. Journal of Gems and Gemmology, 19(5): 30–36.
- Zhao, Y., Song, Y., Liu, Y., Liang, H., and Dou, B., 2011. Visualization and measurement of CO2 flooding in porous media using MRI. Industrial and Engineering Chemistry Research, 50(8): 4707–4715.
- Zhao, Z., Li, X., He, J., Mao, T., Zheng, B., and Li, G., 2018. A laboratory investigation of fracture propagation induced by supercritical carbon dioxide fracturing in continental shale with interbeds. Journal of Petroleum Science and Engineering, 166: 739–746.
- Zheng, B., and Qi, S., 2016. A new index to describe joint roughness coefficient (JRC) under cyclic shear. Engineering Geology, 212: 72–85.
- Zheng, B., Qi, S., Guo, S., and Huang, X., 2020a. A new shear strength criterion for rock masses with non-persistent discontinuities considering the nonlinear progressive failure process. Materials, 13(21): 4694.
- Zheng, B., Qi, S., Huang, X., and Guo, S., 2020b. An advanced shear strength criterion for rock discontinuities considering size and low shear rate. Applied Sciences, 10(12): 4095.
- Zheng, B., Qi, S., Luo, G., Liu, F., Huang, X., and Guo, S., 2021. Characterization of discontinuity surface morphology based on 3D fractal dimension by integrating laser scanning with ArcGIS. Bulletin of Engineering Geology and the Environment, 80(3): 2261–2281.
- Zhou, D., Zhang, G., Wang, Y., and Xing, Y., 2018. Experimental investigation on fracture propagation modes in supercritical carbon dioxide fracturing using acoustic emission monitoring. International Journal of Rock Mechanics and Mining Sciences, 110: 111–119.
- Zou, Y., Li, N., Ma, X., Zhang, S., and Li, S., 2018. Experimental study on the growth behavior of supercritical CO2-induced fractures in a layered tight sandstone formation. Journal of Natural Gas Science and Engineering, 49: 145–156.