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Structural Characterization of a Polyaluminosilazane Precursor Prepared by Polymerizing Hexamethylcyclotrisilazane with Aluminum Acetylacetonate^†

Zeng-Yong Chu

[email protected]

Key Laboratory of New Ceramic Fibers & Composites, National University of Defense Technology, Changsha, Hunan 410073, China

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Chun-Xiang Feng,

Chun-Xiang Feng

Key Laboratory of New Ceramic Fibers & Composites, National University of Defense Technology, Changsha, Hunan 410073, China

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Yong-Cai Song,

Yong-Cai Song

Key Laboratory of New Ceramic Fibers & Composites, National University of Defense Technology, Changsha, Hunan 410073, China

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Xiao-Dong Li,

Xiao-Dong Li

Key Laboratory of New Ceramic Fibers & Composites, National University of Defense Technology, Changsha, Hunan 410073, China

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Jia-Yu Xiao,

Jia-Yu Xiao

Key Laboratory of New Ceramic Fibers & Composites, National University of Defense Technology, Changsha, Hunan 410073, China

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Zeng-Yong Chu,

Zeng-Yong Chu

[email protected]

Key Laboratory of New Ceramic Fibers & Composites, National University of Defense Technology, Changsha, Hunan 410073, China

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Chun-Xiang Feng,

Chun-Xiang Feng

Key Laboratory of New Ceramic Fibers & Composites, National University of Defense Technology, Changsha, Hunan 410073, China

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Yong-Cai Song,

Yong-Cai Song

Key Laboratory of New Ceramic Fibers & Composites, National University of Defense Technology, Changsha, Hunan 410073, China

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Xiao-Dong Li,

Xiao-Dong Li

Key Laboratory of New Ceramic Fibers & Composites, National University of Defense Technology, Changsha, Hunan 410073, China

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Jia-Yu Xiao,

Jia-Yu Xiao

Key Laboratory of New Ceramic Fibers & Composites, National University of Defense Technology, Changsha, Hunan 410073, China

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First published: 26 August 2010

https://doi.org/10.1002/cjoc.20030210751

Citations: 3

^†

Dedicated to Professor ZHOU Wei-Shan on the occasion of his 80th birthday.

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Abstract

A new polyaluminosilazane precursor was prepared by polymerizing hexamethylcyclotrisilazane (HMCTS) with aluminum acetylacetonate and the structure of the precursor was characterized by FT-IR and XPS analysis. Result shows that aluminum was incorporated mainly in form of Al—N bond. Oxygen was also detected and found that it was mainly bonded to silicon.

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Volume21, Issue7

July 2003

Pages 975-978

Structural Characterization of a Polyaluminosilazane Precursor Prepared by Polymerizing Hexamethylcyclotrisilazane with Aluminum Acetylacetonate^†

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Structural Characterization of a Polyaluminosilazane Precursor Prepared by Polymerizing Hexamethylcyclotrisilazane with Aluminum Acetylacetonate†

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Structural Characterization of a Polyaluminosilazane Precursor Prepared by Polymerizing Hexamethylcyclotrisilazane with Aluminum Acetylacetonate^†