Volume 23, Issue 22
Preparative Organic Chemistry
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ChemInform Abstract: Microwave Heating in Synthesis: Preparation of Allyldiphenylphosphine Oxide.

R. J. GIGUERE

R. J. GIGUERE

Dep. Chem. Phys., Skidmore Coll., Saratoga Springs, NY 12866-1632, USA

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B. HERBERICH

B. HERBERICH

Dep. Chem. Phys., Skidmore Coll., Saratoga Springs, NY 12866-1632, USA

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First published: June 2, 1992

Abstract

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ChemInform Abstract

Ethyl diphenylphosphinite (I) reacts with allyl bromide (II) to give the title compound (III). Application of microwave irradiation reduces the reaction time from 24h to 2 min. (Mechanism).

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