Volume 22, Issue 15
Organoelement Compounds
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ChemInform Abstract: Synthesis and Structural Characterization of Tetrakis(tert.- butyldimethylsilyl)diphosphine.

H. WESTERMANN

H. WESTERMANN

Anorg.-Chem. Inst., Univ. Bonn, W-5300 Bonn 1, Fed. Rep. Ger.

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M. NIEGER

M. NIEGER

Anorg.-Chem. Inst., Univ. Bonn, W-5300 Bonn 1, Fed. Rep. Ger.

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First published: April 16, 1991

Abstract

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ChemInform Abstract

The title compound is prepared in 38% yield from lithio-di(tert.- butyldimethylsilyl)phosphide using a method analogous to that known for (Me3Si)4P2 and crystallizes in Pbcn with Z = 4.

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