Volume 17, Issue 22
Physical Organic Chemistry
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ChemInform Abstract: Double Coupling Reaction of a Diazonium Salt with 2,10-Dimethoxy-1,6-methano[10]annulene and X-Ray Structure Analysis.

First published: June 3, 1986

Abstract

The title compound (III) is obtained by a double Coupling reaction of the annulene (I) with the diazonium salt (II).

ChemInform Abstract

The title compound (III) is obtained by a double Coupling reaction of the annulene (I) with the diazonium salt (II). The E/Z-structure of (III) is derived from its 1H NMR spectrum and is further elucidated by an X-ray analysis. Compound (III) crystallizes (with one molecule of CHCl3) in the space group P21/c; Z=4.

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