Measurement of Disodium 5'-Inosinate and Disodium 5'-Guanylate in Aqueous Ethanol by Attenuated Total Reflection Ultraviolet Method
Binghui Li
South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, 510640 Guangzhou, Tianhe District, China
Search for more papers by this authorYang Song
South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, 510640 Guangzhou, Tianhe District, China
Search for more papers by this authorLiangjie Sun
South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, 510640 Guangzhou, Tianhe District, China
Search for more papers by this authorGuoqiang Guan
South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, 510640 Guangzhou, Tianhe District, China
Search for more papers by this authorCorresponding Author
Yanbin Jiang
South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, 510640 Guangzhou, Tianhe District, China
Correspondence: Yanbin Jiang ([email protected]), South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, Tianhe District, 510640 Guangzhou, China.Search for more papers by this authorBinghui Li
South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, 510640 Guangzhou, Tianhe District, China
Search for more papers by this authorYang Song
South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, 510640 Guangzhou, Tianhe District, China
Search for more papers by this authorLiangjie Sun
South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, 510640 Guangzhou, Tianhe District, China
Search for more papers by this authorGuoqiang Guan
South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, 510640 Guangzhou, Tianhe District, China
Search for more papers by this authorCorresponding Author
Yanbin Jiang
South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, 510640 Guangzhou, Tianhe District, China
Correspondence: Yanbin Jiang ([email protected]), South China University of Technology, School of Chemistry and Chemical Engineering, 381 Wushan Road, Tianhe District, 510640 Guangzhou, China.Search for more papers by this authorAbstract
An online concentration monitoring method was established by using attenuated total reflection ultraviolet (ATR-UV) coupled with a suitable partial least squares regression for a multi-solute crystallization system, namely, disodium 5'-inosinate (IMP) and disodium 5'-guanylate (GMP) in aqueous ethanol. The results indicated that the established method accurately predicted the concentration of IMP and GMP in the solution. The solubility data was measured at various temperatures and ethanol/water mass ratios, and the experimental data was well correlated by applying the modified Apelblat equation and modified Jouyban-Acree model. The implementation of cooling crystallization demonstrates that the developed calibration model is suitable for online concentration monitoring with reasonable accuracy and precision.
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