A low pollution surface pretreatment of PC-ABS under acidic conditions
Wei Zhao
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Conceptualization (lead), Data curation (lead), Formal analysis (lead), Funding acquisition (lead), Investigation (lead), Methodology (lead), Project administration (lead), Resources (lead), Software (lead), Supervision (lead), Validation (lead), Visualization (lead), Writing - original draft (lead), Writing - review & editing (lead)
Search for more papers by this authorCorresponding Author
Wenxia Zhao
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Correspondence
Wenxia Zhao, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan 756000, China.
Email: [email protected]
Contribution: Writing - original draft (equal), Writing - review & editing (equal)
Search for more papers by this authorXinwei Li
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Investigation (equal), Methodology (supporting), Project administration (equal)
Search for more papers by this authorXin Liu
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Formal analysis (equal), Funding acquisition (equal), Investigation (supporting)
Search for more papers by this authorKaihong Hui
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Supervision (equal), Validation (equal), Visualization (supporting)
Search for more papers by this authorYifan Song
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Resources (supporting), Software (equal), Supervision (supporting)
Search for more papers by this authorHuaijun Chen
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Formal analysis (supporting), Funding acquisition (supporting)
Search for more papers by this authorYubo Cui
Department of Chemistry, Dezhou No.2 Middle School, Dezhou, China
Contribution: Validation (supporting), Visualization (supporting)
Search for more papers by this authorQian Zhu
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Resources (supporting), Software (supporting)
Search for more papers by this authorJing Liu
Medical college, Shandong Xiehe University, Jinan, China
Contribution: Software (supporting), Supervision (equal)
Search for more papers by this authorLiang Qiao
Division of Fundamental Research, Petrochina Petrochemical Research Institute, Beijing, China
Contribution: Investigation (supporting), Methodology (equal), Project administration (equal)
Search for more papers by this authorYani Yan
Department of Science, Xi'an Aerospace City No. 4 Primary School, Xi'an, China
Contribution: Software (equal), Validation (supporting)
Search for more papers by this authorWei Zhao
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Conceptualization (lead), Data curation (lead), Formal analysis (lead), Funding acquisition (lead), Investigation (lead), Methodology (lead), Project administration (lead), Resources (lead), Software (lead), Supervision (lead), Validation (lead), Visualization (lead), Writing - original draft (lead), Writing - review & editing (lead)
Search for more papers by this authorCorresponding Author
Wenxia Zhao
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Correspondence
Wenxia Zhao, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan 756000, China.
Email: [email protected]
Contribution: Writing - original draft (equal), Writing - review & editing (equal)
Search for more papers by this authorXinwei Li
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Investigation (equal), Methodology (supporting), Project administration (equal)
Search for more papers by this authorXin Liu
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Formal analysis (equal), Funding acquisition (equal), Investigation (supporting)
Search for more papers by this authorKaihong Hui
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Supervision (equal), Validation (equal), Visualization (supporting)
Search for more papers by this authorYifan Song
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Resources (supporting), Software (equal), Supervision (supporting)
Search for more papers by this authorHuaijun Chen
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Formal analysis (supporting), Funding acquisition (supporting)
Search for more papers by this authorYubo Cui
Department of Chemistry, Dezhou No.2 Middle School, Dezhou, China
Contribution: Validation (supporting), Visualization (supporting)
Search for more papers by this authorQian Zhu
College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Ningxia Key Laboratory of Green Catalytic Materials and Technology, College of Chemistry and Chemical Engineering, Ningxia Normal University, Guyuan, China
Contribution: Resources (supporting), Software (supporting)
Search for more papers by this authorJing Liu
Medical college, Shandong Xiehe University, Jinan, China
Contribution: Software (supporting), Supervision (equal)
Search for more papers by this authorLiang Qiao
Division of Fundamental Research, Petrochina Petrochemical Research Institute, Beijing, China
Contribution: Investigation (supporting), Methodology (equal), Project administration (equal)
Search for more papers by this authorYani Yan
Department of Science, Xi'an Aerospace City No. 4 Primary School, Xi'an, China
Contribution: Software (equal), Validation (supporting)
Search for more papers by this authorWei Zhao and Wenxia Zhao contributed equally to this work.
Abstract
In the present study, the low pollution acidic potassium permanganate system has been used in the study of its micro-etching effect on polycarbonate-acrylonitrile butadiene styrene (PC-ABS). Prior to micro-etching using a N methyl pyrrolidone (NMP)-glycol butyl ether solution was used as the swelling system of PC-ABS. Reasonable swelling conditions were determined, a 2-min expansion period at a temperature of 35°C with an NMP concentration of 80%. After the swelling processes, the effects of the volume ratio of :, micro-etching temperature, and micro-etching duration on the PC-ABS surface morphology, surface roughness, surface hydrophilicity, and peel strength, have been investigated. It was finally determined that the best micro-etching effect could be obtained by reacting at : = 1:2 and a temperature of 60°C for 25 min. The surface of the PC-ABS copolymers was characterized by x-ray photoelectron spectroscopy, atomic force microscopy, and Fourier-transform infrared spectroscopy. The results showed that the micro-etching process changed the morphology of the PC-ABS surface and generated cavities. In addition, the surface roughness increased from the initial Ra = 9.69 to Ra = 197 nm. Also, the water contact angle on the PC-ABS surface decreased from 92.2° to 28.6°, and the peel strength increased to 0.98 kN/m.
CONFLICT OF INTEREST STATEMENT
The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.
Open Research
DATA AVAILABILITY STATEMENT
The data that support the findings of this study are available from the corresponding author upon reasonable request..
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