Improve the interfacial properties of carbon fiber reinforced epoxy resin composites by maleimide-modified waterborne polyurethane sizing agent
Chengsen Li
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Contribution: Data curation (lead), Formal analysis (lead), Investigation (lead), Methodology (lead), Writing - original draft (lead)
Search for more papers by this authorCorresponding Author
Xueping Gao
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Correspondence
Xueping Gao and Bo Zhu, Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong 250061, China.
Email: [email protected] and [email protected]
Contribution: Data curation (supporting), Supervision (supporting), Writing - review & editing (supporting)
Search for more papers by this authorCorresponding Author
Bo Zhu
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Correspondence
Xueping Gao and Bo Zhu, Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong 250061, China.
Email: [email protected] and [email protected]
Contribution: Funding acquisition (lead)
Search for more papers by this authorXiaomin Yuan
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Contribution: Data curation (supporting), Formal analysis (supporting), Methodology (supporting)
Search for more papers by this authorZhijie Qiu
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Contribution: Data curation (supporting), Formal analysis (supporting), Methodology (supporting)
Search for more papers by this authorYe Zhang
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Contribution: Data curation (supporting), Formal analysis (supporting), Methodology (supporting)
Search for more papers by this authorShuhan Yan
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Contribution: Data curation (supporting), Formal analysis (supporting)
Search for more papers by this authorChengsen Li
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Contribution: Data curation (lead), Formal analysis (lead), Investigation (lead), Methodology (lead), Writing - original draft (lead)
Search for more papers by this authorCorresponding Author
Xueping Gao
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Correspondence
Xueping Gao and Bo Zhu, Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong 250061, China.
Email: [email protected] and [email protected]
Contribution: Data curation (supporting), Supervision (supporting), Writing - review & editing (supporting)
Search for more papers by this authorCorresponding Author
Bo Zhu
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Correspondence
Xueping Gao and Bo Zhu, Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong 250061, China.
Email: [email protected] and [email protected]
Contribution: Funding acquisition (lead)
Search for more papers by this authorXiaomin Yuan
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Contribution: Data curation (supporting), Formal analysis (supporting), Methodology (supporting)
Search for more papers by this authorZhijie Qiu
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Contribution: Data curation (supporting), Formal analysis (supporting), Methodology (supporting)
Search for more papers by this authorYe Zhang
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Contribution: Data curation (supporting), Formal analysis (supporting), Methodology (supporting)
Search for more papers by this authorShuhan Yan
Key Laboratory of Liquid-Solid Structural Evolution and Processing of Materials of Ministry of Education, State Key Laboratory of Crystal Materials, Shandong University, Jinan, Shandong, China
Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, Shandong, China
Contribution: Data curation (supporting), Formal analysis (supporting)
Search for more papers by this authorFunding information: Key Research and Development Program of Shandong Province, Grant/Award Number: 2021ZLGX01; Natural Science Foundation of Shandong Province, Grant/Award Number: ZR202105210012
Abstract
The N-(4-hydroxyphenyl) maleimide (4-HPM) modified waterborne polyurethane emulsions (MWPU) were used as surface sizing agents to improve the interfacial adhesion between carbon fibers (CF) and epoxy resin matrix. Dynamic light scattering (DLS), transmission electron microscope (TEM), and thermogravimetric analysis (TGA) showed the particle size distribution, storage stability, and thermal stability of the modified MWPU. And the surface reactivity of CF increased significantly after sizing. The interfacial shear strength (IFSS) and the interlaminar shear strength (ILSS) of CFREs were tested, and the fracture morphology was observed. The result showed that a continuous and uniform sizing layer is formed on the surface of CF. In particular, the comprehensive performance and interfacial modification effect of the MWPU emulsion outperformed other samples when the 4-HPM content was 1.0 wt%. Compared with unsized carbon fibers, the IFSS and ILSS are up to 71.30% and 30.81% higher, respectively.
Open Research
DATA AVAILABILITY STATEMENT
Research data are not shared.
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