A physical and chemical double enhancement strategy for 3D printing of cellulose reinforced nanocomposite
Bo Wang
Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorGuojiao Ding
Institute of Advanced Structure Technology, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorKen Chen
Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorShuai Jia
Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorJie Wei
Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorYongzhi Wang
Institute of Advanced Structure Technology, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorCorresponding Author
Rujie He
Institute of Advanced Structure Technology, Beijing Institute of Technology, Beijing, China
Correspondence
Rujie He, Institute of Advanced Structure Technology, Beijing Institute of Technology, Beijing 100081, China.
Email: [email protected]
Ziqiang Shao, Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing 100081, China.
Email: [email protected]
Search for more papers by this authorCorresponding Author
Ziqiang Shao
Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing, China
Correspondence
Rujie He, Institute of Advanced Structure Technology, Beijing Institute of Technology, Beijing 100081, China.
Email: [email protected]
Ziqiang Shao, Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing 100081, China.
Email: [email protected]
Search for more papers by this authorBo Wang
Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorGuojiao Ding
Institute of Advanced Structure Technology, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorKen Chen
Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorShuai Jia
Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorJie Wei
Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorYongzhi Wang
Institute of Advanced Structure Technology, Beijing Institute of Technology, Beijing, China
Search for more papers by this authorCorresponding Author
Rujie He
Institute of Advanced Structure Technology, Beijing Institute of Technology, Beijing, China
Correspondence
Rujie He, Institute of Advanced Structure Technology, Beijing Institute of Technology, Beijing 100081, China.
Email: [email protected]
Ziqiang Shao, Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing 100081, China.
Email: [email protected]
Search for more papers by this authorCorresponding Author
Ziqiang Shao
Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing, China
Correspondence
Rujie He, Institute of Advanced Structure Technology, Beijing Institute of Technology, Beijing 100081, China.
Email: [email protected]
Ziqiang Shao, Beijing Engineering Research Centre of Cellulose and Its Derivatives, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing 100081, China.
Email: [email protected]
Search for more papers by this authorFunding information: Beijing Natural Science Foundation, Grant/Award Number: 2192050
Abstract
Nanocellulose as reinforcing filler added into resin matrix has been widely used in many studies, but it remains challenging when some rigorous applications are taken into consideration. In this study, a novel nanocomposite with high performance was successfully developed for stereolithography (SLA) through physical (cellulose nanocrystal [CNC] physical enhancement) and chemical (esterification reaction) double enhancement effects during post-curing process. Compound additive (CA), composed of CNCs, butanetetracarboxylic acid, and sodium hypophosphite, were added into methacrylic acid resin to form a novel nanocomposite for SLA and post-curing. Mechanical properties of samples added with CA were better than those added with CNC only. When the content of CNC in the CA was 0.5 wt%, the sample possessed optimal mechanical properties and improved thermal stability after post-curing. Meanwhile, dynamic mechanical analysis showed that samples added with CA improved storage modulus and meaningfully increased toughness when used at near room temperature.
Supporting Information
| Filename | Description |
|---|---|
| app49164-sup-0001-supinfo.pdfPDF document, 354.7 KB | Figure S1 Tensile strength of printed samples added with different amounts of unmodified CNC. Figure S2. Variation of viscosity with shear rate of different formula resins at room temperature. Figure S3. The zoomed in FTIR spectra of 3D printed uncured (a) samples and cured (b) samples |
Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article.
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