Volume 11, Issue 2 pp. 102-106
Free to Read

Boron derivatives of dithiophosphoric acids

Il'yas S. Nizamov

Corresponding Author

Il'yas S. Nizamov

A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Arbuzov Str. 8, 420088 Kazan, Russia

A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Arbuzov Str. 8, 420088 Kazan, RussiaSearch for more papers by this author
Gul'nur G. Sergeenko

Gul'nur G. Sergeenko

A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Arbuzov Str. 8, 420088 Kazan, Russia

Search for more papers by this author
Elvira S. Batyeva

Elvira S. Batyeva

A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Arbuzov Str. 8, 420088 Kazan, Russia

Search for more papers by this author
Nail M. Azancheev

Nail M. Azancheev

A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Arbuzov Str. 8, 420088 Kazan, Russia

Search for more papers by this author
Vladimir A. Al'fonsov

Vladimir A. Al'fonsov

A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences, Arbuzov Str. 8, 420088 Kazan, Russia

Search for more papers by this author

Abstract

The reactions of tetraphosphorus decasulfide 1 with trialkyl borates 2a,b and O-isobutyl diphenylborate 2c were studied. On the basis of these studies, a novel method of synthesizing S-boron derivatives of dithiophosphoric acids was developed. The use of low frequency ultrasonic irradiation (22 kHz, power 130 W) leads to a reduction in reaction temperature and time required for completion of the reactions studied. © 2000 John Wiley & Sons, Inc. Heteroatom Chem 11:102–106, 2000

The full text of this article hosted at iucr.org is unavailable due to technical difficulties.